Article(id=1324026907720819435, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1324026895225991447, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1264262400000, receivedDateStr=2010-01-24, revisedDate=1270051200000, revisedDateStr=2010-04-01, acceptedDate=null, acceptedDateStr=null, onlineDate=1793602214030, onlineDateStr=2026-11-02, pubDate=1313337600000, pubDateStr=2011-08-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793602214030, onlineIssueDateStr=2026-11-02, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793602214030, creator=13701087609, updateTime=1793602214030, updator=13701087609, issue=Issue{id=1324026895225991447, tenantId=1146029695717560320, journalId=1255847867265597444, year='2011', volume='25', issue='4', pageStart='289', pageEnd='384', issueExtLink='null', onlineDate='null', pubDate='1313337600000', pubDateStr='2011-08-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793602211051, creator='13701087609', updateTime=1793602835854, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1324029515936170233, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1324026895225991447, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1324029515936170234, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1324026895225991447, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=303, endPage=309, ext={EN=ArticleExt(id=1324026907896980204, articleId=1324026907720819435, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=Use and Pressure Calibration of 1 000 Tons Walker Module High Pressure and High Temperature Apparatus, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The two-stage 1 000 tons Walker module large-volume high temperature and high pressure apparatus can generate different pressures with different truncated edge lengths of anvils (12, 8, 6, and 4 mm). If tungsten carbide is chosen as an anvil, the maximum pressure obtained is above 20 GPa. The sample assemblies of Walker module apparatus are determined. The pressure calibration is performed by the fixed points of phase transitions method for different truncated edge lengths. The phase transition pressures of standard materials of pressure calibration (Bi, Tl, ZnTe, Pb, ZnS, GaAs) are achieved by measuring the resistance change with oil load under high pressure. The calibration curve of the sample pressure versus load is obtained, which provides exact information for future high pressure experiments using this apparatus.

, authors=Bin YANG, Feng-Guo LU, Xu-Dong ZHAO, Xiao-Yang LIU, authorsList=Bin YANG, Feng-Guo LU, Xu-Dong ZHAO, Xiao-Yang LIU, authorCompany=null, correspAuthors=Xiao-Yang LIU, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1324026908094112493, articleId=1324026907720819435, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=1 000 t Walker型高温高压装置的使用与压力标定, columnId=0, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

介绍了一种6-8型二级加压装置——1 000 t Walker型大腔体高温高压装置中样品的组装方式、组装件材料和压力标定方法。采用碳化钨作为压砧时,获得的最高压力超过20 GPa。压力标定方法采用相变点法,即利用Bi、Tl、ZnTe、Pb、SnS、GaAs等标准压力标定物质,通过测量其在室温高压下的电阻变化,确定相变点,进而获得高压腔体内的压力与外加载荷的关系。对具有不同二级压砧截角边长(4、6、8、12 mm)组装的内部实际压力进行标定,得到了外加载荷与内部压力的关系曲线,为今后在该装置上的实验样品组装及样品实际压力确定提供了准确的数据。

, authors=杨斌, 陆凤国, 赵旭东, 刘晓旸, authorsList=杨斌, 陆凤国, 赵旭东, 刘晓旸, authorCompany=null, correspAuthors=刘晓旸, authorNote=

杨斌(1981-),男,博士研究生,主要从事大腔体超高压技术研究. E-mail:

, correspAuthorsNote=
刘晓旸(1964-),男,教授,博士生导师,主要从事高温高压化学研究. E-mail:
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杨斌(1981-),男,博士研究生,主要从事大腔体超高压技术研究. E-mail:

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1 000 t Walker型高温高压装置的使用与压力标定
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杨斌 , 陆凤国 , 赵旭东 , 刘晓旸
高压物理学报 | 2011,25(4): 303-309
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高压物理学报 | 2011 , 25 (4) : 303 -309
1 000 t Walker型高温高压装置的使用与压力标定
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杨斌(1981-),男,博士研究生,主要从事大腔体超高压技术研究. E-mail:

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杨斌 , 陆凤国, 赵旭东, 刘晓旸
作者信息
  • 吉林大学无机合成与制备化学国家重点实验室,吉林 长春 130012
通讯作者:
刘晓旸(1964-),男,教授,博士生导师,主要从事高温高压化学研究. E-mail:
作者简介:

杨斌(1981-),男,博士研究生,主要从事大腔体超高压技术研究. E-mail:

Use and Pressure Calibration of 1 000 Tons Walker Module High Pressure and High Temperature Apparatus
Bin YANG , Feng-Guo LU, Xu-Dong ZHAO, Xiao-Yang LIU
Affiliations
  • State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130012, China
出版时间: 2011-08-15
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介绍了一种6-8型二级加压装置——1 000 t Walker型大腔体高温高压装置中样品的组装方式、组装件材料和压力标定方法。采用碳化钨作为压砧时,获得的最高压力超过20 GPa。压力标定方法采用相变点法,即利用Bi、Tl、ZnTe、Pb、SnS、GaAs等标准压力标定物质,通过测量其在室温高压下的电阻变化,确定相变点,进而获得高压腔体内的压力与外加载荷的关系。对具有不同二级压砧截角边长(4、6、8、12 mm)组装的内部实际压力进行标定,得到了外加载荷与内部压力的关系曲线,为今后在该装置上的实验样品组装及样品实际压力确定提供了准确的数据。

大腔体  /  高温高压  /  样品组装  /  压力标定

The two-stage 1 000 tons Walker module large-volume high temperature and high pressure apparatus can generate different pressures with different truncated edge lengths of anvils (12, 8, 6, and 4 mm). If tungsten carbide is chosen as an anvil, the maximum pressure obtained is above 20 GPa. The sample assemblies of Walker module apparatus are determined. The pressure calibration is performed by the fixed points of phase transitions method for different truncated edge lengths. The phase transition pressures of standard materials of pressure calibration (Bi, Tl, ZnTe, Pb, ZnS, GaAs) are achieved by measuring the resistance change with oil load under high pressure. The calibration curve of the sample pressure versus load is obtained, which provides exact information for future high pressure experiments using this apparatus.

large-volume  /  high pressure and high temperature  /  sample assembly  /  pressure calibration
杨斌, 陆凤国, 赵旭东, 刘晓旸. 1 000 t Walker型高温高压装置的使用与压力标定. 高压物理学报, 2011 , 25 (4) : 303 -309 .
Bin YANG, Feng-Guo LU, Xu-Dong ZHAO, Xiao-Yang LIU. Use and Pressure Calibration of 1 000 Tons Walker Module High Pressure and High Temperature Apparatus[J]. Chinese Journal of High Pressure Physics, 2011 , 25 (4) : 303 -309 .
  • 国家自然科学基金(20471022; 40673051; 20121103)
  • 教育部新世纪优秀人才支持计划
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2011年第25卷第4期
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  • 接收时间:2010-01-24
  • 首发时间:2026-11-02
  • 出版时间:2011-08-15
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  • 收稿日期:2010-01-24
  • 修回日期:2010-04-01
基金
国家自然科学基金(20471022; 40673051; 20121103)
教育部新世纪优秀人才支持计划
作者信息
    吉林大学无机合成与制备化学国家重点实验室,吉林 长春 130012

通讯作者:

刘晓旸(1964-),男,教授,博士生导师,主要从事高温高压化学研究. E-mail:
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