Article(id=1289282153808769611, tenantId=1146029695717560320, journalId=1287019424739590152, issueId=1289282136750539420, articleNumber=null, orderNo=null, doi=10.12442/j.issn.1002-185X.20250141, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1752076800000, receivedDateStr=2025-07-10, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1785318419172, onlineDateStr=2026-07-29, pubDate=1783612800000, pubDateStr=2026-07-10, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1785318419172, onlineIssueDateStr=2026-07-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1785318419172, creator=13701087609, updateTime=1785318419172, updator=13701087609, issue=Issue{id=1289282136750539420, tenantId=1146029695717560320, journalId=1287019424739590152, year='2026', volume='55', issue='7', pageStart='1701', pageEnd='1848', issueExtLink='null', onlineDate='null', pubDate='1783612800000', pubDateStr='2026-07-10', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=1, specialIssue=null, createTime=1785318415105, creator='13701087609', updateTime=1785389094930, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1289578589494555490, tenantId=1146029695717560320, journalId=1287019424739590152, issueId=1289282136750539420, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1289578589498749795, tenantId=1146029695717560320, journalId=1287019424739590152, issueId=1289282136750539420, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1833, endPage=1839, ext={EN=ArticleExt(id=1289282153963958860, articleId=1289282153808769611, tenantId=1146029695717560320, journalId=1287019424739590152, language=EN, title=Effect of Heat Treatment Process on Recrystallization of Directional-Solidified Superalloy 4777DS, columnId=null, journalTitle=Rare Metal Materials and Engineering, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The effects of different heat treatment processes, alloy states, and stress relief annealing processes on recrystallization defects in 4777DS superalloy were studied using SEM and EBSD. SEM observation shows that the γ' phase near the surface of the sandblasted sample undergoes deformation, changing from an initial butterfly shape to a long strip distribution on the alloy surface. The observation of recrystallization of the alloy after insulation at different heat treatment temperatures shows that the temperature at which recrystallization occurs is 1055 ℃. When the heat treatment temperature is higher than the dissolution temperature of the γ' phase, recrystallization presents an equiaxed morphology, while when the heat treatment temperature is lower than the dissolution temperature of the γ' phase, it presents a cellular recrystallization morphology. With the prolongation of heat treatment time, the proportion of large angle grain boundaries decreases, and the resulting annealing twins help to reduce distortion energy. A comparison of recrystallization behavior under different initial alloy states reveals that the as-cast alloy exhibits the highest tendency for recrystallization. In line with practical engineering requirements, a shorter annealing time can effectively reduce the recrystallization degree of alloys.

, authors=Qiongyuan Zhang1, 2, 4, Ziyue Zhang3, Atao Yang1, 4, Mengxue Lv3, Qungong He1, 4, Zhihao Yao3, Haiyang Wang1, 4, Jianxin Dong3, authorsList=Qiongyuan Zhang, Ziyue Zhang, Atao Yang, Mengxue Lv, Qungong He, Zhihao Yao, Haiyang Wang, Jianxin Dong, authorCompany=null, correspAuthors=Zhihao Yao, authorNote=null, correspAuthorsNote=
Yao Zhihao, Ph. D., Professor, School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, P. R. China, Tel: 0086-10-62332884, E-mail:
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采用SEM、EBSD研究了不同热处理工艺、不同合金状态以及去应力退火工艺对4777DS合金再结晶缺陷的影响。合金不同热处理温度下保温后观察再结晶的情况表明:合金发生再结晶的温度为1055 ℃,热处理温度高于γ'相溶解温度时,再结晶呈现等轴再结晶形貌,而低于γ'相溶解温度时则呈现胞状再结晶形貌。随着热处理时间的延长,大角度晶界占比减少,产生的退火孪晶有助于降低畸变能。对比不同合金初始状态发生再结晶的情况可以发现,铸态合金发生再结晶的倾向最大,结合工程实际,发现较短时间的退火可有效地降低合金再结晶的情况。

, authors=张琼元1, 2, 4, 张子越3, 杨啊涛1, 4, 吕梦雪3, 贺群功1, 4, 姚志浩3, 王海洋1, 4, 董建新3, authorsList=张琼元, 张子越, 杨啊涛, 吕梦雪, 贺群功, 姚志浩, 王海洋, 董建新, authorCompany=null, correspAuthors=姚志浩, authorNote=

张琼元,男,1987年生,硕士,高级工程师,清洁高效透平动力装备全国重点实验室,四川 德阳 618000,E-mail:

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张琼元,男,1987年生,硕士,高级工程师,清洁高效透平动力装备全国重点实验室,四川 德阳 618000,E-mail:

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热处理工艺对定向凝固高温合金4777DS再结晶的影响
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张琼元 1, 2, 4 , 张子越 3 , 杨啊涛 1, 4 , 吕梦雪 3 , 贺群功 1, 4 , 姚志浩 3 , 王海洋 1, 4 , 董建新 3
稀有金属材料与工程 | 材料科学 2026,55(7): 1833-1839
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稀有金属材料与工程 |材料科学 2026 , 55 (7) : 1833 -1839
热处理工艺对定向凝固高温合金4777DS再结晶的影响
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张琼元1, 2, 4 , 张子越3, 杨啊涛1, 4, 吕梦雪3, 贺群功1, 4, 姚志浩3 , 王海洋1, 4, 董建新3
作者信息
  • 1.清洁高效透平动力装备全国重点实验室,四川 德阳 618000
  • 2.清华大学 材料学院,北京 100084
  • 3.北京科技大学 材料科学与工程学院,北京 100083
  • 4.东方电气集团东方汽轮机有限公司,四川 德阳 618000
作者简介:

张琼元,男,1987年生,硕士,高级工程师,清洁高效透平动力装备全国重点实验室,四川 德阳 618000,E-mail:

Effect of Heat Treatment Process on Recrystallization of Directional-Solidified Superalloy 4777DS
Qiongyuan Zhang1, 2, 4 , Ziyue Zhang3, Atao Yang1, 4, Mengxue Lv3, Qungong He1, 4, Zhihao Yao3 , Haiyang Wang1, 4, Jianxin Dong3
Affiliations
  • 1.State Key Laboratory of Clean and Efficient Turbomachinery Power Equipment, Deyang 618000, China
  • 2.School of Materials Sciences and Engineering, Tsinghua University, Beijing 100084, China
  • 3.School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China
  • 4.Dongfang Electric Corporation Dongfang Turbine Co., Ltd, Deyang 618000, China
出版时间: 2026-07-10 doi: 10.12442/j.issn.1002-185X.20250141
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采用SEM、EBSD研究了不同热处理工艺、不同合金状态以及去应力退火工艺对4777DS合金再结晶缺陷的影响。合金不同热处理温度下保温后观察再结晶的情况表明:合金发生再结晶的温度为1055 ℃,热处理温度高于γ'相溶解温度时,再结晶呈现等轴再结晶形貌,而低于γ'相溶解温度时则呈现胞状再结晶形貌。随着热处理时间的延长,大角度晶界占比减少,产生的退火孪晶有助于降低畸变能。对比不同合金初始状态发生再结晶的情况可以发现,铸态合金发生再结晶的倾向最大,结合工程实际,发现较短时间的退火可有效地降低合金再结晶的情况。

定向凝固  /  高温合金  /  再结晶  /  热处理  /  合金状态

The effects of different heat treatment processes, alloy states, and stress relief annealing processes on recrystallization defects in 4777DS superalloy were studied using SEM and EBSD. SEM observation shows that the γ' phase near the surface of the sandblasted sample undergoes deformation, changing from an initial butterfly shape to a long strip distribution on the alloy surface. The observation of recrystallization of the alloy after insulation at different heat treatment temperatures shows that the temperature at which recrystallization occurs is 1055 ℃. When the heat treatment temperature is higher than the dissolution temperature of the γ' phase, recrystallization presents an equiaxed morphology, while when the heat treatment temperature is lower than the dissolution temperature of the γ' phase, it presents a cellular recrystallization morphology. With the prolongation of heat treatment time, the proportion of large angle grain boundaries decreases, and the resulting annealing twins help to reduce distortion energy. A comparison of recrystallization behavior under different initial alloy states reveals that the as-cast alloy exhibits the highest tendency for recrystallization. In line with practical engineering requirements, a shorter annealing time can effectively reduce the recrystallization degree of alloys.

directional solidification  /  superalloy  /  recrystallization  /  heat treatment  /  alloy state
张琼元, 张子越, 杨啊涛, 吕梦雪, 贺群功, 姚志浩, 王海洋, 董建新. 热处理工艺对定向凝固高温合金4777DS再结晶的影响. 稀有金属材料与工程, 2026 , 55 (7) : 1833 -1839 . DOI: 10.12442/j.issn.1002-185X.20250141
Qiongyuan Zhang, Ziyue Zhang, Atao Yang, Mengxue Lv, Qungong He, Zhihao Yao, Haiyang Wang, Jianxin Dong. Effect of Heat Treatment Process on Recrystallization of Directional-Solidified Superalloy 4777DS[J]. Rare Metal Materials and Engineering, 2026 , 55 (7) : 1833 -1839 . DOI: 10.12442/j.issn.1002-185X.20250141
  • 清洁高效透平动力装备全国重点实验室开放课题(DEC8300CG202320365EE280525)
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doi: 10.12442/j.issn.1002-185X.20250141
  • 接收时间:2025-07-10
  • 首发时间:2026-07-29
  • 出版时间:2026-07-10
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  • 收稿日期:2025-07-10
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清洁高效透平动力装备全国重点实验室开放课题(DEC8300CG202320365EE280525)
作者信息
    1.清洁高效透平动力装备全国重点实验室,四川 德阳 618000
    2.清华大学 材料学院,北京 100084
    3.北京科技大学 材料科学与工程学院,北京 100083
    4.东方电气集团东方汽轮机有限公司,四川 德阳 618000

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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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