Article(id=1297161222466597562, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, articleNumber=null, orderNo=null, doi=10.13550/j.jxhg.20250179, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1742227200000, receivedDateStr=2025-03-18, revisedDate=null, revisedDateStr=null, acceptedDate=1744819200000, acceptedDateStr=2025-04-17, onlineDate=1787196935525, onlineDateStr=2026-08-20, pubDate=1778774400000, pubDateStr=2026-05-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1787196935525, onlineIssueDateStr=2026-08-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1787196935525, creator=13701087609, updateTime=1787196935525, updator=13701087609, issue=Issue{id=1297161216049308076, tenantId=1146029695717560320, journalId=1296125381406982186, year='2026', volume='43', issue='5', pageStart='929', pageEnd='1184', issueExtLink='null', onlineDate='null', pubDate='1778774400000', pubDateStr='2026-05-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1787196933996, creator='13701087609', updateTime=1787202244949, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1297183491922354645, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1297183491922354646, tenantId=1146029695717560320, journalId=1296125381406982186, issueId=1297161216049308076, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1008, endPage=1020, ext={EN=ArticleExt(id=1297161222667924155, articleId=1297161222466597562, tenantId=1146029695717560320, journalId=1296125381406982186, language=EN, title=Preparation of ZIF-8/BiOI heterojunction and its performance in activating PMS for visible light catalytic degradation of Orange Ⅱ, columnId=null, journalTitle=Fine Chemicals, columnName=null, runingTitle=null, highlight=null, articleAbstract=

3D spherical visible light catalyst ZIF-8/BiOI composites was prepared from Bi(NO₃)₃•5H₂O, KI and self-made metal-organic framework material ZIF-8 by ethylene glycol solvothermal method, characterized by XRD, FTIR, SEM, EDS, BET and UV-Vis, and evaluated for its performance in activating peroxymonosulfate (PMS) oxidation to remove sodium 4-(2-hydroxy-1-naphthalenazo) benzenesulfonate (Orange Ⅱ) under light conditions. The effects of ZIF-8 addition amount (based on the mass of BiOI, the same below) and reaction conditions on the degradation rate of Orange Ⅱ were investigated, while the mechanism of Orange Ⅱ oxidative removal by activated PMS with ZIF-8/BiOI composites was speculated. The results showed that ZIF-8/BiOI composites exhibited good visible light response performance. Under the conditions of 500 mg/L ZIF-8/BiOI with 10% ZIF-8 as catalyst, 350 W xenon lamp simulated illumination, 0.5 mmol/L PMS, 100 mg/L Orange Ⅱ, adjust initial pH of solution 7.0, and 60 min, the degradation rate of Orange Ⅱ reached as high as 95.4%. The reaction process conformed to the first-order kinetic model. and showed a significant effect while , Cl⁻, and displayed almost no influence on the reaction system. The 10%ZIF-8/BiOI also showed good reusability, with the degradation rate of Orange Ⅱ at 60 min still could reach 83.2% after 4 recycles. Hydroxyl radicals, singlet oxygen and holes were the main active substances in the degradation process, with sulfate radicals playing an auxiliary role. During the degradation process, the holes and electrons of BiOI and ZIF-8 were transferred to each other, enhancing the separation efficiency of photogenerated electron-hole pairs. With the synergistic coupling effect of type Ⅰ band structure heterojunctions and PMS, ZIF-8/BiOI accelerated the generation of free radicals in the degradation system.

, authors=Rui WANG, Xianxiong CHENG^*, Junfeng LIAN, Jiahua TANG, Xin LIU, Rong YAO, authorsList=Rui WANG, Xianxiong CHENG, Junfeng LIAN, Jiahua TANG, Xin LIU, Rong YAO, authorCompany=null, correspAuthors=Xianxiong CHENG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1297161225847206604, articleId=1297161222466597562, tenantId=1146029695717560320, journalId=1296125381406982186, language=CN, title=ZIF-8/BiOI异质结的制备及其活化PMS可见光催化降解金橙Ⅱ性能, columnId=1297161221933913088, journalTitle=精细化工, columnName=功能材料, runingTitle=null, highlight=null, articleAbstract=

以Bi(NO₃)₃•5H₂O、KI和自制的金属有机骨架材料ZIF-8为原料，通过乙二醇溶剂热法制备了3D球状可见光催化剂ZIF-8/BiOI复合材料。采用XRD、FTIR、SEM、EDS、BET、UV-Vis对其进行了表征。探究了光照条件下，ZIF-8/BiOI复合材料活化过硫酸氢钾（PMS）氧化去除4-(2-羟基-1-萘偶氮)苯磺酸钠盐（金橙Ⅱ）的性能，考察了ZIF-8添加量（以BiOI的质量计，下同）及反应条件对金橙Ⅱ降解率的影响，并推测了ZIF-8/BiOI复合材料活化PMS氧化去除金橙Ⅱ的机理。结果表明，ZIF-8/BiOI复合材料具有良好的可见光响应性能，以ZIF-8添加量（以BiOI质量计，下同）10%制备的10%ZIF-8/BiOI为催化剂，在其投加量500 mg/L、350 W氙灯模拟光照、PMS浓度 0.5 mmol/L、金橙Ⅱ质量浓度100 mg/L，调节溶液初始pH=7.0、60 min的条件下，金橙Ⅱ降解率高达95.4%，反应过程符合一级动力学模型，、对反应体系影响较大，、Cl⁻、几乎不影响反应过程。10%ZIF-8/BiOI具有良好的重复利用性，经4次循环后，60 min时的金橙Ⅱ降解率仍可达83.2%。羟基自由基、单线态氧和空穴是降解过程中的主要活性物质，而硫酸根自由基具有辅助作用。降解过程中，BiOI和ZIF-8的空穴与电子相互转移，提升了光生电子-空穴对的分离效率，ZIF-8/BiOI凭借Ⅰ型能带结构异质结与PMS的协同耦合效应，加速了降解体系中自由基的生成。

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王芮（2001—），女，硕士生，E-mail: 1083750770@qq.com。

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王芮（2001—），女，硕士生，E-mail: 1083750770@qq.com。

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