Article(id=1324026443507827023, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1324026415431164669, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1266854400000, receivedDateStr=2010-02-23, revisedDate=1288108800000, revisedDateStr=2010-10-27, acceptedDate=null, acceptedDateStr=null, onlineDate=1793602103354, onlineDateStr=2026-11-02, pubDate=1308067200000, pubDateStr=2011-06-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793602103354, onlineIssueDateStr=2026-11-02, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793602103354, creator=13701087609, updateTime=1793602103354, updator=13701087609, issue=Issue{id=1324026415431164669, tenantId=1146029695717560320, journalId=1255847867265597444, year='2011', volume='25', issue='3', pageStart='193', pageEnd='288', issueExtLink='null', onlineDate='null', pubDate='1308067200000', pubDateStr='2011-06-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793602096660, creator='13701087609', updateTime=1793602819353, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1324029446684028999, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1324026415431164669, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1324029446684029000, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1324026415431164669, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=242, endPage=246, ext={EN=ArticleExt(id=1324026443977589072, articleId=1324026443507827023, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=The Study on Black cBN Synthesis with Different Systems, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

As well known, cubic boron nitride display more integrated morphology and larger crystal sizes with the color burn. In this paper, black cBN crystals were synthesized in the systems of Mg+hBN, LiH+hBN, Li3N+hBN+B and B+Li3N, respectively. Optical microscope (OM), X-ray diffraction and Raman spectroscopy were used to make a comparison with different black cBN crystals on the aspect of the synthetic condition, crystal morphology, grain size and residual stress. The results showed that the synthesized cBN with the different system exhibited obvious difference. In order to optimize the cBN synthesis, the appropriate system should be chosen according to diverse demands in practical applications.

, authors=Yong-Hui DU1, Tie-Chen ZHANG2, Wei-Sen ZHANG1, authorsList=Yong-Hui DU, Tie-Chen ZHANG, Wei-Sen ZHANG, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1324026445206520145, articleId=1324026443507827023, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=用不同合成体系制备黑色立方氮化硼的研究, columnId=0, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

立方氮化硼(cBN)晶体随颜色的加深,晶体的晶形越完整,晶体尺寸也越大。采用Mg+hBN、LiH+hBN、Li3N+hBN+B和B+Li3N 4种体系分别合成出了黑色的立方氮化硼晶体。通过光学显微镜、X射线衍射、拉曼光谱等测试分析手段,从合成条件、晶体形貌、颗粒度及残余应力等方面对不同体系合成出的黑色cBN晶体作了比较。结果表明,不同体系的合成效果有很大差别。在实际应用中应该根据需要采用不同的体系,以达到最优化合成目的。

, authors=杜勇慧1, 张铁臣2, 张伟森1, authorsList=杜勇慧, 张铁臣, 张伟森, authorCompany=null, correspAuthors=null, authorNote=

杜勇慧(1979—),女,博士研究生,主要从事高温高压下材料的合成研究. E-mail:

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杜勇慧(1979—),女,博士研究生,主要从事高温高压下材料的合成研究. E-mail:

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用不同合成体系制备黑色立方氮化硼的研究
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杜勇慧 1 , 张铁臣 2 , 张伟森 1
高压物理学报 | 2011,25(3): 242-246
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高压物理学报 | 2011 , 25 (3) : 242 -246
用不同合成体系制备黑色立方氮化硼的研究
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杜勇慧1 , 张铁臣2, 张伟森1
作者信息
  • 1.北华大学物理学院,吉林 吉林 132013
  • 2.吉林大学超硬材料国家重点实验室,吉林 长春 130012
作者简介:

杜勇慧(1979—),女,博士研究生,主要从事高温高压下材料的合成研究. E-mail:

The Study on Black cBN Synthesis with Different Systems
Yong-Hui DU1 , Tie-Chen ZHANG2, Wei-Sen ZHANG1
Affiliations
  • 1.School of Physics, Beihua University, Jilin 132013, China
  • 2.National Laborary of Superhard Materials, Jilin University, Changchun 130012, China
出版时间: 2011-06-15
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立方氮化硼(cBN)晶体随颜色的加深,晶体的晶形越完整,晶体尺寸也越大。采用Mg+hBN、LiH+hBN、Li3N+hBN+B和B+Li3N 4种体系分别合成出了黑色的立方氮化硼晶体。通过光学显微镜、X射线衍射、拉曼光谱等测试分析手段,从合成条件、晶体形貌、颗粒度及残余应力等方面对不同体系合成出的黑色cBN晶体作了比较。结果表明,不同体系的合成效果有很大差别。在实际应用中应该根据需要采用不同的体系,以达到最优化合成目的。

立方氮化硼  /  触媒  /  添加剂  /  残余应力

As well known, cubic boron nitride display more integrated morphology and larger crystal sizes with the color burn. In this paper, black cBN crystals were synthesized in the systems of Mg+hBN, LiH+hBN, Li3N+hBN+B and B+Li3N, respectively. Optical microscope (OM), X-ray diffraction and Raman spectroscopy were used to make a comparison with different black cBN crystals on the aspect of the synthetic condition, crystal morphology, grain size and residual stress. The results showed that the synthesized cBN with the different system exhibited obvious difference. In order to optimize the cBN synthesis, the appropriate system should be chosen according to diverse demands in practical applications.

cBN  /  catalyst  /  additive  /  residual stress
杜勇慧, 张铁臣, 张伟森. 用不同合成体系制备黑色立方氮化硼的研究. 高压物理学报, 2011 , 25 (3) : 242 -246 .
Yong-Hui DU, Tie-Chen ZHANG, Wei-Sen ZHANG. The Study on Black cBN Synthesis with Different Systems[J]. Chinese Journal of High Pressure Physics, 2011 , 25 (3) : 242 -246 .

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[1]
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2011年第25卷第3期
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  • 接收时间:2010-02-23
  • 首发时间:2026-11-02
  • 出版时间:2011-06-15
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  • 收稿日期:2010-02-23
  • 修回日期:2010-10-27
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    1.北华大学物理学院,吉林 吉林 132013
    2.吉林大学超硬材料国家重点实验室,吉林 长春 130012
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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