Article(id=1289282137862025608, tenantId=1146029695717560320, journalId=1287019424739590152, issueId=1289282136750539420, articleNumber=null, orderNo=null, doi=10.12442/j.issn.1002-185X.20250143, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1752681600000, receivedDateStr=2025-07-17, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1785318415370, onlineDateStr=2026-07-29, pubDate=1783612800000, pubDateStr=2026-07-10, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1785318415370, onlineIssueDateStr=2026-07-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1785318415370, creator=13701087609, updateTime=1785318415370, updator=13701087609, issue=Issue{id=1289282136750539420, tenantId=1146029695717560320, journalId=1287019424739590152, year='2026', volume='55', issue='7', pageStart='1701', pageEnd='1848', issueExtLink='null', onlineDate='null', pubDate='1783612800000', pubDateStr='2026-07-10', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1785318415105, creator='13701087609', updateTime=1785389094930, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1289578589494555490, tenantId=1146029695717560320, journalId=1287019424739590152, issueId=1289282136750539420, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1289578589498749795, tenantId=1146029695717560320, journalId=1287019424739590152, issueId=1289282136750539420, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1733, endPage=1740, ext={EN=ArticleExt(id=1289282138017214857, articleId=1289282137862025608, tenantId=1146029695717560320, journalId=1287019424739590152, language=EN, title=Effects of Early Transition Metal Doping on Structure and Magnetic Properties of Fe_85.5B₁₃Cu_1.5 Nanocrystalline Alloy, columnId=null, journalTitle=Rare Metal Materials and Engineering, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The effects of adding 1at% early transition metals (M=Ti, V, Cr, Zr, Nb, Mo) on the melt-spun structure, crystallized microstructure, and magnetic properties of Fe_84.5B₁₃Cu_1.5M₁ alloys were investigated. The mechanisms of different M elements in regulating the alloy structure and magnetic performance were also discussed. Results show that except for the M=Zr alloy presenting fully amorphous state in the as-spun condition, other alloys all contain pre-existing α -Fe grains dispersed in amorphous matrix with average grain sizes (d_α-Fe) smaller than 10 nm and high numerical density (N_d). M doping can reduce both N_d and d_α-Fe of pre-existing α -Fe phases to varying degrees, with reduction effectiveness following the sequence: Cr<V<Mo<Nb<Ti<Zr. This trend positively correlates with the enhanced amorphous-forming ability derived from increased atomic size mismatch and negative mixing enthalpy induced by M elements. M doping significantly influences the α -Fe phase/amorphous-nanocrystalline composite structure and magnetic properties after heat treatment. Compared with Fe_85.5B₁₃Cu_1.5 alloy, alloys with M=V/Cr/Nb/Mo exhibit reduced average grain size (D_α-Fe) and coercivity (H_c) of α-Fe, while alloy counterparts with M=Ti/Zr show increased D_α-Fe and H_c. All doped alloys demonstrate slightly decreased saturation magnetic induction (B_s). Notably, the Mo-doped alloy achieves optimal nanocrystalline structure and soft magnetic properties, showing D_α-Fe=14.9 nm, H_c=8.3 A/m and B_s =1.84 T, which significantly outperforms the results as 17.9 nm, 22.1 A/m and 1.90 T of reference alloy, respectively. Mo doping attains optimized matching between N_d and d_α-Fe of pre-existing α-Fe grains in melt-spun alloys, which enhances the coordinated intergranular competitive growth effects during thermal crystallization. This mechanism effectively refines the nanocrystalline structure, reduces magnetocrystalline anisotropy, and consequently improves soft magnetic properties.

, authors=Yu Sun¹, Yanhui Li¹, Zhengwang Zhu², Li Jiang¹, Haifeng Zhang², Wei Zhang^{1, 2}, authorsList=Yu Sun, Yanhui Li, Zhengwang Zhu, Li Jiang, Haifeng Zhang, Wei Zhang, authorCompany=null, correspAuthors=Wei Zhang, authorNote=null, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1289282138327593354, articleId=1289282137862025608, tenantId=1146029695717560320, journalId=1287019424739590152, language=CN, title=前过渡族金属掺杂对Fe_85.5B₁₃Cu_1.5纳米晶合金结构和磁性能的影响, columnId=1289282137585205918, journalTitle=稀有金属材料与工程, columnName=材料科学, runingTitle=null, highlight=null, articleAbstract=

研究了添加1at%前过渡族金属（M=Ti, V, Cr, Zr, Nb, Mo）对Fe_84.5B₁₃Cu_1.5M₁合金快淬结构、晶化组织以及磁性能的影响规律，探讨了不同M影响合金结构及其磁性能的机理。结果表明，除M=Zr快淬合金为完全非晶态外，其余合金均有平均晶粒尺寸（d_α-Fe）小于10 nm的高数密度（N_d）的预存α-Fe晶粒弥散分布于非晶基体中；M掺杂可不同程度降低合金中预存α-Fe的N_d和d_α-Fe，降幅顺次为Cr<V<Mo<Nb<Ti<Zr，与M元素增大合金的原子尺寸错配度和负混合焓值而提升非晶形成能力的程度呈正相关。M掺杂对热处理后获得的α-Fe相/非晶纳米复相组织和磁性能影响显著，相较于Fe_85.5B₁₃Cu_1.5，M=V/Cr/Nb/Mo合金的α-Fe平均晶粒尺寸（D_α-Fe）和矫顽力（H_c）降低，而M=Ti/Zr合金的D_α-Fe和H_c增加；掺杂合金的饱和磁感应强度（B_s）均略有减小；其中，M=Mo合金具有最佳的纳米晶组织和软磁性能，其D_α-Fe、H_c和B_s分别为14.9 nm、8.3 A/m和1.84 T，显著优于Fe_85.5B₁₃Cu_1.5合金的17.9 nm、22.1 A/m和1.90 T。掺杂Mo实现了快淬合金中预存α-Fe晶粒的N_d和d_α-Fe的优化匹配，增强了热处理晶化过程中的α-Fe晶间协调竞争生长效应，有效细化了纳米晶组织，因而降低磁晶各向异性，提高软磁性。

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孙毓，男，1998年生，硕士，大连理工大学材料科学与工程学院，辽宁 大连 116024，E-mail: 15940760152@163.com

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孙毓，男，1998年生，硕士，大连理工大学材料科学与工程学院，辽宁 大连 116024，E-mail: 15940760152@163.com

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