Article(id=1282029998617899437, tenantId=1146029695717560320, journalId=1146031787341344770, issueId=1282029960869167928, articleNumber=null, orderNo=null, doi=10.16265/j.cnki.issn1003-3033.2025.07.1462, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1739462400000, receivedDateStr=2025-02-14, revisedDate=1744905600000, revisedDateStr=2025-04-18, acceptedDate=null, acceptedDateStr=null, onlineDate=1783589370636, onlineDateStr=2026-07-09, pubDate=1753632000000, pubDateStr=2025-07-28, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1783589370636, onlineIssueDateStr=2026-07-09, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1783589370636, creator=13701087609, updateTime=1783589370636, updator=13701087609, issue=Issue{id=1282029960869167928, tenantId=1146029695717560320, journalId=1146031787341344770, year='2025', volume='35', issue='7', pageStart='1', pageEnd='252', issueExtLink='null', onlineDate='null', pubDate='1753632000000', pubDateStr='2025-07-28', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1783589361636, creator='13701087609', updateTime=1783589710614, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1282031424651903975, tenantId=1146029695717560320, journalId=1146031787341344770, issueId=1282029960869167928, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1282031424656098280, tenantId=1146029695717560320, journalId=1146031787341344770, issueId=1282029960869167928, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=114, endPage=121, ext={EN=ArticleExt(id=1282029999104438702, articleId=1282029998617899437, tenantId=1146029695717560320, journalId=1146031787341344770, language=EN, title=Curing and pyrolysis kinetics of flame-retardant epoxy resin/low-molecular-weight polyphenylene oxide composites, columnId=1149733269173878863, journalTitle=China Safety Science Journal, columnName=Safety engineering technology, runingTitle=null, highlight=null, articleAbstract=

To improve the safety of EP in application fields, Calcium Terephthalate(CaT), a metal-organic framework (MOF) material, was utilized synergistically with the liquid flame retardant bisphenol A bis (diphenyl phosphate) (BDP) to flame-retardant modify the EP/PPO system. The flame retardant properties were characterized using the limiting oxygen index, vertical burning test, and cone calorimeter tests. The curing kinetics and pyrolysis kinetics of the modified EP/PPO system were investigated using the Kissinger, FWO (Flynn-Wall-Ozawa), and Crane equations. The results show that when 8% BDP and 2% CaT are added to EP, the composite exhibits good flame retardant performance. 34.5% of the limiting oxygen index is reached. V-0 rating of the vertical burning test is achieved. The peak heat release rate and the total heat release are reduced by 76.6% and 51.5% respectively compared to pure EP. The incorporation of CaT is found to be beneficial for the curing reaction. The optimal curing temperature could be determined by extrapolation from non-isothermal differential scanning calorimetry curves. It is an initial stage at 100 ℃, followed by 120 ℃, and finally 170 ℃. Analysis of non-isothermal thermogravimetric analysis curves and pyrolysis kinetics demonstrates that EP/PPO system exhibits lower activation energy.

, authors=Xueying SHAN¹, Jiafu ZHANG¹, Qixin HUANG¹, Yuxuan DIAO¹, Jinchun LI², Lingyu LI², authorsList=Xueying SHAN, Jiafu ZHANG, Qixin HUANG, Yuxuan DIAO, Jinchun LI, Lingyu LI, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1282029999549034927, articleId=1282029998617899437, tenantId=1146029695717560320, journalId=1146031787341344770, language=CN, title=阻燃型环氧树脂/低分子聚苯醚材料固化及热解动力学, columnId=1149733269727526997, journalTitle=中国安全科学学报, columnName=安全工程技术, runingTitle=null, highlight=null, articleAbstract=

为提高环氧树脂（EP）在应用领域的安全性，使用苯二甲酸钙（CaT）这一有机金属框架化合物（MOF）材料，协同液体阻燃剂双酚A双（二苯基磷酸酯）（BDP）阻燃改性EP/低分子聚苯醚（PPO）体系，通过极限氧指数、垂直燃烧测试和锥形量热测试表征其阻燃性能，并利用Kissinger、FWO和Crane方程研究改性EP/PPO体系的固化动力学及热解动力学。结果表明：当添加8%BDP和2%CaT至EP中，复合材料表现出良好的阻燃性能，极限氧指数达34.5%，垂直燃烧测试获V-0级别，且其峰值热释放速率和总热释放较纯EP分别降低76.6%及51.5%；CaT有利于固化反应；利用非等温差示扫描量热曲线外推法能够得到最佳固化温度为：初始100 ℃，后120 ℃，最后170 ℃；通过非等温热重分析及热解动力学分析可发现EP/PPO体系表现出更低的活化能。

, authors=单雪影副教授¹, 张家傅¹, 黄其鑫¹, 刁玉璇¹, 李锦春教授², 李玲玉², authorsList=单雪影副教授, 张家傅, 黄其鑫, 刁玉璇, 李锦春教授, 李玲玉, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=fELjHU+QriRTBXfdHDnXrQ==, magXml=NEG8S9bniMowRS1kf4l0PA==, pdfUrl=null, pdf=l4mgZFZNT+aIFeBVJy1A/w==, pdfFileSize=11142130, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=pVlj4zqVNiqG/iho8Zvo4w==, mapNumber=null, fund=null)}, authors=[Author(id=1282029999976853943, tenantId=1146029695717560320, journalId=1146031787341344770, articleId=1282029998617899437, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=xyshan@cczu.edu.cn, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1282030000052351417, tenantId=1146029695717560320, journalId=1146031787341344770, articleId=1282029998617899437, authorId=1282029999976853943, language=EN, stringName=Xueying SHAN, firstName=Xueying, middleName=null, lastName=SHAN, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=¹, address=¹School of Safety Science and Engineering, Changzhou University, Changzhou Jiangsu 213164, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1282030000140431802, tenantId=1146029695717560320, journalId=1146031787341344770, articleId=1282029998617899437, authorId=1282029999976853943, language=CN, stringName=单雪影副教授, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=¹, address=¹常州大学 安全科学与工程学院，江苏 常州 213164, bio={"content":"

单雪影（1986—），女，安徽宿州人，博士，副教授，主要从事高分子材料改性、材料火灾安全方面的研究。E-mail: xyshan@cczu.edu.cn。

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单雪影（1986—），女，安徽宿州人，博士，副教授，主要从事高分子材料改性、材料火灾安全方面的研究。E-mail: xyshan@cczu.edu.cn。

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