Article(id=1323703570066973080, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1323703525947093661, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1123603200000, receivedDateStr=2005-08-10, revisedDate=1129737600000, revisedDateStr=2005-10-20, acceptedDate=null, acceptedDateStr=null, onlineDate=1793525124327, onlineDateStr=2026-11-01, pubDate=1149436800000, pubDateStr=2006-06-05, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793525124327, onlineIssueDateStr=2026-11-01, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793525124327, creator=13701087609, updateTime=1793525124327, updator=13701087609, issue=Issue{id=1323703525947093661, tenantId=1146029695717560320, journalId=1255847867265597444, year='2006', volume='20', issue='2', pageStart='113', pageEnd='224', issueExtLink='null', onlineDate='null', pubDate='1149436800000', pubDateStr='2006-06-05', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793525113807, creator='13701087609', updateTime=1793525113807, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=220, endPage=224, ext={EN=ArticleExt(id=1323703570268299673, articleId=1323703570066973080, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=Study on the Synthesis of New Energetic Fullerene Derivative, columnId=1322942130796245184, journalTitle=Chinese Journal of High Pressure Physics, columnName=Research Note, runingTitle=null, highlight=null, articleAbstract=

A new fullerene derivative 1 which contains energy-producing groups was prepared by the Prato reaction, and the reaction conditions affecting the yield of product 1 were investigated. The optimized reaction conditions which afforded 65.8% (based on consumed C₆₀) of product 1 are: molar ratio of C₆₀, 2,4-dinitrobenzaldehyde and N-methylglycine 1∶2∶6, reaction temperature 95 ℃, reaction time 40 h. The structure of product 1 was characterized by UV-vis, FT-IR, ¹H NMR and MS. Further study on the property and application of 1 is under way.

, authors=Bo JIN¹, Ru-Fang PENG¹, Yuan-Jie SHU², Fa-Chun ZHONG², Shi-Jin CHU¹, authorsList=Bo JIN, Ru-Fang PENG, Yuan-Jie SHU, Fa-Chun ZHONG, Shi-Jin CHU, authorCompany=null, correspAuthors=Ru-Fang PENG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1323703570612232602, articleId=1323703570066973080, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=新型含能富勒烯衍生物的合成研究, columnId=1322942131614134466, journalTitle=高压物理学报, columnName=研究简报, runingTitle=null, highlight=null, articleAbstract=

利用N-甲基甘氨酸、2，4-二硝基苯甲醛和C₆₀反应，合成分离出了含有两个硝基的新型富勒烯吡咯烷衍生物1，并对其工艺条件进行了研究，探讨了反应物剂量比、温度和时间对产物1产率的影响，得到了合成产物1的最佳工艺条件：反应物剂量比为1∶2∶6、温度为95 ℃、反应时间为40 h，此时产物1产率可达到65.8%（以消耗的C₆₀计）。同时用¹H NMR、FT-IR、MS、UV-Vis等光谱手段确定了产物1的分子结构。

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金波（1982—），男，硕士研究生.

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