Article(id=1322282093284020227, tenantId=1146029695717560320, journalId=1220038251117760515, issueId=1322281938308677669, articleNumber=null, orderNo=null, doi=10.11868/j.issn.1001-4381.2024.000352, pmid=null, cstr=32421.14.j.issn.1001-4381.2024.000352, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=research-article, receivedDate=1715616000000, receivedDateStr=2024-05-14, revisedDate=null, revisedDateStr=null, acceptedDate=1724083200000, acceptedDateStr=2024-08-20, onlineDate=1793186217852, onlineDateStr=2026-10-28, pubDate=1784476800000, pubDateStr=2026-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793186217852, onlineIssueDateStr=2026-10-28, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793186217852, creator=13701087609, updateTime=1793186217852, updator=13701087609, issue=Issue{id=1322281938308677669, tenantId=1146029695717560320, journalId=1220038251117760515, year='2026', volume='54', issue='7', pageStart='1', pageEnd='347', issueExtLink='null', onlineDate='null', pubDate='1784476800000', pubDateStr='2026-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=0, createTime=1793186180903, creator='13701087609', updateTime=1793186267843, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322282303045349604, tenantId=1146029695717560320, journalId=1220038251117760515, issueId=1322281938308677669, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322282303045349605, tenantId=1146029695717560320, journalId=1220038251117760515, issueId=1322281938308677669, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=231, endPage=240, ext={EN=ArticleExt(id=1322282094957547524, articleId=1322282093284020227, tenantId=1146029695717560320, journalId=1220038251117760515, language=EN, title=Effect of heat treatment on microstructure and mechanical properties of Ti-B25 titanium alloys, columnId=1220689384450478826, journalTitle=Journal of Materials Engineering, columnName=RESEARCH ARTICLE, runingTitle=null, highlight=null, articleAbstract=

The effect of solution temperatures，aging temperatures and aging time on the microstructure and mechanical properties of novel high-strength Ti-B25 titanium alloy is investigated by means of optical microscope，scanning electron microscope and electron backscatter diffraction. The results show that the microstructure of Ti-B25 titanium alloy consists of equiaxed primary α phase （α_p） and β matrix after solution treatment. As the solution temperature increases，the volume fraction and size of α_p phase gradually decrease，accompanied by the simultaneous deterioration of strength and ductility of the alloy. When the solution temperature is 780 ℃ and 800 ℃，with the increase of aging temperature，the secondary α phase （α_s） coarsens and decreases in volume fraction，causing a decrease in strength and an increase in ductility. At the solution temperature of 800 ℃ and aging temperature of 600 ℃，with the increase of aging time，the α_s phase continuously coarsens，and the volume fraction of α_s phase increases firstly and then decreases，resulting in an increase and then a decrease in the strength of the alloy，but little change in the ductility. After solution and aging treatment at 800 ℃/1 h/AC+600 ℃/8 h/AC，the size and volume fraction of α_s phase achieve a good balance，and the alloy achieves the best balance between strength and ductility. The tensile strength and yield strength reach 1270 MPa and 1220 MPa，respectively，while the elongation and reduction of area are 15% and 49%. Therefore，the optimal heat treatment scheme of the alloy is determined to be 800 ℃/1 h/AC+600 ℃/8 h/AC. After the optimal heat treatment，the volume fraction and grain orientation of α and β phases in the Ti-B25 titanium alloy microstructure change significantly. The volume fraction of the α phase and the proportion of high angle grain boundaries increase obviously. The α phase texture transforms from T-type texture to B-type texture，〈11\overline{\mathrm{2}}0〉∥TD and 〈10\overline{\mathrm{1}}0〉∥AD fiber texture，while the β phase texture changes from cubic texture to〈111〉∥TD fiber texture，and the texture intensity of both phases is enhanced.

, authors=Guifu ZHANG^{1, 2}, Huamei SUN², Shewei XIN^{1, 2}, Zhaoyong NING^{1, 2}, Jianhua CAI², Rong NAN², Yunlian QI², authorsList=Guifu ZHANG, Huamei SUN, Shewei XIN, Zhaoyong NING, Jianhua CAI, Rong NAN, Yunlian QI, authorCompany=null, correspAuthors=Huamei SUN, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322282096438136851, articleId=1322282093284020227, tenantId=1146029695717560320, journalId=1220038251117760515, language=CN, title=热处理对Ti-B25钛合金显微组织和力学性能的影响, columnId=1220689384622445292, journalTitle=材料工程, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

采用光学显微镜、扫描电镜、电子背散射衍射等表征技术，研究固溶温度、时效温度和时效时间对新型高强Ti-B25钛合金显微组织和力学性能的影响。结果表明：Ti-B25钛合金经固溶处理后，显微组织由等轴状初生α相（α_p）和β基体组成。随着固溶温度的升高，α_p相体积分数和尺寸不断减小，合金强度和塑性同时下降。当固溶温度为780 ℃和800 ℃时，随着时效温度的升高，次生α相（α_s）发生粗化，体积分数减少，合金强度降低而塑性升高。当固溶温度为800 ℃，时效温度为600 ℃时，随着时效时间的增加，α_s相不断粗化但体积分数先增加后减少，合金强度先升高后下降，而塑性变化不大。在800 ℃/1 h/AC+600 ℃/8 h/AC固溶时效时，α_s相尺寸和数量获得了较好的匹配，此时合金强塑性匹配最佳，抗拉强度和屈服强度分别为1270 MPa和1220 MPa，伸长率和断面收缩率分别为15%和49%。由此确定合金的最优热处理制度为：800 ℃/1 h/AC+600 ℃/8 h/AC。经过最优热处理制度处理后，Ti-B25钛合金组织中的α相和β相体积分数与晶粒取向发生显著改变，α相体积分数和大角度晶界含量明显增加。α相织构由T型织构转变为B型织构、〈11\overline{\mathrm{2}}0〉∥TD和〈10\overline{\mathrm{1}}0〉∥AD丝织构，β相织构则由立方织构转变为〈111〉∥TD丝织构，两相织构强度均有所增加。

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keyword=Ti-B25钛合金), Keyword(id=1322282100724715590, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, orderNo=2, keyword=热处理), Keyword(id=1322282100821184583, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, orderNo=3, keyword=力学性能), Keyword(id=1322282100917653576, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, orderNo=4, keyword=显微组织)], refs=[Reference(id=1322282104646389858, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, doi=null, pmid=null, pmcid=null, year=2024, volume=891, issue=null, pageStart=145970, pageEnd=null, url=null, language=null, rfNumber=[1], rfOrder=0, authorNames=LIU L L, HUANG M D, GENG D H, journalName=Materials Science and Engineering：A, refType=null, unstructuredReference=LIU L L， HUANG M D， GENG D H，et al.Achieving high strength and ductility of a metastable β-titanium alloy via coupling thermomechanical processing and heat treatments［J］.Materials Science and Engineering：A，2024，891：145970., articleTitle=Achieving high strength and ductility of a metastable β-titanium alloy via coupling thermomechanical processing and heat treatments, refAbstract=null), Reference(id=1322282104713498723, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, doi=null, pmid=null, pmcid=null, year=2024, volume=890, issue=null, pageStart=145863, pageEnd=null, url=null, language=null, rfNumber=[2], rfOrder=1, authorNames=WANG W, CHEN C Y, ZHAO R X, journalName=Materials Science and Engineering：A, refType=null, unstructuredReference=WANG W， CHEN C Y， ZHAO R X，et al.A laser additive manufactured metastable Ti-10V-2Fe-3Al β-titanium alloy：microstructure，mechanical properties，and deformation mechanisms［J］.Materials Science and Engineering：A，2024，890：145863., articleTitle=A laser additive manufactured metastable 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journalId=1220038251117760515, articleId=1322282093284020227, doi=null, pmid=null, pmcid=null, year=2021, volume=38, issue=1, pageStart=25, pageEnd=29, url=null, language=null, rfNumber=[4], rfOrder=3, authorNames=孙花梅, 刘伟, 戚运莲, journalName=钛工业进展, refType=null, unstructuredReference=孙花梅，刘伟，戚运莲，等.Ti-B25钛合金管材挤压成形数值模拟及实验研究［J］.钛工业进展，2021，38（1）：25-29., articleTitle=Ti-B25钛合金管材挤压成形数值模拟及实验研究, refAbstract=null), Reference(id=1322282104939991142, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, doi=null, pmid=null, pmcid=null, year=2021, volume=38, issue=1, pageStart=25, pageEnd=29, url=null, language=null, rfNumber=[4], rfOrder=4, authorNames=SUN H M, LIU W, QI Y L, journalName=Titanium Industry Progress, refType=null, unstructuredReference=SUN H M， LIU W， QI Y L，et al.Numerical simulation and experimental study of extrusion forming of Ti-B25 titanium alloy pipe［J］.Titanium Industry Progress，2021，38（1）：25-29., articleTitle=null, refAbstract=null), Reference(id=1322282105002905703, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, doi=null, pmid=null, pmcid=null, year=2022, volume=39, issue=1, pageStart=6, pageEnd=11, url=null, language=null, rfNumber=[5], rfOrder=5, authorNames=孙花梅, 刘伟, 戚运莲, journalName=钛工业进展, refType=null, unstructuredReference=孙花梅，刘伟，戚运莲，等.Ti-B25合金高温变形时的塑性流动软化行为［J］.钛工业进展，2022，39（1）：6-11., articleTitle=Ti-B25合金高温变形时的塑性流动软化行为, refAbstract=null), Reference(id=1322282105070014568, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, doi=null, pmid=null, pmcid=null, year=2022, volume=39, issue=1, pageStart=6, pageEnd=11, url=null, language=null, rfNumber=[5], rfOrder=6, authorNames=SUN H M, LIU W, QI Y L, journalName=Titanium Industry Progress, refType=null, unstructuredReference=SUN H M， LIU W， QI Y L，et al.Plastic flow softening behavior of Ti-B25 alloy during high temperature deformation［J］.Titanium Industry 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ArticleFig(id=1322282101160923210, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, label=图1, caption=锻态Ti-B25钛合金的光学显微组织, figureFileSmall=a+760JQzBHn2JKPo5NyjQA==, figureFileBig=7TvkP6cNVwELefuSKXDAdg==, tableContent=null), ArticleFig(id=1322282101433552971, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=EN, label=Fig.2, caption=Microstructures of Ti-B25 titanium alloy at different solution temperatures, figureFileSmall=ZNoi/I5oyzhGQqqBeBnIRg==, figureFileBig=my7Yj3g+innOfmXmzqgXrQ==, tableContent=null), ArticleFig(id=1322282101530021964, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, label=图2, caption=Ti-B25钛合金在不同固溶温度下的显微组织

（a）780 ℃；（b）800 ℃；（c）840 ℃

, figureFileSmall=ZNoi/I5oyzhGQqqBeBnIRg==, figureFileBig=my7Yj3g+innOfmXmzqgXrQ==, tableContent=null), ArticleFig(id=1322282101609713741, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=EN, label=Fig.3, caption=Microstructures of Ti-B25 titanium alloy at different solution temperatures and aged at different temperatures, figureFileSmall=85FhJMf6gYl07BM2yq1C3A==, figureFileBig=/hMlcrvRidibiS2gahm6lQ==, tableContent=null), ArticleFig(id=1322282101718765646, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, label=图3, caption=Ti-B25钛合金在不同固溶温度下经不同温度时效时的显微组织

（a）780 ℃/1 h+550 ℃/8 h；（b）780 ℃/1 h+600 ℃/8 h；（c）800 ℃/1 h+550 ℃/8 h；（d）800 ℃/1 h+600 ℃/8 h

, figureFileSmall=85FhJMf6gYl07BM2yq1C3A==, figureFileBig=/hMlcrvRidibiS2gahm6lQ==, tableContent=null), ArticleFig(id=1322282101785874511, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=EN, label=Fig.4, caption=Microstructures of Ti-B25 titanium alloy aged at 600 ℃ for different time after solution treatment at 800 ℃, figureFileSmall=GUTqaOugVfk9mc8TSM0b9g==, figureFileBig=lzvHCormAH3kR9Z8XciykQ==, tableContent=null), ArticleFig(id=1322282101861371985, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, label=图4, caption=Ti-B25钛合金800 ℃固溶处理后在600 ℃时效不同时间的显微组织

（a）4 h；（b）6 h；（c）8 h；（d）10 h

（a）4 h；（b）6 h；（c）8 h；（d）10 h

, figureFileSmall=GUTqaOugVfk9mc8TSM0b9g==, figureFileBig=lzvHCormAH3kR9Z8XciykQ==, tableContent=null), ArticleFig(id=1322282101924286546, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=EN, label=Fig.5, caption=Phase distribution maps（1） and grain orientation maps（2） of as-forged and solution-aged Ti-B25 titanium alloy（a）as-forged；（b）800 ℃/1 h/AC+600 ℃/8 h/AC, figureFileSmall=mdvF8WXRDfJWEH75ZU77xw==, figureFileBig=19ET8LDXS6Fp5VFfqfYhIQ==, tableContent=null), ArticleFig(id=1322282102008172627, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, label=图5, caption=Ti-B25钛合金锻态和固溶时效态的相分布图（1）和晶粒取向图（2）（a）锻态；（b）800 ℃/1 h/AC+600 ℃/8 h/AC, figureFileSmall=mdvF8WXRDfJWEH75ZU77xw==, figureFileBig=19ET8LDXS6Fp5VFfqfYhIQ==, tableContent=null), ArticleFig(id=1322282102071087188, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=EN, label=Fig.6, caption=Misorientation angle distribution maps of as-forged and 800 ℃/1 h/AC+600 ℃/8 h/AC solution-aged Ti-B25 titanium alloy（a）α phase；（b）β phase, figureFileSmall=5d2c2c9U/Utp28+Gl6LY4A==, figureFileBig=EhDv2EdxgwNyYDPLn3UGQQ==, tableContent=null), ArticleFig(id=1322282102138196053, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, label=图6, caption=Ti-B25钛合金锻态和800 ℃/1 h/AC+600 ℃/8 h/AC固溶时效态晶粒取向差分布图（a）α相；（b）β相, figureFileSmall=5d2c2c9U/Utp28+Gl6LY4A==, figureFileBig=EhDv2EdxgwNyYDPLn3UGQQ==, tableContent=null), ArticleFig(id=1322282103782363223, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=EN, label=Fig.7, caption=Pole figures of Ti-B25 titanium alloy under different states

（a）as-forged；（b）800 ℃/1 h/AC+600 ℃/8 h/AC

, figureFileSmall=ToISJIHHjEkRzjdCAvrAzA==, figureFileBig=hFtk1WKEcvo2aHq+9dTm/w==, tableContent=null), ArticleFig(id=1322282103891415128, tenantId=1146029695717560320, journalId=1220038251117760515, articleId=1322282093284020227, language=CN, label=图7, caption=Ti-B25钛合金不同状态下的极图

（a）锻态；（b）800 ℃/1 h/AC+600 ℃/8 h/AC

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Different heat treatment schemes

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Sample No.	Heat treatment
1	780 ℃/1 h/AC
2	800 ℃/1 h/AC
3	820 ℃/1 h/AC
4	840 ℃/1 h/AC
5	780 ℃/1 h/AC+550 ℃/8 h/AC
6	780 ℃/1 h/AC+580 ℃/8 h/AC
7	780 ℃/1 h/AC+600 ℃/8 h/AC
8	800 ℃/1 h/AC+550 ℃/8 h/AC
9	800 ℃/1 h/AC+580 ℃/8 h/AC
10	800 ℃/1 h/AC+600 ℃/8 h/AC
11	800 ℃/1 h/AC+600 ℃/4 h/AC
12	800 ℃/1 h/AC+600 ℃/6 h/AC
13	800 ℃/1 h/AC+600 ℃/10 h/AC

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不同的热处理制度

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Sample No.	Heat treatment
1	780 ℃/1 h/AC
2	800 ℃/1 h/AC
3	820 ℃/1 h/AC
4	840 ℃/1 h/AC
5	780 ℃/1 h/AC+550 ℃/8 h/AC
6	780 ℃/1 h/AC+580 ℃/8 h/AC
7	780 ℃/1 h/AC+600 ℃/8 h/AC
8	800 ℃/1 h/AC+550 ℃/8 h/AC
9	800 ℃/1 h/AC+580 ℃/8 h/AC
10	800 ℃/1 h/AC+600 ℃/8 h/AC
11	800 ℃/1 h/AC+600 ℃/4 h/AC
12	800 ℃/1 h/AC+600 ℃/6 h/AC
13	800 ℃/1 h/AC+600 ℃/10 h/AC

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Room temperature tensile properties of Ti-B25 titanium alloy at different solution temperatures

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Condition	Rm/MPa	Rp0.2/MPa	A/%	Z/%
780 ℃/1 h/AC	1034±3.51	998±6.51	18±0.25	66±1.00
800 ℃/1 h/AC	1015±0.58	951±5.51	19±0.75	61±0.50
820 ℃/1 h/AC	1009±3.00	949±5.00	17.5±1.75	57±0.50
840 ℃/1 h/AC	983±6.00	908±1.53	17±1.25	44±0.50

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Ti-B25钛合金在不同固溶温度下的室温拉伸性能

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Condition	Rm/MPa	Rp0.2/MPa	A/%	Z/%
780 ℃/1 h/AC	1034±3.51	998±6.51	18±0.25	66±1.00
800 ℃/1 h/AC	1015±0.58	951±5.51	19±0.75	61±0.50
820 ℃/1 h/AC	1009±3.00	949±5.00	17.5±1.75	57±0.50
840 ℃/1 h/AC	983±6.00	908±1.53	17±1.25	44±0.50

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Room temperature tensile properties of Ti-B25 titanium alloy at different aging temperatures

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Condition	Rm/MPa	Rp0.2/MPa	A/%	Z/%
780 ℃/1 h/AC+550 ℃/8 h/AC	1256±1.53	1214±3.51	16±0.25	53±0.50
780 ℃/1 h/AC+580 ℃/8 h/AC	1284±5.00	1235±4.51	11.5±0.50	50±1.00
780 ℃/1 h/AC+600 ℃/8 h/AC	1169±7.00	1137±0.58	17±0.00	53±0.00
800 ℃/1 h/AC+550 ℃/8 h/AC	1401±1.53	1308±3.00	11.5±1.00	49±3.50
800 ℃/1 h/AC+580 ℃/8 h/AC	1284±11.50	1231±10.50	13.5±1.00	48±1.00
800 ℃/1 h/AC+600 ℃/8 h/AC	1270±3.00	1220±2.52	15±0.75	49±0.50

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Ti-B25钛合金在不同时效温度下的室温拉伸性能

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Condition	Rm/MPa	Rp0.2/MPa	A/%	Z/%
780 ℃/1 h/AC+550 ℃/8 h/AC	1256±1.53	1214±3.51	16±0.25	53±0.50
780 ℃/1 h/AC+580 ℃/8 h/AC	1284±5.00	1235±4.51	11.5±0.50	50±1.00
780 ℃/1 h/AC+600 ℃/8 h/AC	1169±7.00	1137±0.58	17±0.00	53±0.00
800 ℃/1 h/AC+550 ℃/8 h/AC	1401±1.53	1308±3.00	11.5±1.00	49±3.50
800 ℃/1 h/AC+580 ℃/8 h/AC	1284±11.50	1231±10.50	13.5±1.00	48±1.00
800 ℃/1 h/AC+600 ℃/8 h/AC	1270±3.00	1220±2.52	15±0.75	49±0.50

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Room temperature tensile properties of Ti-B25 titanium alloy under different aging time

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Condition	Rm/MPa	Rp0.2/MPa	A/%	Z/%
800 ℃/1 h/AC+600 ℃/4 h/AC	1234±7.00	1173±7.00	16±0.75	47±0.00
800 ℃/1 h/AC+600 ℃/6 h/AC	1235±3.00	1177±0.58	14.5±0.50	46±4.50
800 ℃/1 h/AC+600 ℃/8 h/AC	1270±3.00	1220±2.52	15±0.75	49±0.50
800 ℃/1 h/AC+600 ℃/10 h/AC	1178±11.00	1145±1.00	16±0.75	49±4.50

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Ti-B25钛合金在不同时效时间下的室温拉伸性能

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Condition	Rm/MPa	Rp0.2/MPa	A/%	Z/%
800 ℃/1 h/AC+600 ℃/4 h/AC	1234±7.00	1173±7.00	16±0.75	47±0.00
800 ℃/1 h/AC+600 ℃/6 h/AC	1235±3.00	1177±0.58	14.5±0.50	46±4.50
800 ℃/1 h/AC+600 ℃/8 h/AC	1270±3.00	1220±2.52	15±0.75	49±0.50
800 ℃/1 h/AC+600 ℃/10 h/AC	1178±11.00	1145±1.00	16±0.75	49±4.50

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