Article(id=1322941735042691593, tenantId=1146029695717560320, journalId=1322258508890079423, issueId=1322941491332657306, articleNumber=null, orderNo=null, doi=10.13809/j.cnki.cn32-1825/te.2025440, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1773849600000, receivedDateStr=2026-03-19, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343488703, onlineDateStr=2026-10-30, pubDate=1795622400000, pubDateStr=2026-11-26, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343488703, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343488703, creator=13701087609, updateTime=1793343488703, updator=13701087609, issue=Issue{id=1322941491332657306, tenantId=1146029695717560320, journalId=1322258508890079423, year='2026', volume='16', issue='6', pageStart='1137', pageEnd='1368', issueExtLink='null', onlineDate='null', pubDate='1795622400000', pubDateStr='2026-11-26', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1793343430598, creator='13701087609', updateTime=1793344116766, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322944369447285513, tenantId=1146029695717560320, journalId=1322258508890079423, issueId=1322941491332657306, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322944369447285514, tenantId=1146029695717560320, journalId=1322258508890079423, issueId=1322941491332657306, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1304, endPage=1312, ext={EN=ArticleExt(id=1322941735256601100, articleId=1322941735042691593, tenantId=1146029695717560320, journalId=1322258508890079423, language=EN, title=Research on dynamic imbibition mechanism of shale oil based on NMR experiments, columnId=1322941693024141328, journalTitle=Petroleum Reservoir Evaluation and Development, columnName=Oil and Gas Development, runingTitle=null, highlight=
Continental shale oil resources in China are abundant and serve as an important strategic replacement resource for ensuring national energy security. Shale oil reservoirs are characterized by well-developed nanopores and ultra-low porosity and permeability, and clarifying the imbibition mechanism is of great significance for increasing the shale oil recovery degree. Taking laminated argillaceous calcareous shale from the Jiyang Depression as the research object, the pore structure characteristics were quantitatively evaluated using focused ion beam-scanning electron microscopy (FIB-SEM) three-dimensional imaging and digital core reconstruction methods. On this basis, high-temperature and high-pressure nuclear magnetic resonance (NMR) dynamic imbibition experiments were conducted to simulate co-current imbibition during high-pressure injection of fracturing fluid. By acquiring transverse relaxation time (T2) spectra at different imbibition times, the mobilization characteristics of crude oil in pores of different scales were quantitatively analyzed. The T2 cutoff method was employed to distinguish the contributions of displacement and imbibition to oil recovery. Meanwhile, the effects of displacement pressure difference and bedding fractures on dynamic imbibition performance were analyzed. Based on similarity criteria, the relationship between laboratory scale and reservoir scale was established to calculate and optimize the soaking time after hydraulic fracturing. The results showed that (1) the dynamic imbibition process could be divided into three stages—rapid imbibition, slow imbibition, and imbibition equilibrium, exhibiting a pattern of elastic oil displacement in large pores and imbibition-driven oil replacement in small pores. (2) Under experimental conditions, an optimal displacement pressure difference range existed for dynamic imbibition (2.67-4.16 MPa). Within this range, the total recovery degree increased by 9.02%-10.26% compared with that under the lower displacement pressure difference condition (1.05 MPa). (3) Bedding fractures improved the connectivity of the pore structure and increased imbibition efficiency, serving as favorable petrophysical conditions for enhancing shale oil mobilization. (4) Based on similarity criteria and dynamic imbibition experimental results, the recommended soaking time for shale oil reservoirs after hydraulic fracturing was 15 d.
, articleAbstract=null, authors=GUANG LU1, SHIMING ZHANG2, XIAOPENG CAO1, LYU QI1, LONG JIANG1, HONGXIA SUN1, ZUPENG LIU1, ZHONGXIN LI1, YAN LIU1, ZENGHUI CAO1, authorsList=GUANG LU, SHIMING ZHANG, XIAOPENG CAO, LYU QI, LONG JIANG, HONGXIA SUN, ZUPENG LIU, ZHONGXIN LI, YAN LIU, ZENGHUI CAO, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322941739337658921, articleId=1322941735042691593, tenantId=1146029695717560320, journalId=1322258508890079423, language=CN, title=基于核磁共振实验的页岩油动态渗吸机理研究, columnId=1322941693259022355, journalTitle=油气藏评价与开发, columnName=油气开发, runingTitle=null, highlight=
中国陆相页岩油资源丰富,是保障国家能源安全的重要战略性接替资源。页岩油藏纳米孔隙发育且孔隙度、渗透率极低,阐明渗吸机理对提高页岩油采出程度具有重要意义。以济阳坳陷纹层状灰质页岩为研究对象,基于聚焦离子束-扫描电子显微镜(FIB-SEM)三维成像与数字岩心重构方法,定量表征其孔隙结构特征。在此基础上,开展高温高压核磁共振动态渗吸实验,模拟压裂液高压注入过程中的同向渗吸行为。通过获取不同渗吸时间下核磁共振T2谱的演化特征谱,定量表征不同尺度孔隙中原油的动用特征。采用T2截止值法区分驱替作用与渗吸作用对采出程度的贡献,分析驱替压差及层理缝对动态渗吸效果的影响。结合渗吸相似准则,建立实验与油藏尺度的对应关系,计算并优化页岩油藏压裂后的焖井时间。结果表明:①动态渗吸过程可划分为快速渗吸、缓慢渗吸和渗吸平衡3个阶段,整体呈现“大孔隙弹性驱动、小孔隙渗吸换油”的动用特征;②实验条件下,动态渗吸存在最优驱替压差范围(2.67~4.16 MPa),该区间内总采出程度较低驱替压差(1.05 MPa)条件下提高9.02%~10.26%;③层理缝可改善孔隙结构的连通性,提高渗吸置换效率,是提升页岩油动用程度的有利储层条件;④基于相似准则及动态渗吸实验结果,推荐页岩油藏压裂后合理焖井时间为15 d。
, articleAbstract=null, authors=路广1, 张世明2, 曹小朋1, 吕琦1, 蒋龙1, 孙红霞1, 刘祖鹏1, 李忠新1, 刘艳1, 曹增辉1, authorsList=路广, 张世明, 曹小朋, 吕琦, 蒋龙, 孙红霞, 刘祖鹏, 李忠新, 刘艳, 曹增辉, authorCompany=null, correspAuthors=null, authorNote=
路广(1993—),男,博士,助理研究员,主要从事油气田开发研究工作。地址:山东省东营市东营区聊城路 2 号,邮政编码:257015。E-mail: 1263556399@qq.com
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路广(1993—),男,博士,助理研究员,主要从事油气田开发研究工作。地址:山东省东营市东营区聊城路 2 号,邮政编码:257015。E-mail: 1263556399@qq.com
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路广(1993—),男,博士,助理研究员,主要从事油气田开发研究工作。地址:山东省东营市东营区聊城路 2 号,邮政编码:257015。E-mail: 1263556399@qq.com
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1 Exploration and Development Research Institute, Sinopec Shengli Oilfield Company, Dongying, Shandong 257015, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1322941742684713537, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, authorId=1322941742512747070, language=CN, stringName=曹小朋, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, address=
1 中国石化胜利油田分公司勘探开发研究院,山东 东营 257015, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1322941739601900074, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, xref=1, ext=[AuthorCompanyExt(id=1322941739622871595, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, companyId=1322941739601900074, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
1 Exploration and Development Research Institute, Sinopec Shengli Oilfield Company, Dongying, Shandong 257015, China), AuthorCompanyExt(id=1322941739635454508, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, companyId=1322941739601900074, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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1 Exploration and Development Research Institute, Sinopec Shengli Oilfield Company, Dongying, Shandong 257015, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1322941742957343302, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, authorId=1322941742785376835, language=CN, stringName=吕琦, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, address=
1 中国石化胜利油田分公司勘探开发研究院,山东 东营 257015, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1322941739601900074, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, xref=1, ext=[AuthorCompanyExt(id=1322941739622871595, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, companyId=1322941739601900074, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
1 Exploration and Development Research Institute, Sinopec Shengli Oilfield Company, Dongying, Shandong 257015, China), AuthorCompanyExt(id=1322941739635454508, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, companyId=1322941739601900074, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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1 Exploration and Development Research Institute, Sinopec Shengli Oilfield Company, Dongying, Shandong 257015, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1322941743297081932, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, authorId=1322941743032840777, language=CN, stringName=蒋龙, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, address=
1 中国石化胜利油田分公司勘探开发研究院,山东 东营 257015, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null)}, companyList=[AuthorCompany(id=1322941739601900074, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, xref=1, ext=[AuthorCompanyExt(id=1322941739622871595, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, companyId=1322941739601900074, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
1 Exploration and Development Research Institute, Sinopec Shengli Oilfield Company, Dongying, Shandong 257015, China), AuthorCompanyExt(id=1322941739635454508, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, companyId=1322941739601900074, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=
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1 Exploration and Development Research Institute, Sinopec Shengli Oilfield Company, Dongying, Shandong 257015, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1322941743649403474, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, authorId=1322941743376773710, language=CN, stringName=孙红霞, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=1, address=
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High-resolution MAPS images of laminated argillaceous calcareous shale in Boxing Subsag, Jiyang Depression, figureFileSmall=IAYPapMZ3zRhGaX39kt3Cw==, figureFileBig=Oc5hAeY3MIX26q6R8pQ05g==, tableContent=null), ArticleFig(id=1322941752214172287, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图1, caption=
济阳坳陷博兴洼陷纹层状灰质页岩高分辨率MAPS图像, figureFileSmall=IAYPapMZ3zRhGaX39kt3Cw==, figureFileBig=Oc5hAeY3MIX26q6R8pQ05g==, tableContent=null), ArticleFig(id=1322941752851706497, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 2, caption=
3D reconstruction of digital cores and pore network extraction based on FIB-SEM serial images, figureFileSmall=pNHthGh1XJy10RlLtR6wVQ==, figureFileBig=Ylg8ea3UhZDDJE1eHjytlQ==, tableContent=null), ArticleFig(id=1322941752927203971, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图2, caption=
三维FIB-SEM序列图像的数字岩心三维孔隙网络提取, figureFileSmall=pNHthGh1XJy10RlLtR6wVQ==, figureFileBig=Ylg8ea3UhZDDJE1eHjytlQ==, tableContent=null), ArticleFig(id=1322941753262748292, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 3, caption=
Frequency histograms of pore diameter distributions, figureFileSmall=kvH7/UUkqpCkFXfNHeYhQw==, figureFileBig=4tnx2JFFX+XAQLr2FXVJTg==, tableContent=null), ArticleFig(id=1322941753363411589, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图3, caption=
孔隙直径分布频率直方图, figureFileSmall=kvH7/UUkqpCkFXfNHeYhQw==, figureFileBig=4tnx2JFFX+XAQLr2FXVJTg==, tableContent=null), ArticleFig(id=1322941753430520455, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 4, caption=
Frequency histograms of pore coordination number distributions, figureFileSmall=goWn3nZc4BNerPzR/aUcjg==, figureFileBig=u7dwVG3oN8PfE5hG6W4Msg==, tableContent=null), ArticleFig(id=1322941753501823624, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图4, caption=
孔隙配位数分布频率直方图, figureFileSmall=goWn3nZc4BNerPzR/aUcjg==, figureFileBig=u7dwVG3oN8PfE5hG6W4Msg==, tableContent=null), ArticleFig(id=1322941753694761609, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 5, caption=
Schematic diagram of dynamic imbibition experimental device, figureFileSmall=8a6QAVfs3PTOfvkZZMHuJA==, figureFileBig=SkB5s7SPMavoRz4I6cyzCQ==, tableContent=null), ArticleFig(id=1322941753799619211, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图5, caption=
动态渗吸实验装置, figureFileSmall=8a6QAVfs3PTOfvkZZMHuJA==, figureFileBig=SkB5s7SPMavoRz4I6cyzCQ==, tableContent=null), ArticleFig(id=1322941754118386316, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 6, caption=
NMR T2 spectra of cores during dynamic imbibition, figureFileSmall=e3gWYfcEJHKrWIXKnBGFtA==, figureFileBig=rOHCI91z2cEOGZiItRDV+g==, tableContent=null), ArticleFig(id=1322941755833856654, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图6, caption=
岩心动态渗吸核磁共振T2谱, figureFileSmall=e3gWYfcEJHKrWIXKnBGFtA==, figureFileBig=rOHCI91z2cEOGZiItRDV+g==, tableContent=null), ArticleFig(id=1322941755913548431, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 7, caption=
Relationship curves between core recovery degree and dynamic imbibition time, figureFileSmall=an2KZmp7uo93kfcloeqr2w==, figureFileBig=vxVwGnM5E7V05YiUEHEycw==, tableContent=null), ArticleFig(id=1322941756249092752, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图7, caption=
岩心采出程度与动态渗吸时间关系曲线, figureFileSmall=an2KZmp7uo93kfcloeqr2w==, figureFileBig=vxVwGnM5E7V05YiUEHEycw==, tableContent=null), ArticleFig(id=1322941756618191505, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 8, caption=
Relationship curves between recovery degree of different pore sizes and dynamic imbibition time for core 3, figureFileSmall=GYP2IqFEesJQN72R7AY0PQ==, figureFileBig=2y/4+RqkR18nMGXOay1wTA==, tableContent=null), ArticleFig(id=1322941756718854802, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图8, caption=
3号岩心不同孔径孔隙采出程度与动态渗吸时间关系曲线, figureFileSmall=GYP2IqFEesJQN72R7AY0PQ==, figureFileBig=2y/4+RqkR18nMGXOay1wTA==, tableContent=null), ArticleFig(id=1322941757058593427, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 9, caption=
Bar chart of recovery degree by imbibition and displacement, and variation curve of total recovery degree under different displacement pressure differences, figureFileSmall=n2CY+Y/xU3UzbmIL4OczSQ==, figureFileBig=wnqZusJNBYznpAlNMUwTVw==, tableContent=null), ArticleFig(id=1322941757146673812, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图9, caption=
不同驱替压差下渗吸与驱替作用采出程度柱状图及总采出程度变化曲线, figureFileSmall=n2CY+Y/xU3UzbmIL4OczSQ==, figureFileBig=wnqZusJNBYznpAlNMUwTVw==, tableContent=null), ArticleFig(id=1322941757461246613, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Fig. 10, caption=
Comparison of dynamic imbibition recovery degree between horizontal and vertical core samples, figureFileSmall=AZjDo8W+2UOsqfAAR0Imzg==, figureFileBig=zIsap6o6zRedG4BivCyDLg==, tableContent=null), ArticleFig(id=1322941757557715606, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=图10, caption=
水平岩样与垂直岩样动态渗吸采出程度对比, figureFileSmall=AZjDo8W+2UOsqfAAR0Imzg==, figureFileBig=zIsap6o6zRedG4BivCyDLg==, tableContent=null), ArticleFig(id=1322941757629018775, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=EN, label=Table 1, caption=
Basic parameters of laminated argillaceous calcareous shale cores from Boxing Subsag,Jiyang Depression, figureFileSmall=null, figureFileBig=null, tableContent=
| 岩心编号 | 长度/ cm | 直径/ cm | 孔隙度/ % | 渗透率/ 10-3 μm2 | 备注 |
|---|
| 1 | 4.32 | 2.45 | 2.9 | 0.002 4 | 水平岩样 |
| 2 | 3.53 | 2.45 | 3.1 | 0.013 1 | 水平岩样 |
| 3 | 4.02 | 2.47 | 2.7 | 0.004 8 | 水平岩样 |
| 4 | 4.28 | 2.48 | 3.6 | 0.019 9 | 水平岩样 |
| 5 | 4.31 | 2.44 | 3.9 | 0.032 6 | 水平岩样 |
| 6V | 3.98 | 2.45 | 3.5 | 0.020 9 | 垂直岩样 |
), ArticleFig(id=1322941757876482712, tenantId=1146029695717560320, journalId=1322258508890079423, articleId=1322941735042691593, language=CN, label=表1, caption=
济阳坳陷博兴洼陷的纹层状灰质页岩岩心基础参数
, figureFileSmall=null, figureFileBig=null, tableContent=
| 岩心编号 | 长度/ cm | 直径/ cm | 孔隙度/ % | 渗透率/ 10-3 μm2 | 备注 |
|---|
| 1 | 4.32 | 2.45 | 2.9 | 0.002 4 | 水平岩样 |
| 2 | 3.53 | 2.45 | 3.1 | 0.013 1 | 水平岩样 |
| 3 | 4.02 | 2.47 | 2.7 | 0.004 8 | 水平岩样 |
| 4 | 4.28 | 2.48 | 3.6 | 0.019 9 | 水平岩样 |
| 5 | 4.31 | 2.44 | 3.9 | 0.032 6 | 水平岩样 |
| 6V | 3.98 | 2.45 | 3.5 | 0.020 9 | 垂直岩样 |
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