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Methyl orange （MO） is a typical water-soluble azo organic dye. It is commonly used as an acid-base indicator in basic experiments and as a common organic dye in industrial production. It has strong polluting effects on water bodies. If azo dyes are accidentally ingested， the azo bond is cleaved by azoreductase， generating highly toxic aromatic amines that pose potential carcinogenic risks. Ionic covalent organic frameworks （ICOFs） are novel materials derived from covalent organic frameworks， featuring charged structures on their frameworks and pores. ICOFs exhibit excellent adsorption performance in aqueous solutions. Their high surface area and abundant porous channels facilitate rapid diffusion of pollutants into the inner structure， enabling effective pollutant adsorption. Eggplant is a sustainable biomass material with regular vertical macropores， which can be used as a substrate. This experiment employed an in-situ solvothermal method to prepare a highly efficient adsorbent monolithic material of eggplant composite aerogel （EP@PDA-TGDha COF）. It is applied to organic dye wastewater treatment. Developing this experiment as an undergraduate teaching module of “I love the laboratory” helps cultivate and enhance students’ abilities in sample pretreatment， material synthesis， structural and property characterization， and practical sample analysis. Students enter the research group offline， experience the academic atmosphere， keep abreast of cutting-edge research， taking the crucial first step in their academic journey. Through the “I Love the Lab” research training program， students significantly enhance their professional knowledge， experimental skills， and research-oriented thinking abilities. It also fosters students’ environmental protection awareness and enables them to apply their knowledge and skills to environmental conservation.

, authors=Yunmeng LI, Hongyi LI, Dongxiao CAO, Anna TANG^*, Deming KONG, authorsList=Yunmeng LI, Hongyi LI, Dongxiao CAO, Anna TANG, Deming KONG, authorCompany=null, correspAuthors=Anna TANG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1321834264681890162, articleId=1321834262421160283, tenantId=1146029695717560320, journalId=1283840372199657495, language=CN, title=“我爱实验室”科研训练：一种阳离子型共价有机框架气凝胶用于有机染料去除, columnId=1284557520232493975, journalTitle=色谱, columnName=教学研究, runingTitle=null, highlight=null, articleAbstract=

甲基橙（MO）是一种典型的水溶性偶氮类有机染料。在基础实验中常被用作酸碱指示剂，在工业生产中是一种常见的有机染料，对水体具有强污染性。如果不慎食用偶氮染料，偶氮键被体内偶氮还原酶裂解，生成的芳香胺毒性大且有致癌风险。离子型共价有机框架（ICOFs）是共价有机框架（COFs）材料的框架和孔道上带有电荷的新型材料。ICOFs在水溶液中展现出良好的吸附性能，其高比表面积和丰富的多孔通道有利于污染物快速扩散到内层结构中，能有效吸附污染物。将具有规则的垂直大孔的绿色物质茄子作为基质，通过原位生长法制备出一种对MO高效吸附的阳离子型共价有机框架茄子复合气凝胶（EP@PDA-TGDha COF），并将其应用于有机染料污水处理中。将该实验开发为本科生“我爱实验室”科研训练实验，有助于培养和提升学生在样品前处理材料合成、材料结构和性质表征及实际样品分析方面的实验技能和独立分析问题、解决问题的能力。学生通过线下接触优秀课题组，感受科研氛围，了解学术前沿，跨出学术道路关键的第一步。通过“我爱实验室”科研训练，学生的专业知识储备、实验技能及科研思维能力均得到大幅提高。同时将思政元素有机融入科研训练中，培养学生的环境保护意识。

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Angew Chem Int Ed， 2020， 59： 8713, articleTitle=null, refAbstract=null)], funds=null, companyList=[AuthorCompany(id=1321834264933548403, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, xref=1, ext=[AuthorCompanyExt(id=1321834264950325620, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, companyId=1321834264933548403, language=EN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=¹Research Center for Analytical Sciences， Tianjin Key Laboratory of Biosensing and Molecular Recognition， National Demonstration Center for Experimental Chemistry Education， College of Chemistry， Nankai University， Tianjin 300071， China), AuthorCompanyExt(id=1321834264962908533, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, companyId=1321834264933548403, language=CN, country=null, province=null, city=null, postcode=null, companyName=null, departmentName=null, remark=¹南开大学化学学院， 分析科学研究中心， 天津市生物传感与分子识别重点实验室， 化学国家级实验教学示范中心， 天津 300071)])], figs=[ArticleFig(id=1321834268439986583, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=EN, label=Fig.1, caption=Synthesis of triaminoguanidine-dihydroxyterephthalaldehyde covalent organic framework （TGDha COF）, figureFileSmall=An3PZ6nSJMf+aaT9fyyO6A==, figureFileBig=UYYJb1HMv9WC6dvFMYFUBg==, tableContent=null), ArticleFig(id=1321834268570010008, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=CN, label=图1, caption=TGDha COF材料的合成反应

TGCl： triaminoguanidine hydrochloride； 2，5-Dha： 2，5-dihydroxyterephthalaldehyde.

, figureFileSmall=An3PZ6nSJMf+aaT9fyyO6A==, figureFileBig=UYYJb1HMv9WC6dvFMYFUBg==, tableContent=null), ArticleFig(id=1321834269027189145, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=EN, label=Fig.2, caption=（a） Infrared spectra of 2，5-Dha， TGCl， EP， EP@PDA， TGDha COF and EP@PDA-TGDha COF； （b） ¹³C NMR spectrum of TGDha COF； （c） PXRD patterns of EP， EP@PDA， TGDha COF， and EP@PDA-TGDha COF； SEM images of （d， e） EP and （f） TGDha COF powder， and （g） EP@PDA-TGDha COF, figureFileSmall=m/z9n/CoJXPhr4FiFbqqXw==, figureFileBig=9W2OXBBpcsHqo/kJms7IHA==, tableContent=null), ArticleFig(id=1321834269220127130, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=CN, label=图2, caption=（a）2，5-Dha、TGCl、EP、EP@PDA、TGDha COF和EP@PDA-TGDha COF的红外光谱图；（b）TGDha COF的¹³C核磁共振谱图；（c）EP、EP@PDA、TGDha COF和EP@PDA-TGDha COF的PXRD图；（d，e）EP、（f）TGDha COF粉末和（g）EP@PDA-TGDha COF的扫描电镜图

EP： eggplant； PDA： polydopamine； EP@PDA： PDA-modified eggplant aerogel； EP@PDA-TGDha COF： final hierarchical composite aerogel； NMR： nuclear magnetic resonance； PXRD： powder X-ray diffraction； SEM： scanning electron microscopy.

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caption=Contact angles of water of EP， EP@PDA， TGDha COF， EP@PDA-TGDha COF at room temperature, figureFileSmall=2FfwIXLRkgf7b4RdM4+7Sw==, figureFileBig=C7L4rJB1VvVhcWPCCI/LZw==, tableContent=null), ArticleFig(id=1321834269979296158, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=CN, label=图4, caption=EP、EP@PDA、TGDha COF和EP@PDA-TGDha COF在室温下的水接触角, figureFileSmall=2FfwIXLRkgf7b4RdM4+7Sw==, figureFileBig=C7L4rJB1VvVhcWPCCI/LZw==, tableContent=null), ArticleFig(id=1321834270113513887, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=EN, label=Fig.5, caption=（a） Infrared spectra and （b） PXRD patterns of the untreated EP@PDA-TGDha COF and the EP@PDA-TGDha COF soaked in HCl， NaOH and N，N-dimethylformamide （DMF） for three days， respectively, figureFileSmall=9cAnN3C3JaeFRaOwR3UScA==, figureFileBig=dL0UMaX1L11MjjDMRDACRA==, tableContent=null), ArticleFig(id=1321834270319034784, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=CN, label=图5, caption=未处理过和分别用HCl、NaOH溶液和DMF浸泡3天的EP@PDA-TGDha COF的（a）红外光谱图和（b）PXRD图, figureFileSmall=9cAnN3C3JaeFRaOwR3UScA==, figureFileBig=dL0UMaX1L11MjjDMRDACRA==, tableContent=null), ArticleFig(id=1321834270470029729, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=EN, label=Fig.6, caption=Rremoval rates of methyl orange （MO） with EP@PDA-TGDha COF under different pH conditions, figureFileSmall=4JURYWyXj/UDm3Ta7UySuA==, figureFileBig=b1nipZE1pITspPJyXE4J5A==, tableContent=null), ArticleFig(id=1321834270650384802, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=CN, label=图6, caption=不同pH条件下EP@PDA-TGDha COF对甲基橙的去除率, figureFileSmall=4JURYWyXj/UDm3Ta7UySuA==, figureFileBig=b1nipZE1pITspPJyXE4J5A==, tableContent=null), ArticleFig(id=1321834270834934179, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=EN, label=Fig.7, caption=（a） Langmuir and （b） Freundlich isotherm adsorption models, figureFileSmall=cUOs+eaD5ToaVdIsEni03A==, figureFileBig=IcWpIX5golpxERjyWri3Iw==, tableContent=null), ArticleFig(id=1321834270990123428, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=CN, label=图7, caption=（a）Langmuir和（b）Freundlich等温吸附模型, figureFileSmall=cUOs+eaD5ToaVdIsEni03A==, figureFileBig=IcWpIX5golpxERjyWri3Iw==, tableContent=null), ArticleFig(id=1321834271124341157, tenantId=1146029695717560320, journalId=1283840372199657495, articleId=1321834262421160283, language=EN, label=Fig.8, caption=（a） Pseudo-first-order and （b） pseudo-second-order kinetic models of the adsorption process of MO by EP@PDA-TGDha COF, figureFileSmall=xXJWDBq574mxULPXdHE1rw==, figureFileBig=Ocm/cMKJ+EsBwMeOZy73Ww==, tableContent=null), ArticleFig(id=1321834271283724710, tenantId=1146029695717560320, 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