Article(id=1323704258046075372, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1323704219571724466, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1169222400000, receivedDateStr=2007-01-20, revisedDate=1177516800000, revisedDateStr=2007-04-26, acceptedDate=null, acceptedDateStr=null, onlineDate=1793525288353, onlineDateStr=2026-11-01, pubDate=1204646400000, pubDateStr=2008-03-05, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793525288353, onlineIssueDateStr=2026-11-01, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793525288353, creator=13701087609, updateTime=1793525288353, updator=13701087609, issue=Issue{id=1323704219571724466, tenantId=1146029695717560320, journalId=1255847867265597444, year='2008', volume='22', issue='1', pageStart='1', pageEnd='112', issueExtLink='null', onlineDate='null', pubDate='1204646400000', pubDateStr='2008-03-05', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793525279180, creator='13701087609', updateTime=1793525279180, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=35, endPage=38, ext={EN=ArticleExt(id=1323704258201264621, articleId=1323704258046075372, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=Synthesis and Characterization of Two-Dimensional Rh-C₆₀ Polymer, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A rhombohedral two-dimensional (2D-Rh) C₆₀ polymer has been successfully synthesized by cubic press methods under the conditions of 6 GPa and 700 ℃. X-ray diffraction (XRD) and nuclear magenatic resonance (NMR) were performed to characterize the samples. XRD spectrum indicates that the C₆₀ polymer is rhombohedral, and sp³ bonds have formed between adjacent fullerene molecules via [2+2] cycloaddition reaction. ¹³C MAS NMR spectrum shows a broadened peak at δ145, which has two sidebands, and one small peak at about δ72. The broadening of the peak at δ145 could be related to the presence of inequivalent sp² sites and structure disorder. The sidebands of the peak at δ145 show the large structure anisotropy of the corresponding carbons. The peak at δ72 indicates the presence sp³ bond of adjacent C₆₀ molecules.

, authors=Su-Qin WANG^{1, 2}, Min GU², authorsList=Su-Qin WANG, Min GU, authorCompany=null, correspAuthors=Min GU, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1323704258402591214, articleId=1323704258046075372, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=二维Rh-C₆₀聚合相的制备和表征, columnId=0, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

利用高压合成装置在6 GPa压力、700 ℃温度条件下合成了二维C₆₀聚合相，并用X射线衍射（XRD）和高分辨核磁共振（NMR）等方法对样品进行了表征。XRD分析结果表明，C₆₀分子在高温高压下发生了聚合反应，晶体结构由面心立方结构变为菱形结构，通过[2+2]加环反应在邻近分子间形成sp³杂化共价键。¹³C核磁共振魔角谱（¹³C MAS NMR）在δ145和δ72处出现了两个共振峰，其中在δ145附近的峰展宽并有两个边带。δ145附近的峰的展宽与分裂主要是由于C₆₀分子上出现了不等价的sp²杂化碳和高温高压条件下产生的结构无序，边带的形成说明了其结构的各向异性；位置为δ72附近的峰证明了聚合物内C₆₀分子之间出现了sp³杂化键。

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^2.National Laboratory of Solid State Microstructures, Nanjing University, Nanjing 210093, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1323704258964627962, tenantId=1146029695717560320, journalId=1255847867265597444, articleId=1323704258046075372, authorId=1323704258788467190, language=CN, stringName=王素芹, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=^{1, 2}, address=^1.淮海工学院数理科学系，江苏 连云港　222005
^2.南京大学固体微结构国家重点实验室，南京大学物理系，江苏 南京　210093, bio={"content":"

王素芹（1973—），女，硕士研究生，讲师，主要从事凝聚态物理研究. E-mail：hhitwsq@126.com

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王素芹（1973—），女，硕士研究生，讲师，主要从事凝聚态物理研究. E-mail：hhitwsq@126.com

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