Article(id=1297161221699032062, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, articleNumber=null, orderNo=null, doi=10.13550/j.jxhg.20250294, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1745683200000, receivedDateStr=2025-04-27, revisedDate=null, revisedDateStr=null, acceptedDate=1747584000000, acceptedDateStr=2025-05-19, onlineDate=1787196935343, onlineDateStr=2026-08-20, pubDate=1778774400000, pubDateStr=2026-05-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1787196935343, onlineIssueDateStr=2026-08-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1787196935343, creator=13701087609, updateTime=1787196935343, updator=13701087609, issue=Issue{id=1297161216049308076, tenantId=1146029695717560320, journalId=1296125381406982186, year='2026', volume='43', issue='5', pageStart='929', pageEnd='1184', issueExtLink='null', onlineDate='null', pubDate='1778774400000', pubDateStr='2026-05-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1787196933996, creator='13701087609', updateTime=1787202244949, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1297183491922354645, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1297183491922354646, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=990, endPage=997, ext={EN=ArticleExt(id=1297161221858415615, articleId=1297161221699032062, tenantId=1146029695717560320, journalId=1296125381406982186, language=EN, title=Preparation and thermochromic behavior of palygorskite/Cr-doped BiVO₄ composite materials, columnId=null, journalTitle=Fine Chemicals, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A series of Cr³⁺ doped BiVO₄ (Cr-BiVO₄) and palygorskite (PGS)/Cr-BiVO₄ composite materials were prepared by hydrothermal method using Bi(NO₃)₃•5H₂O, NH₄VO₃, Cr₂O₃ and PGS as raw materials, and characterized by XRD, SEM, TEM and UV-Vis for analyses on structure, composition, morphology and optical performance. The thermochromic behavior of the composite materials was evaluated, with the color change mechanism speculated. The results indicated that the doping of Cr³⁺and PGS showed no effect on the monoclinic phase of BiVO₄ but widened the absorption range of the material in the visible light region. The maximum absorption edge of 30% Cr-BiVO₄ with a Cr³⁺ doping content (based on the mass of BiVO₄, the same below) redshifted from 536 nm to 634 nm and the absorbance was enhanced. Both Cr-BiVO₄ and PGS/Cr-BiVO₄ displayed reversible thermochromic properties at 20~500 ℃. Compared with that of BiVO₄ (from bright yellow to red, r.t.~300 ℃), the color changing temperature of 30% Cr-BiVO₄ decreased 100 ℃ and achieved reversible change between dark orange and red at r.t.~200 ℃. 30% Cr-BiVO₄ could repeat reversible thermochromic behavior more than 12 times at 20~500 ℃. Meanwhile, the water-based coating from 20% PGS/30% Cr-BiVO₄ composite materials prepared with 20% mass fraction of PGS exhibited reversible thermochromic between orange yellow to red. The phase transition between the monoclinic and tetragonal phases of BiVO₄ in the composite material was the fundamental cause for its reversible thermochromic property.

, authors=Danfeng YU¹, Xueli SONG¹, Xue'e MA¹, Yue CHANG^{1, 2, 3, *}, Fei ZHA¹, authorsList=Danfeng YU, Xueli SONG, Xue'e MA, Yue CHANG, Fei ZHA, authorCompany=null, correspAuthors=Yue CHANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1297161222210736128, articleId=1297161221699032062, tenantId=1146029695717560320, journalId=1296125381406982186, language=CN, title=坡缕石/Cr掺杂BiVO₄复合材料的制备及热致变色行为, columnId=1297161221933913088, journalTitle=精细化工, columnName=功能材料, runingTitle=null, highlight=null, articleAbstract=

以Bi(NO₃)₃•5H₂O、NH₄VO₃、Cr₂O₃和坡缕石（PGS）为原料，通过水热法制备了一系列Cr³⁺掺杂BiVO₄（Cr-BiVO₄）和PGS/Cr-BiVO₄复合材料。采用XRD、SEM、TEM、UV-Vis对样品结构组成、微观形貌、光学性能进行了表征，考察了复合材料的热致变色行为，并推测了其机理。结果表明，Cr³⁺、PGS的掺杂对BiVO₄的单斜晶相无影响，拓宽了其在可见光区的吸收区域，Cr³⁺掺杂量（以BiVO₄质量计，下同）30%的Cr-BiVO₄（30% Cr-BiVO₄）最大吸收边缘从水热法BiVO₄的536 nm移至634 nm，并且吸光度增强。在20~500 ℃，Cr-BiVO₄、PGS/Cr-BiVO₄均具有可逆热致变色性能，相比BiVO₄在室温~300 ℃的亮黄色与红色的可逆变化，30% Cr-BiVO₄热致变红色的温度降低了100 ℃，在室温~200 ℃实现了深橙色与红色的可逆变化，20~500 ℃可重复12次以上可逆热致变色行为。PGS质量分数20%的20% PGS/30% Cr-BiVO₄复合材料的水性涂层在浅橙黄色与红色可逆变色。复合材料中BiVO₄单斜相与四方相间的相变是引起其可逆热致变色的根本原因。

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余丹凤（2000—），女，硕士生，E-mail: 2963996886@qq.com。

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余丹凤（2000—），女，硕士生，E-mail: 2963996886@qq.com。

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