Article(id=1323704240597770590, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1323704219571724466, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1170604800000, receivedDateStr=2007-02-05, revisedDate=1180022400000, revisedDateStr=2007-05-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1793525284194, onlineDateStr=2026-11-01, pubDate=1204646400000, pubDateStr=2008-03-05, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793525284194, onlineIssueDateStr=2026-11-01, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793525284194, creator=13701087609, updateTime=1793525284194, updator=13701087609, issue=Issue{id=1323704219571724466, tenantId=1146029695717560320, journalId=1255847867265597444, year='2008', volume='22', issue='1', pageStart='1', pageEnd='112', issueExtLink='null', onlineDate='null', pubDate='1204646400000', pubDateStr='2008-03-05', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793525279180, creator='13701087609', updateTime=1793525279180, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=99, endPage=102, ext={EN=ArticleExt(id=1323704240803291487, articleId=1323704240597770590, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus, columnId=1322942130796245184, journalTitle=Chinese Journal of High Pressure Physics, columnName=Research Note, runingTitle=null, highlight=null, articleAbstract=

By a self-made system based on a cubic anvil high-pressure apparatus and an Agilent 4294A accurate impedance analyzer, real time high frequency dielectricity measurement under hydrostatic pressure is realized by the standard four-wire method widely used in ambient pressure dielectric research. The sealing of liquid cell in solid pressure-transmission medium and multi signal lines out through gaskets including four micro-coaxial cables is achieved by the pre-formation of pyrophyllite cube together with gaskets. The testing fixture, 10 mm×10 mm sample, pressure-temperature sensors and as many as 16 signal wires including 4 micro-coaxial cables with an outer diameters of 1.6 mm respectively can be contained simultaneously in a liquid testing cell with a volume of (Ø13×15) mm3. Four-wire impedance spectroscopy can be obtained by this system in a measurement range of room temperature to 300 ℃, ambient pressure to about 3 GPa hydrostatic pressure and testing frequency from 40 Hz to 5 MHz with an experiment error below 3%. The pressure induced ferroelectric-paraelectric phase transition of a BaTiO3 single crystal is observed using this setting up.

, authors=Zhong LU1, Xiao-Hong ZHAN1, Da-Hu CAO1, Liang-Ying ZHANG2, Xi YAO2, authorsList=Zhong LU, Xiao-Hong ZHAN, Da-Hu CAO, Liang-Ying ZHANG, Xi YAO, authorCompany=null, correspAuthors=Da-Hu CAO, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1323704241050755424, articleId=1323704240597770590, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=一套基于六面顶高压装置的静水压高频介电测试系统, columnId=1322942131614134466, journalTitle=高压物理学报, columnName=研究简报, runingTitle=null, highlight=null, articleAbstract=

以一套6×14 400 kN六面顶高压装置和一台Agilent 4294A精密阻抗分析仪为主体,建立了一套静水压高频介电实时测试系统。通过固体传压介质预成型方法,解决了液体测试腔在固体传压介质中的密封以及包括4根微同轴电缆在内的多根测量导线引出密封边问题,将常压下通用的四同轴阻抗谱测试技术引入了高压研究。液体测试腔容积可达(Ø13×15)mm3,可同时容纳10 mm×10 mm样品、高频测试夹具、温度与压力传感器、加热装置,以及包括4根外径为1.6 mm、特性阻抗为50 Ω微同轴电缆在内的16根引线,进行室温至300 ℃、常压至3 GPa静水压力、测试频率40 Hz~5 MHz范围材料的四线阻抗谱测量,实验误差小于3%。利用这套装置观察了室温下,BaTiO3单晶在约2.6 GPa静水压力下的压致铁电-顺电相变。

, authors=陆中1, 战晓红1, 曹大呼1, 张良莹2, 姚熹2, authorsList=陆中, 战晓红, 曹大呼, 张良莹, 姚熹, authorCompany=null, correspAuthors=曹大呼, authorNote=

陆中(1969—),男,硕士研究生. E-mail:

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曹大呼(1967—),男,教授,硕士生导师,主要研究方向为高温高压下材料合成及介电性能测试. E-mail:
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陆中(1969—),男,硕士研究生. E-mail:

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一套基于六面顶高压装置的静水压高频介电测试系统
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陆中 1 , 战晓红 1 , 曹大呼 1 , 张良莹 2 , 姚熹 2
高压物理学报 | 研究简报 2008,22(1): 99-102
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高压物理学报 |研究简报 2008 , 22 (1) : 99 -102
一套基于六面顶高压装置的静水压高频介电测试系统
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陆中1 , 战晓红1, 曹大呼1 , 张良莹2, 姚熹2
作者信息
  • 1.江苏工业学院材料科学与工程系,江苏 常州 213164
  • 2.同济大学功能材料研究所,上海 200000
通讯作者:
曹大呼(1967—),男,教授,硕士生导师,主要研究方向为高温高压下材料合成及介电性能测试. E-mail:
作者简介:

陆中(1969—),男,硕士研究生. E-mail:

A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus
Zhong LU1 , Xiao-Hong ZHAN1, Da-Hu CAO1 , Liang-Ying ZHANG2, Xi YAO2
Affiliations
  • 1.Material Science and Engineering Department, Jiangsu Polytechnic University, Changzhou 213164, China
  • 2.Functional Materials Research Laboratory, Tongji University, Shanghai 200000, China
出版时间: 2008-03-05
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以一套6×14 400 kN六面顶高压装置和一台Agilent 4294A精密阻抗分析仪为主体,建立了一套静水压高频介电实时测试系统。通过固体传压介质预成型方法,解决了液体测试腔在固体传压介质中的密封以及包括4根微同轴电缆在内的多根测量导线引出密封边问题,将常压下通用的四同轴阻抗谱测试技术引入了高压研究。液体测试腔容积可达(Ø13×15)mm3,可同时容纳10 mm×10 mm样品、高频测试夹具、温度与压力传感器、加热装置,以及包括4根外径为1.6 mm、特性阻抗为50 Ω微同轴电缆在内的16根引线,进行室温至300 ℃、常压至3 GPa静水压力、测试频率40 Hz~5 MHz范围材料的四线阻抗谱测量,实验误差小于3%。利用这套装置观察了室温下,BaTiO3单晶在约2.6 GPa静水压力下的压致铁电-顺电相变。

BaTiO3  /  静水压  /  四线阻抗谱

By a self-made system based on a cubic anvil high-pressure apparatus and an Agilent 4294A accurate impedance analyzer, real time high frequency dielectricity measurement under hydrostatic pressure is realized by the standard four-wire method widely used in ambient pressure dielectric research. The sealing of liquid cell in solid pressure-transmission medium and multi signal lines out through gaskets including four micro-coaxial cables is achieved by the pre-formation of pyrophyllite cube together with gaskets. The testing fixture, 10 mm×10 mm sample, pressure-temperature sensors and as many as 16 signal wires including 4 micro-coaxial cables with an outer diameters of 1.6 mm respectively can be contained simultaneously in a liquid testing cell with a volume of (Ø13×15) mm3. Four-wire impedance spectroscopy can be obtained by this system in a measurement range of room temperature to 300 ℃, ambient pressure to about 3 GPa hydrostatic pressure and testing frequency from 40 Hz to 5 MHz with an experiment error below 3%. The pressure induced ferroelectric-paraelectric phase transition of a BaTiO3 single crystal is observed using this setting up.

BaTiO3  /  hydrostatic pressure  /  four-wire method
陆中, 战晓红, 曹大呼, 张良莹, 姚熹. 一套基于六面顶高压装置的静水压高频介电测试系统. 高压物理学报, 2008 , 22 (1) : 99 -102 .
Zhong LU, Xiao-Hong ZHAN, Da-Hu CAO, Liang-Ying ZHANG, Xi YAO. A High Frequency Hydrostatic Pressure Dielectricity Measuring System Based on Cubic Anvil Apparatus[J]. Chinese Journal of High Pressure Physics, 2008 , 22 (1) : 99 -102 .
  • 江苏省青蓝工程资助项目
  • 常州市工业攻关项目(CE2006095)
  • 江苏工业学院重大基金
参考文献 引证文献
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Samara G A, Venturini E L, Hugo S V. Dielectric Properties and Phase Transitions of [Pb(Zn1/3Nb2/3)O3]0.905·(PbTiO3)0.095: Influence of Pressure[J]. Phys Rev B, 2001, 63: 184104-184115.
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Yasuda N, Ohwa H, Oohashi J, et al. Pressure-Induced Dielectric Change from Relaxor to Antiferroelectric Behavior in Disordered Pb(In1/2Nb1/2)O3[J]. J Phys Soc Jpn, 1997, 66: 1920-1923.
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Yasuda N, Ohwa H, Oohashi J, et al. The Temperature and Pressure Dependence of the Dielectric Properties of Disordered and Ordered Pb(In1/2Nb1/2)O3 Single Crystals[J]. J Phys Soc Jpn, 1998, 67: 3952-3957.
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Nomura K, Shingai T, Yasuda N, et al. Pressure-Induced Structural Phase Transition from Relaxor Phase to Antiferroelectric Phase in Disordered Pb(In1/2Nb1/2)O3[J]. J Phys Soc Jpn, 1999, 68: 866-870.
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Samara G A. Pressure and Temperature Dependences of the Dielectric Properties of the Perovskites BaTiO3 and SrTiO3[J]. Phys Rev, 1966, 151: 378-386.
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Samara G A. Pressure as a Probe of the Glassy Properties of Compositionally Disordered Soft Mode Ferroelectrics: (Pb0.82La0.12) (Zr0.40Ti0.60)O3 (PLZT 12/40/60)[J]. J Appl Phys, 1998, 84: 2538-2545.
2008年第22卷第1期
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  • 接收时间:2007-02-05
  • 首发时间:2026-11-01
  • 出版时间:2008-03-05
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  • 收稿日期:2007-02-05
  • 修回日期:2007-05-25
基金
江苏省青蓝工程资助项目
常州市工业攻关项目(CE2006095)
江苏工业学院重大基金
作者信息
    1.江苏工业学院材料科学与工程系,江苏 常州 213164
    2.同济大学功能材料研究所,上海 200000

通讯作者:

曹大呼(1967—),男,教授,硕士生导师,主要研究方向为高温高压下材料合成及介电性能测试. E-mail:
参考文献
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2种不同金属材料的力学参数
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species
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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