Article(id=1323704226530074841, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1323704219571724466, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1171468800000, receivedDateStr=2007-02-15, revisedDate=1180281600000, revisedDateStr=2007-05-28, acceptedDate=null, acceptedDateStr=null, onlineDate=1793525280839, onlineDateStr=2026-11-01, pubDate=1204646400000, pubDateStr=2008-03-05, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793525280839, onlineIssueDateStr=2026-11-01, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793525280839, creator=13701087609, updateTime=1793525280839, updator=13701087609, issue=Issue{id=1323704219571724466, tenantId=1146029695717560320, journalId=1255847867265597444, year='2008', volume='22', issue='1', pageStart='1', pageEnd='112', issueExtLink='null', onlineDate='null', pubDate='1204646400000', pubDateStr='2008-03-05', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793525279180, creator='13701087609', updateTime=1793525279180, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=85, endPage=88, ext={EN=ArticleExt(id=1323704226697847003, articleId=1323704226530074841, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=Possible Existence of Ultra Fast Polarity Diffusion Process of ZnO under High Pressure, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The effects of heating temperature and duration time on the process of ZnO crystallization under the pressure of 5 GPa are studied systemically by the methods of X-ray diffraction (XRD) and scanning electron microscopy (SEM). The experimental results show that the diffusion rate of ZnO increases greatly under high-pressure and the sample density higher than 99% of the theoretical value can be achieved after heated at 400 ℃ and 5 GPa for 0.5 h. With the increasing of the heating temperature, micro-cracks develop along crystal boundary in all samples, and eventually ZnO powder mixed with single crystals and poly-crystals forms above 500 ℃. The pale yellow crystallites with an average size of 100 μm and the largest size more than 350 μm was obtained at 850 ℃ after heating of 5 min. The sample morphology analysis shows that the reason for the ultra fast crystallization of ZnO under high-pressure is possibly caused by a very quick diffusion rate of ZnO along certain direction. The crystal boundary along such direction moves very quickly under high-pressure until the neighboring micro-crystals merge into a single crystal in a short time, while the micro-crystals shrink in the other direction and cause micro-cracks along other crystal boundaries.

, authors=Xiao-Hong ZHAN, Da-Hu CAO, Zhong LU, Hui-Hui DING, authorsList=Xiao-Hong ZHAN, Da-Hu CAO, Zhong LU, Hui-Hui DING, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1323704226878202076, articleId=1323704226530074841, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=高压下ZnO超快极性扩散过程研究, columnId=0, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

利用X射线衍射（XRD）、扫描电镜（SEM）等手段，研究了在5 GPa压力下六方ZnO粉末的结晶过程。系统考查了温度与保温时间对ZnO扩散与结晶过程的影响。结果发现，在高压下ZnO固体的扩散速度大大增加，400 ℃保温0.5 h即可获得理论密度达99%以上的单相、致密的六方相ZnO陶瓷，所有样品均沿晶界开裂，并导致500 ℃以上只能获得单晶与多晶混合的粉末样品；850 ℃保温5 min可制备出平均尺寸超过100 μm、最大尺寸超过350 μm的浅黄色单晶。对实验结果的分析表明：ZnO固体在高压下可能存在一种超快极性扩散机制，这一效应使高压下的ZnO晶粒沿择优方向迅速生长，晶界快速迁移，相邻晶粒生长融合，最后形成单晶；而晶粒在生长过程中沿其它方向发生收缩，促使样品沿晶界开裂。

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战晓红（1982—），女，硕士研究生，主要研究方向为高压下材料制备. E-mail：zhanxiaohong0214@163.com

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战晓红（1982—），女，硕士研究生，主要研究方向为高压下材料制备. E-mail：zhanxiaohong0214@163.com

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