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Article(id=1325114990159594057, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1325114904314786565, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1290096000000, receivedDateStr=2010-11-19, revisedDate=1297353600000, revisedDateStr=2011-02-11, acceptedDate=null, acceptedDateStr=null, onlineDate=1793861633098, onlineDateStr=2026-11-05, pubDate=1344960000000, pubDateStr=2012-08-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793861633098, onlineIssueDateStr=2026-11-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793861633098, creator=13701087609, updateTime=1793861633098, updator=13701087609, issue=Issue{id=1325114904314786565, tenantId=1146029695717560320, journalId=1255847867265597444, year='2012', volume='26', issue='4', pageStart='361', pageEnd='480', issueExtLink='null', onlineDate='null', pubDate='1344960000000', pubDateStr='2012-08-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793861612632, creator='13701087609', updateTime=1793861612632, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=421, endPage=425, ext={EN=ArticleExt(id=1325114990419640906, articleId=1325114990159594057, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=Experimental Study on Phase Transformation of TiO2 Induced by High Energy Milling, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The mixture of TiO2 and dicyandiamide powder is processed by high energy milling at different milling speed and milling time. The structure and phase composition of the recovered samples are determined by X-ray diffraction (XRD). The results show that anatase transforms to rutile and srilankite appears at milling speed of 700 r/min. With milling time increasing, srilankite high-pressure phase content increases and gradually approaches a constant value. When the milling speed is raised to 1 000 r/min, the transformation of anatase to srilankite is dominant, and the mass fraction of srilankite high-pressure phase is increased greatly to 47.8%.

, authors=Xiang GAO1, 2, Peng-Wan CHEN1, Jian-Jun LIU3, Guang-Yuan XIONG1, authorsList=Xiang GAO, Peng-Wan CHEN, Jian-Jun LIU, Guang-Yuan XIONG, authorCompany=null, correspAuthors=Peng-Wan CHEN, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1325114990654521931, articleId=1325114990159594057, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=高能球磨条件下TiO2相变的实验研究, columnId=0, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用高能球磨法处理二氧化钛（TiO2）与双氰胺粉末混合物，对不同球磨时间和球磨转速条件下TiO2的相变进行了研究。利用X射线衍射仪对回收产物的相组成进行表征。结果表明，在700 r/min的高速球磨条件下，TiO2发生了由锐钛矿相向金红石相和Srilankite高压相的转变，随着球磨时间的增加，Srilankite高压相和金红石相的含量逐步增加并逐渐趋于平衡；进一步提高球磨转速至1 000 r/min，锐钛矿相向Srilankite高压相的转变占主导，更易于形成Srilankite高压相，Srilankite高压相的质量分数可增加至47.8%。

, authors=高翔1, 2, 陈鹏万1, 刘建军3, 熊光源1, authorsList=高翔, 陈鹏万, 刘建军, 熊光源, authorCompany=null, correspAuthors=陈鹏万, authorNote=

高翔（1983—），男，博士研究生，主要从事爆炸合成材料及改性研究. E-mail：

, correspAuthorsNote=
陈鹏万（1971—），男，博士，教授，主要从事爆炸力学与冲击力学研究. E-mail：
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高翔（1983—），男，博士研究生，主要从事爆炸合成材料及改性研究. E-mail：

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高翔 1, 2 , 陈鹏万 1 , 刘建军 3 , 熊光源 1
高压物理学报 | 2012,26(4): 421-425
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高翔1, 2 , 陈鹏万1 , 刘建军3, 熊光源1
作者信息
  • 1.北京理工大学爆炸科学与技术国家重点实验室，北京　100081
  • 2.中国运载火箭技术研究院北京航天长征科技信息研究所，北京　100076
  • 3.北京化工大学化工资源有效利用国家重点实验室，北京　100029
通讯作者:
陈鹏万（1971—），男，博士，教授，主要从事爆炸力学与冲击力学研究. E-mail：
作者简介:

高翔（1983—），男，博士研究生，主要从事爆炸合成材料及改性研究. E-mail：

Experimental Study on Phase Transformation of TiO2 Induced by High Energy Milling
Xiang GAO1, 2 , Peng-Wan CHEN1 , Jian-Jun LIU3, Guang-Yuan XIONG1
Affiliations
  • 1.State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081, China
  • 2.Beijing Aerospace Long March Scientific and Technical Information Institute, China Academy of Launch Vehicle Technology, Beijing 100076, China
  • 3.State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing 100029, China
出版时间: 2012-08-15
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采用高能球磨法处理二氧化钛（TiO2）与双氰胺粉末混合物，对不同球磨时间和球磨转速条件下TiO2的相变进行了研究。利用X射线衍射仪对回收产物的相组成进行表征。结果表明，在700 r/min的高速球磨条件下，TiO2发生了由锐钛矿相向金红石相和Srilankite高压相的转变，随着球磨时间的增加，Srilankite高压相和金红石相的含量逐步增加并逐渐趋于平衡；进一步提高球磨转速至1 000 r/min，锐钛矿相向Srilankite高压相的转变占主导，更易于形成Srilankite高压相，Srilankite高压相的质量分数可增加至47.8%。

二氧化钛  /  高能球磨  /  相变  /  锐钛矿  /  金红石  /  Srilankite高压相

The mixture of TiO2 and dicyandiamide powder is processed by high energy milling at different milling speed and milling time. The structure and phase composition of the recovered samples are determined by X-ray diffraction (XRD). The results show that anatase transforms to rutile and srilankite appears at milling speed of 700 r/min. With milling time increasing, srilankite high-pressure phase content increases and gradually approaches a constant value. When the milling speed is raised to 1 000 r/min, the transformation of anatase to srilankite is dominant, and the mass fraction of srilankite high-pressure phase is increased greatly to 47.8%.

titania  /  high energy milling  /  phase transformation  /  anatase  /  rutile  /  srilankite high-pressure phase
高翔, 陈鹏万, 刘建军, 熊光源. 高能球磨条件下TiO2相变的实验研究. 高压物理学报, 2012 , 26 (4) : 421 -425 .
Xiang GAO, Peng-Wan CHEN, Jian-Jun LIU, Guang-Yuan XIONG. Experimental Study on Phase Transformation of TiO2 Induced by High Energy Milling[J]. Chinese Journal of High Pressure Physics, 2012 , 26 (4) : 421 -425 .
基金
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  • 国家自然科学基金(10972039)
  • 高等学校博士学科点专项科研基金(200800070033)
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2012年第26卷第4期
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  • 接收时间：2010-11-19
  • 首发时间：2026-11-05
  • 出版时间：2012-08-15
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出版历史
  • 收稿日期：2010-11-19
  • 修回日期：2011-02-11
基金
国家自然科学基金(10972039)
高等学校博士学科点专项科研基金(200800070033)
作者信息
    1.北京理工大学爆炸科学与技术国家重点实验室，北京　100081
    2.中国运载火箭技术研究院北京航天长征科技信息研究所，北京　100076
    3.北京化工大学化工资源有效利用国家重点实验室，北京　100029

通讯作者:

陈鹏万（1971—），男，博士，教授，主要从事爆炸力学与冲击力学研究. E-mail：
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genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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