Article(id=1319225503060439776, tenantId=1146029695717560320, journalId=1185652524569653253, issueId=1319225473155060024, articleNumber=null, orderNo=null, doi=10.13647/j.cnki.btgkj.2019.06.022, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1568563200000, receivedDateStr=2019-09-16, revisedDate=null, revisedDateStr=null, acceptedDate=null, acceptedDateStr=null, onlineDate=1792457469953, onlineDateStr=2026-10-20, pubDate=1571932800000, pubDateStr=2019-10-25, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1792457469953, onlineIssueDateStr=2026-10-20, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1792457469953, creator=13701087609, updateTime=1792457469953, updator=13701087609, issue=Issue{id=1319225473155060024, tenantId=1146029695717560320, journalId=1185652524569653253, year='2019', volume='45', issue='6', pageStart='1', pageEnd='98', issueExtLink='null', onlineDate='null', pubDate='1577203200000', pubDateStr='2019-12-25', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1792457462824, creator='13701087609', updateTime=1792734666403, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1320388149310771859, tenantId=1146029695717560320, journalId=1185652524569653253, issueId=1319225473155060024, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1320388149310771860, tenantId=1146029695717560320, journalId=1185652524569653253, issueId=1319225473155060024, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=91, endPage=94, ext={EN=ArticleExt(id=1319225504796881634, articleId=1319225503060439776, tenantId=1146029695717560320, journalId=1185652524569653253, language=EN, title=Determination of Lanthanum, Cerium, Praseodymium, Neodymium and Samarium in Steel with Inductively Coupled Plasma Mass Spectrum, columnId=1187102804364640261, journalTitle=Science & Technology of Baotou Steel, columnName=Others, runingTitle=null, highlight=null, articleAbstract=

In the paper, the dissolution methods of such samples as steel and alloy are studied. Dissolve the samples with hydrochloric acid and nitric acid as well as the optimum instrument conditions of inductively coupled plasma mass spectrum (ICP-MS), select the spectral lines of elements to be tested with high sensitivity and fewer interferences as the analytical lines. The matrix matching is used to eliminate the influences of matrix effect in calibration curve so that the contents of lanthanum, cerium, praseodymium, neodymium and samarium in steel and alloys can be determined with the inductively coupled plasma source mass spectrometer.

, authors=Yan-qiu Wang1, 2, Jian-jun Zhang1, Gang-yao Liu1, authorsList=Yan-qiu Wang, Jian-jun Zhang, Gang-yao Liu, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1319225505992258276, articleId=1319225503060439776, tenantId=1146029695717560320, journalId=1185652524569653253, language=CN, title=等离子体质谱法测定钢中镧、铈、镨、钕、钐, columnId=1185882040642716431, journalTitle=包钢科技, columnName=其他, runingTitle=null, highlight=null, articleAbstract=

文章研究了钢铁及合金等试样的溶解方法,采用盐酸、硝酸溶解样品,在最佳化的ICP-MS仪器条件下,选择待测元素灵敏度高、干扰少的谱线为分析线,校准曲线采用了基体匹配消除基体效应影响,实现了采用电感耦合等离子体质谱仪测定钢铁及合金中镧、铈、镨、钕、钐元素含量。

, authors=王宴秋1, 2, 张建军1, 刘钢耀1, authorsList=王宴秋, 张建军, 刘钢耀, authorCompany=null, correspAuthors=null, authorNote=

王宴秋(1979-),男,内蒙古包头市人,高级工程师,现从事冶金分析工作。

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王宴秋(1979-),男,内蒙古包头市人,高级工程师,现从事冶金分析工作。

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等离子体质谱法测定钢中镧、铈、镨、钕、钐
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王宴秋 1, 2 , 张建军 1 , 刘钢耀 1
包钢科技 | 其他 2019,45(6): 91-94
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包钢科技 |其他 2019 , 45 (6) : 91 -94
等离子体质谱法测定钢中镧、铈、镨、钕、钐
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王宴秋1, 2, 张建军1, 刘钢耀1
作者信息
  • 1.内蒙古包钢钢联股份有限公司技术中心,内蒙古 包头 014010
  • 2.内蒙古自治区稀土钢产品研发企业重点实验室,内蒙古 包头 014010
作者简介:

王宴秋(1979-),男,内蒙古包头市人,高级工程师,现从事冶金分析工作。

Determination of Lanthanum, Cerium, Praseodymium, Neodymium and Samarium in Steel with Inductively Coupled Plasma Mass Spectrum
Yan-qiu Wang1, 2, Jian-jun Zhang1, Gang-yao Liu1
Affiliations
  • 1.Technical Center of Inner Mongolia Baotou Steel Union Co., Ltd., Baotou 014010, Inner Mongolia Autonomous Region, China
  • 2.Inner Mongolia Enterprise Key Laboratory of Rare Earth Steel Products Research & Development, Baotou 014010, Inner Mongolia Autonomous Region, China
出版时间: 2019-10-25 doi: 10.13647/j.cnki.btgkj.2019.06.022
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文章研究了钢铁及合金等试样的溶解方法,采用盐酸、硝酸溶解样品,在最佳化的ICP-MS仪器条件下,选择待测元素灵敏度高、干扰少的谱线为分析线,校准曲线采用了基体匹配消除基体效应影响,实现了采用电感耦合等离子体质谱仪测定钢铁及合金中镧、铈、镨、钕、钐元素含量。

钢铁及合金  /  等离子体质谱  /  稀土

In the paper, the dissolution methods of such samples as steel and alloy are studied. Dissolve the samples with hydrochloric acid and nitric acid as well as the optimum instrument conditions of inductively coupled plasma mass spectrum (ICP-MS), select the spectral lines of elements to be tested with high sensitivity and fewer interferences as the analytical lines. The matrix matching is used to eliminate the influences of matrix effect in calibration curve so that the contents of lanthanum, cerium, praseodymium, neodymium and samarium in steel and alloys can be determined with the inductively coupled plasma source mass spectrometer.

steel and alloys  /  inductively coupled plasma mass spectrum  /  rare earth
王宴秋, 张建军, 刘钢耀. 等离子体质谱法测定钢中镧、铈、镨、钕、钐. 包钢科技, 2019 , 45 (6) : 91 -94 . DOI: 10.13647/j.cnki.btgkj.2019.06.022
Yan-qiu Wang, Jian-jun Zhang, Gang-yao Liu. Determination of Lanthanum, Cerium, Praseodymium, Neodymium and Samarium in Steel with Inductively Coupled Plasma Mass Spectrum[J]. Science & Technology of Baotou Steel, 2019 , 45 (6) : 91 -94 . DOI: 10.13647/j.cnki.btgkj.2019.06.022

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doi: 10.13647/j.cnki.btgkj.2019.06.022
  • 接收时间:2019-09-16
  • 首发时间:2026-10-20
  • 出版时间:2019-10-25
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  • 收稿日期:2019-09-16
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    1.内蒙古包钢钢联股份有限公司技术中心,内蒙古 包头 014010
    2.内蒙古自治区稀土钢产品研发企业重点实验室,内蒙古 包头 014010
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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