Article(id=1323703578354917850, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1323703525947093661, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1120406400000, receivedDateStr=2005-07-04, revisedDate=1130169600000, revisedDateStr=2005-10-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1793525126303, onlineDateStr=2026-11-01, pubDate=1149436800000, pubDateStr=2006-06-05, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793525126303, onlineIssueDateStr=2026-11-01, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793525126302, creator=13701087609, updateTime=1793525126302, updator=13701087609, issue=Issue{id=1323703525947093661, tenantId=1146029695717560320, journalId=1255847867265597444, year='2006', volume='20', issue='2', pageStart='113', pageEnd='224', issueExtLink='null', onlineDate='null', pubDate='1149436800000', pubDateStr='2006-06-05', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793525113807, creator='13701087609', updateTime=1793525113807, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=122, endPage=126, ext={EN=ArticleExt(id=1323703578539467227, articleId=1323703578354917850, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=Explosive Synthesis of Nanometer Titanium Dioxide and Parameter Control, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Some TiO2 nanoparticle samples with size range from 10 nm to 60 nm were prepared by explosive synthesis method. The influence of the preparation parameters on the size and the crystalline phase of the TiO2 crystallite were studied by means of X-ray diffraction (XRD) technique, SEM, TEM and BET. With these characterizing methods, it indicates that the explosive temperature plays a very important role in the crystalline phase transformation. With increasing the proportion of detonator, the size of TiO2 crystallite increased, and the crystalline phase transforms from the low temperature phases of anatase and brookite to the high temperature phase of rutile.

, authors=Xiao-Jie LI1, Tao CHEN1, Zhao-Long XU2, Rui-Yong LI1, Yan-Dong QU1, Zhan-Lei WANG1, authorsList=Xiao-Jie LI, Tao CHEN, Zhao-Long XU, Rui-Yong LI, Yan-Dong QU, Zhan-Lei WANG, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1323703578761765340, articleId=1323703578354917850, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=爆轰法制备纳米TiO2及其参数控制, columnId=0, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用偏钛酸与炸药混合进行爆轰合成,制备出晶粒尺寸在10 nm到60 nm之间的纳米TiO2粉末。结合XRD、TEM、BET等表征手段,研究了纳米TiO2的制备参数与其晶粒尺寸和晶相结构之间的关系。发现当炸药含量增加时,产物晶粒尺寸增大,同时晶相结构随炸药量的增加逐渐由低温的锐钛矿型和板钛矿型向高温的金红石型转变,爆轰温度在这种转变过程中起着极为重要的作用。

, authors=李晓杰1, 陈涛1, 徐兆龙2, 李瑞勇1, 曲艳东1, 王占磊1, authorsList=李晓杰, 陈涛, 徐兆龙, 李瑞勇, 曲艳东, 王占磊, authorCompany=null, correspAuthors=null, authorNote=

李晓杰(1963—),男,博士,教授,博士生导师,主要从事爆炸与冲击动力学方面的研究. E-mail:

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李晓杰(1963—),男,博士,教授,博士生导师,主要从事爆炸与冲击动力学方面的研究. E-mail:

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李晓杰(1963—),男,博士,教授,博士生导师,主要从事爆炸与冲击动力学方面的研究. E-mail:

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爆轰法制备纳米TiO2及其参数控制
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李晓杰 1 , 陈涛 1 , 徐兆龙 2 , 李瑞勇 1 , 曲艳东 1 , 王占磊 1
高压物理学报 | 2006,20(2): 122-126
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高压物理学报 | 2006 , 20 (2) : 122 -126
爆轰法制备纳米TiO2及其参数控制
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李晓杰1 , 陈涛1, 徐兆龙2, 李瑞勇1, 曲艳东1, 王占磊1
作者信息
  • 1.大连理工大学工业装备结构分析国家重点实验室,辽宁 大连 116023
  • 2.中国石油天然气股份有限公司大连石化分公司有机合成厂,辽宁 大连 116031
作者简介:

李晓杰(1963—),男,博士,教授,博士生导师,主要从事爆炸与冲击动力学方面的研究. E-mail:

Explosive Synthesis of Nanometer Titanium Dioxide and Parameter Control
Xiao-Jie LI1 , Tao CHEN1, Zhao-Long XU2, Rui-Yong LI1, Yan-Dong QU1, Zhan-Lei WANG1
Affiliations
  • 1.Department of Engineering Mechanics of Dalian University of Technology, State Key Laboratory of Structural Analysis for Industrial Equipment, Dalian 116023, China
  • 2.Organic Synthetic Plant of Dalian Pertrochemical Company Limited Petrochina, Dalian 116031, China
出版时间: 2006-06-05
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采用偏钛酸与炸药混合进行爆轰合成,制备出晶粒尺寸在10 nm到60 nm之间的纳米TiO2粉末。结合XRD、TEM、BET等表征手段,研究了纳米TiO2的制备参数与其晶粒尺寸和晶相结构之间的关系。发现当炸药含量增加时,产物晶粒尺寸增大,同时晶相结构随炸药量的增加逐渐由低温的锐钛矿型和板钛矿型向高温的金红石型转变,爆轰温度在这种转变过程中起着极为重要的作用。

爆轰  /  纳米TiO2  /  晶粒尺寸  /  晶型转变

Some TiO2 nanoparticle samples with size range from 10 nm to 60 nm were prepared by explosive synthesis method. The influence of the preparation parameters on the size and the crystalline phase of the TiO2 crystallite were studied by means of X-ray diffraction (XRD) technique, SEM, TEM and BET. With these characterizing methods, it indicates that the explosive temperature plays a very important role in the crystalline phase transformation. With increasing the proportion of detonator, the size of TiO2 crystallite increased, and the crystalline phase transforms from the low temperature phases of anatase and brookite to the high temperature phase of rutile.

explosive  /  nanometer TiO2  /  crystalline size  /  crystalline phase transformation
李晓杰, 陈涛, 徐兆龙, 李瑞勇, 曲艳东, 王占磊. 爆轰法制备纳米TiO2及其参数控制. 高压物理学报, 2006 , 20 (2) : 122 -126 .
Xiao-Jie LI, Tao CHEN, Zhao-Long XU, Rui-Yong LI, Yan-Dong QU, Zhan-Lei WANG. Explosive Synthesis of Nanometer Titanium Dioxide and Parameter Control[J]. Chinese Journal of High Pressure Physics, 2006 , 20 (2) : 122 -126 .
  • 国家自然科学基金(10172025)
  • 辽宁省自然科学基金(2004-40)
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2006年第20卷第2期
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  • 接收时间:2005-07-04
  • 首发时间:2026-11-01
  • 出版时间:2006-06-05
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  • 收稿日期:2005-07-04
  • 修回日期:2005-10-25
基金
国家自然科学基金(10172025)
辽宁省自然科学基金(2004-40)
作者信息
    1.大连理工大学工业装备结构分析国家重点实验室,辽宁 大连 116023
    2.中国石油天然气股份有限公司大连石化分公司有机合成厂,辽宁 大连 116031
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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