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In the paper, the tests of dissolved filtration residue rate and detecting content of naphthalene are designed, key steps of detection are proposed through analyzing charateristics of tar as well as N, N-dimethylacetamide and tetrahydrofuran are determined to select as the solvent for dissolving tar. The temperature of chromatographic column adopts the programmed temperature method and quantification for components of sample is with external standard method.

, authors=Xin Jiang1, Xiao-jiong Li1, Li-na Zhang2, authorsList=Xin Jiang, Xiao-jiong Li, Li-na Zhang, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319244167344140613, articleId=1319244166496891203, tenantId=1146029695717560320, journalId=1185652524569653253, language=CN, title=气相色谱法检测煤焦油中联苯、苊及芴的含量, columnId=1185882040642716431, journalTitle=包钢科技, columnName=其他, runingTitle=null, highlight=null, articleAbstract=

文章通过焦油特性分析,提出检测的关键步骤,设计溶解过滤残渣率试验及萘含量检测试验,确定选用N,N-二甲基乙酰胺和四氢呋喃作为焦油溶解的溶剂。色谱柱温度采用程序升温法,以外标法对试样组分定量。

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江鑫(1975-),男,河北省博野县人,工程师,现从事焦化炼焦配煤及检验技术研究工作。

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江鑫(1975-),男,河北省博野县人,工程师,现从事焦化炼焦配煤及检验技术研究工作。

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江鑫(1975-),男,河北省博野县人,工程师,现从事焦化炼焦配煤及检验技术研究工作。

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气相色谱法检测煤焦油中联苯、苊及芴的含量
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江鑫 1 , 李晓炅 1 , 张利娜 2
包钢科技 | 其他 2021,47(6): 91-95
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包钢科技 |其他 2021 , 47 (6) : 91 -95
气相色谱法检测煤焦油中联苯、苊及芴的含量
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江鑫1, 李晓炅1, 张利娜2
作者信息
  • 1.内蒙古包钢钢联股份有限公司技术中心,内蒙古 包头 014010
  • 2.内蒙古包钢钢联股份有限公司煤焦化工分公司,内蒙古 包头 014010
作者简介:

江鑫(1975-),男,河北省博野县人,工程师,现从事焦化炼焦配煤及检验技术研究工作。

Detection for Content of Biphenyl, Acenaphthene and Fluorene in Coal Tar with Gas Chromatography
Xin Jiang1, Xiao-jiong Li1, Li-na Zhang2
Affiliations
  • 1.Technical Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
  • 2.Coke Chemical Engineering Branch Co. of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
出版时间: 2021-12-25 doi: 10.13647/j.cnki.btgkj.2021.06.008
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文章通过焦油特性分析,提出检测的关键步骤,设计溶解过滤残渣率试验及萘含量检测试验,确定选用N,N-二甲基乙酰胺和四氢呋喃作为焦油溶解的溶剂。色谱柱温度采用程序升温法,以外标法对试样组分定量。

焦油  /  联苯、苊、芴含量  /  气相色谱法

In the paper, the tests of dissolved filtration residue rate and detecting content of naphthalene are designed, key steps of detection are proposed through analyzing charateristics of tar as well as N, N-dimethylacetamide and tetrahydrofuran are determined to select as the solvent for dissolving tar. The temperature of chromatographic column adopts the programmed temperature method and quantification for components of sample is with external standard method.

tar  /  content of biphenyl, acenaphthene and fluorene  /  gas chromatography
江鑫, 李晓炅, 张利娜. 气相色谱法检测煤焦油中联苯、苊及芴的含量. 包钢科技, 2021 , 47 (6) : 91 -95 . DOI: 10.13647/j.cnki.btgkj.2021.06.008
Xin Jiang, Xiao-jiong Li, Li-na Zhang. Detection for Content of Biphenyl, Acenaphthene and Fluorene in Coal Tar with Gas Chromatography[J]. Science & Technology of Baotou Steel, 2021 , 47 (6) : 91 -95 . DOI: 10.13647/j.cnki.btgkj.2021.06.008

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doi: 10.13647/j.cnki.btgkj.2021.06.008
  • 接收时间:2021-06-23
  • 首发时间:2026-10-20
  • 出版时间:2021-12-25
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  • 收稿日期:2021-06-23
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    1.内蒙古包钢钢联股份有限公司技术中心,内蒙古 包头 014010
    2.内蒙古包钢钢联股份有限公司煤焦化工分公司,内蒙古 包头 014010
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
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Number of
species
占总种数比例
Percentage of
total species (%)
属
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Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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