Article(id=1322943239145271756, tenantId=1146029695717560320, journalId=1255847867265597444, issueId=1322943238704869834, articleNumber=null, orderNo=null, doi=null, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1204560000000, receivedDateStr=2008-03-04, revisedDate=1207497600000, revisedDateStr=2008-04-07, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343847309, onlineDateStr=2026-10-30, pubDate=1234627200000, pubDateStr=2009-02-15, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343847309, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343847309, creator=13701087609, updateTime=1793343847309, updator=13701087609, issue=Issue{id=1322943238704869834, tenantId=1146029695717560320, journalId=1255847867265597444, year='2009', volume='23', issue='1', pageStart='1', pageEnd='80', issueExtLink='null', onlineDate='null', pubDate='1234627200000', pubDateStr='2009-02-15', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343847203, creator='13701087609', updateTime=1793343847203, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=9, endPage=16, ext={EN=ArticleExt(id=1322943239308849614, articleId=1322943239145271756, tenantId=1146029695717560320, journalId=1255847867265597444, language=EN, title=p-T Phase Diagram of Coesite Synthesized from Nanometer SiO₂ Powder, columnId=null, journalTitle=Chinese Journal of High Pressure Physics, columnName=null, runingTitle=null, highlight=null, articleAbstract=

With nanometer SiO₂ powder as initial material, the p-T phase diagram (2.0~4.2 GPa, 150~1 200 ℃) of α-quartz and coesite was obtained by a series of experiments under high pressure and high temperature, and the slope of the boundary in the phase diagram is negative below 650 ℃ and is basically horizontal above 650 ℃. By means of transmission electron microscopy (TEM), X-ray diffractometer (XRD), Raman spectrometry (Raman), fourier transform infrared spectrometry (FT-IR), thermogravimetry and differential thermal analysis measurements (TG-DTA), the phenomenon that the water in the nanometer SiO₂ can decrease the synthesis temperature of coesite and quicken reaction velocity was found, and the nanometer SiO₂ can be crystallized into coesite under 4.2 GPa and 190 ℃, which is much lower than the synthesis temperatures of coesite that have been reported. Under ambient pressure, the coesite synthesized from nanometer SiO₂ can stably exist at 800 ℃ and is transformed into cristobalite above 1 000 ℃.

, authors=Guang-Qiang ZHANG¹, Yue XU², Jing-Shu SUN¹, Da-Peng XU¹, De-Yong WANG¹, Lin ZHANG¹, Yan-Feng XUE¹, Geng-Xin SONG¹, Xiao-Mei LIU¹, Wen-Hui SU^{1, 3, 4}, authorsList=Guang-Qiang ZHANG, Yue XU, Jing-Shu SUN, Da-Peng XU, De-Yong WANG, Lin ZHANG, Yan-Feng XUE, Geng-Xin SONG, Xiao-Mei LIU, Wen-Hui SU, authorCompany=null, correspAuthors=Da-Peng XU, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943239501787600, articleId=1322943239145271756, tenantId=1146029695717560320, journalId=1255847867265597444, language=CN, title=纳米SiO₂形成柯石英的p-T相图, columnId=null, journalTitle=高压物理学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

使用纳米SiO₂粉体为原料，在2.0~4.2 GPa、150~1 200 ℃范围内进行了一系列的高压高温实验研究，得到了该压力温度范围内晶化产物α-石英与柯石英的p-T相图，而且该相图中的相边界在650 ℃以下斜率为负，在650 ℃以上基本水平。通过X射线衍射仪（XRD）、Raman光谱仪（Raman）、傅立叶红外光谱仪（FT-IR）、DSC-TGA差热分析仪（TG-DTA）等表征手段，发现纳米SiO₂原粉中水分（包含Si-OH和吸附水）的存在能显著降低合成柯石英的温度和时间，在4.2 GPa压力下得到了目前合成柯石英的最低温度190 ℃。常压下，合成的柯石英在800 ℃以下能够稳定存在，在1 000 ℃以上转化为α-方石英。

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张广强（1979—），男，博士研究生，主要从事高压高温合成研究. E-mail：guangqiang_zhang@yahoo.com.cn

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张广强（1979—），男，博士研究生，主要从事高压高温合成研究. E-mail：guangqiang_zhang@yahoo.com.cn

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