Article(id=1322971598621385076, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1322971592304763246, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1235577600000, receivedDateStr=2009-02-26, revisedDate=1242662400000, revisedDateStr=2009-05-19, acceptedDate=null, acceptedDateStr=null, onlineDate=1793350608734, onlineDateStr=2026-10-30, pubDate=1260806400000, pubDateStr=2009-12-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793350608734, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793350608734, creator=13701087609, updateTime=1793350608734, updator=13701087609, issue=Issue{id=1322971592304763246, tenantId=1146029695717560320, journalId=1255847867265597444, year='2009', volume='23', issue='6', pageStart='401', pageEnd='480', issueExtLink='null', onlineDate='null', pubDate='1260806400000', pubDateStr='2009-12-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793350607229, creator='13701087609', updateTime=1793350607229, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=415, endPage=420, ext={EN=ArticleExt(id=1322971600693371255, articleId=1322971598621385076, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=Detonation Synthesis of Carbon Encapsulated Cobalt/Nickel Nanoparticles, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Carbon encapsulated cobalt and nickel magnetic nanoparticles have been synthesized successfully via detonation technique under nitrogen gas in explosion vessel. The gelatine dynamics are mainly made up of RDX explosive, mixed with nitrate cobalt or nitrate nickel, some orgnatic carbon materials at a proportion. Some testing methods such as XRD, TEM, VSM were carried out on the detonation soots, so as to characterize their morphology and properities. The results of experiments showed that the detonation products consisted of carbon encapsulated cobalt and nickel nanomaterials, with the perfect core-shell structure. The size of carbon encapsulated cobalt particles distributed between 30 and 50 nm, and the grain of carbon encapsulated nickel nanoparticles was 25~60 nm. At room temperature, they exhibited good soft magnetism.

, authors=Ning LUO, Xiao-Jie LI, Hong-Hao YAN, Xiao-Hong WANG, Li-He WANG, authorsList=Ning LUO, Xiao-Jie LI, Hong-Hao YAN, Xiao-Hong WANG, Li-He WANG, authorCompany=null, correspAuthors=Xiao-Jie LI, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322971604900258171, articleId=1322971598621385076, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=爆轰合成碳包覆钴、镍磁性纳米颗粒的探索, columnId=0, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

介绍了爆轰法合成碳包覆钴、镍纳米磁性颗粒研究的初步结果。以黑索今炸药为主体,加入钴、镍金属硝酸盐与有机碳源材料,在爆炸容器中氮气保护下用导爆管雷管引爆,成功地合成了碳包覆钴、镍纳米磁性颗粒。为了探求爆轰固体产物的形貌特征及性能,分别采用了TEM、XRD、VSM等测试手段对其进行表征。实验结果表明,爆轰产物中主要含有碳包覆纳米钴、纳米镍磁性颗粒,成球体或者椭球体,具有完好的核壳结构形貌。合成的碳包覆钴颗粒分布在30~50 nm之间,碳包覆的镍颗粒分布在25~60 nm之间,外层碳壳层主要由无定形碳和石墨构成。磁性测试表明,所得碳包金属钴、镍颗粒在室温下具有良好的软磁特性。

, authors=罗宁, 李晓杰, 闫鸿浩, 王小红, 王立鹤, authorsList=罗宁, 李晓杰, 闫鸿浩, 王小红, 王立鹤, authorCompany=null, correspAuthors=李晓杰, authorNote=

罗宁(1980—),男,博士研究生,主要从事爆炸理论及合成材料方向研究. E-mail:

, correspAuthorsNote=
李晓杰(1963—),男,教授,博士生导师,主要从事爆炸理论以及爆炸效应研究. E-mail:
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爆轰合成碳包覆钴、镍磁性纳米颗粒的探索
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罗宁 , 李晓杰 , 闫鸿浩 , 王小红 , 王立鹤
高压物理学报 | 2009,23(6): 415-420
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高压物理学报 | 2009 , 23 (6) : 415 -420
爆轰合成碳包覆钴、镍磁性纳米颗粒的探索
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罗宁 , 李晓杰 , 闫鸿浩, 王小红, 王立鹤
作者信息
  • 大连理工大学工业装备结构分析国家重点实验室,辽宁 大连 116024
通讯作者:
李晓杰(1963—),男,教授,博士生导师,主要从事爆炸理论以及爆炸效应研究. E-mail:
作者简介:

罗宁(1980—),男,博士研究生,主要从事爆炸理论及合成材料方向研究. E-mail:

Detonation Synthesis of Carbon Encapsulated Cobalt/Nickel Nanoparticles
Ning LUO , Xiao-Jie LI , Hong-Hao YAN, Xiao-Hong WANG, Li-He WANG
Affiliations
  • The State Key Laboratory of Structural Analysis for Industrial Equipment, Dalian University of Technology, Dalian 116024, China
出版时间: 2009-12-15
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介绍了爆轰法合成碳包覆钴、镍纳米磁性颗粒研究的初步结果。以黑索今炸药为主体,加入钴、镍金属硝酸盐与有机碳源材料,在爆炸容器中氮气保护下用导爆管雷管引爆,成功地合成了碳包覆钴、镍纳米磁性颗粒。为了探求爆轰固体产物的形貌特征及性能,分别采用了TEM、XRD、VSM等测试手段对其进行表征。实验结果表明,爆轰产物中主要含有碳包覆纳米钴、纳米镍磁性颗粒,成球体或者椭球体,具有完好的核壳结构形貌。合成的碳包覆钴颗粒分布在30~50 nm之间,碳包覆的镍颗粒分布在25~60 nm之间,外层碳壳层主要由无定形碳和石墨构成。磁性测试表明,所得碳包金属钴、镍颗粒在室温下具有良好的软磁特性。

爆轰合成  /  碳包覆纳米颗粒  /  磁性材料  /  核壳结构

Carbon encapsulated cobalt and nickel magnetic nanoparticles have been synthesized successfully via detonation technique under nitrogen gas in explosion vessel. The gelatine dynamics are mainly made up of RDX explosive, mixed with nitrate cobalt or nitrate nickel, some orgnatic carbon materials at a proportion. Some testing methods such as XRD, TEM, VSM were carried out on the detonation soots, so as to characterize their morphology and properities. The results of experiments showed that the detonation products consisted of carbon encapsulated cobalt and nickel nanomaterials, with the perfect core-shell structure. The size of carbon encapsulated cobalt particles distributed between 30 and 50 nm, and the grain of carbon encapsulated nickel nanoparticles was 25~60 nm. At room temperature, they exhibited good soft magnetism.

detonation synthesis  /  carbon encapsulated nanoparticales  /  magnetic naterials  /  core-shell structure
罗宁, 李晓杰, 闫鸿浩, 王小红, 王立鹤. 爆轰合成碳包覆钴、镍磁性纳米颗粒的探索. 高压物理学报, 2009 , 23 (6) : 415 -420 .
Ning LUO, Xiao-Jie LI, Hong-Hao YAN, Xiao-Hong WANG, Li-He WANG. Detonation Synthesis of Carbon Encapsulated Cobalt/Nickel Nanoparticles[J]. Chinese Journal of High Pressure Physics, 2009 , 23 (6) : 415 -420 .
  • 国家自然科学基金(10602013; 10872044; 10902023)
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2009年第23卷第6期
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  • 接收时间:2009-02-26
  • 首发时间:2026-10-30
  • 出版时间:2009-12-15
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  • 收稿日期:2009-02-26
  • 修回日期:2009-05-19
基金
国家自然科学基金(10602013; 10872044; 10902023)
作者信息
    大连理工大学工业装备结构分析国家重点实验室,辽宁 大连 116024

通讯作者:

李晓杰(1963—),男,教授,博士生导师,主要从事爆炸理论以及爆炸效应研究. E-mail:
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2种不同金属材料的力学参数
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属
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种数
Number of
species
占总种数比例
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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