Article(id=1236340107591087092, tenantId=1146029695717560320, journalId=1235980609244409860, issueId=1236340101991691008, articleNumber=null, orderNo=null, doi=10.3969/j.issn.1000-2561.2023.03.022, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1656950400000, receivedDateStr=2022-07-05, revisedDate=1661875200000, revisedDateStr=2022-08-31, acceptedDate=null, acceptedDateStr=null, onlineDate=1772696051738, onlineDateStr=2026-03-05, pubDate=1679673600000, pubDateStr=2023-03-25, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1772696051738, onlineIssueDateStr=2026-03-05, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1772696051738, creator=13701087609, updateTime=1772696051738, updator=13701087609, issue=Issue{id=1236340101991691008, tenantId=1146029695717560320, journalId=1235980609244409860, year='2023', volume='44', issue='3', pageStart='447', pageEnd='660', issueExtLink='null', onlineDate='null', pubDate='null', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1772696050403, creator=13701087609, updateTime=1772696379070, updator=13701087609, preIssue=null, nextIssue=null, ext={EN=IssueExt(id=1236341480579715870, tenantId=1146029695717560320, journalId=1235980609244409860, issueId=1236340101991691008, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1236341480579715871, tenantId=1146029695717560320, journalId=1235980609244409860, issueId=1236340101991691008, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null}, startPage=647, endPage=660, ext={EN=ArticleExt(id=1236340107897270274, articleId=1236340107591087092, tenantId=1146029695717560320, journalId=1235980609244409860, language=EN, title=Effects of Different Wall Materials on the Microstructure and Thermal Stability of Green Coffee Oil Microcapsules, columnId=1236286112713470633, journalTitle=Chinese Journal of Tropical Crops, columnName=Post-harvest Treatment & Quality Safety, runingTitle=null, highlight=null, articleAbstract=

In this paper, three types of green coffee oil microcapsules were prepared by complex coacervation using the combination of gum arabic (GA) with soybean isolate protein (SPI), whey isolate protein (WPI) and sodium caseinate (SC) as wall materials, respectively. The turbidity, infrared spectral characteristics, apparent morphology and fluorescence co-localization of the wall materials were analyzed by combining different characterization techniques; the encapsulation efficiency, morphology, particle size, structural characterization and thermal stability of the three green coffee oil microcapsules were compared. Gum arabic and different proteins formed complexes through electrostatic interactions, which can be used as a new wall material for encapsulating green coffee oil. Infrared spectral analysis showed that the three wall materials could encapsulate green coffee oil better. The encapsulation rate in a descending order was SPIGA-GCO (69.26%), SCGA-GCO (58.69%), WPIGA-GCO (52.57%). The microstructure of green coffee oil microcapsules had a flat surface without obvious cracks, among which the oil droplets were more uniformly distributed in SPIGA-GCO. DSC analysis showed that the thermal denaturation temperature of microcapsules was higher (103.93-108.33 ℃), with good thermal stability. The results showed that the performance of SPIGA-GCO microcapsules was significantly better than the microcapsule products prepared from the other two wall materials. This study would provide technical support for the development of stable and effective green coffee oil microencapsulated products, and also provide a theoretical basis for the high value utilization of green coffee oil.

, correspAuthors=Zhenzhen ZHANG, Wenjiang DONG, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, authorCompany=null, fund=null, authors=null, authorsList=Jingyi MU, Faguang HU, Zhenzhen ZHANG, Wenjiang DONG, Ya'nan LI, Xiaofei BI, Rongsuo HU, Xiao'ai CHEN), CN=ArticleExt(id=1236340108320894998, articleId=1236340107591087092, tenantId=1146029695717560320, journalId=1235980609244409860, language=CN, title=不同壁材对绿咖啡油微胶囊微观结构及其热稳定性的影响, columnId=1236286112877048492, journalTitle=热带作物学报, columnName=采后处理与质量安全, runingTitle=null, highlight=null, articleAbstract=

分别以阿拉伯胶(gum arabic, GA)与大豆分离蛋白(soybean protein isolate, SPI)、乳清分离蛋白(whey protein isolate, WPI)和酪蛋白酸钠(sodium caseinate, SC)作为壁材,通过复合凝聚法制备3种绿咖啡油(green coffee oil, GCO)微胶囊。结合不同表征技术手段,对壁材的浊度、红外光谱特征、表观形貌以及荧光共定位进行分析;比较3种绿咖啡油微胶囊的包封效率、形貌、粒径、结构表征及热稳定性。结果表明,阿拉伯胶与不同蛋白之间通过静电相互作用形成复聚物,可作为包埋绿咖啡油的新型壁材;红外光谱分析表明,3种壁材均能较好地包埋绿咖啡油,包埋率从大到小依次为SPIGA-GCO(69.26%)>SCGA-GCO(58.69%)>WPIGA-GCO(52.57%);绿咖啡油微胶囊的微观结构表面平坦,无明显裂纹,其中SPIGA-GCO中油滴分布较为均匀;差示扫描热量法分析表明,微胶囊热变性温度较高(103.93~108.33 ℃),具有良好的热稳定性。研究结果表明,SPIGA-GCO微胶囊性能明显优于其他2种壁材制备的微胶囊产品。本研究为开发稳定有效的绿咖啡油微胶囊产品提供技术支撑,也为绿咖啡油的高值化利用提供理论依据。

, correspAuthors=张珍珍, 董文江, authorNote=null, correspAuthorsNote=
* 张珍珍(ZHANG Zhenzhen),E-mail:
董文江(DONG Wenjiang),E-mail:
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慕静怡(1998—),女,硕士研究生,研究方向:食品营养与安全。

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慕静怡(1998—),女,硕士研究生,研究方向:食品营养与安全。

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慕静怡(1998—),女,硕士研究生,研究方向:食品营养与安全。

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不同壁材对绿咖啡油微胶囊微观结构及其热稳定性的影响
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慕静怡 1, 2 , 胡发广 3 , 张珍珍 1, * , 董文江 2, 4, * , 李亚男 3 , 毕晓菲 3 , 胡荣锁 2, 4 , 陈小爱 2, 4
热带作物学报 | 采后处理与质量安全 2023,44(3): 647-660
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热带作物学报 | 采后处理与质量安全 2023, 44(3): 647-660
不同壁材对绿咖啡油微胶囊微观结构及其热稳定性的影响
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慕静怡1, 2, 胡发广3, 张珍珍1, * , 董文江2, 4, * , 李亚男3, 毕晓菲3, 胡荣锁2, 4, 陈小爱2, 4
作者信息
  • 1.新疆农业大学食品科学与药学学院,新疆乌鲁木齐 830053
  • 2.中国热带农业科学院香料饮料研究所,海南万宁 571533
  • 3.云南省农业科学院热带亚热带经济作物研究所,云南保山 678000
  • 4.海南省特色热带作物适宜性加工与品质控制重点实验室,海南万宁 571533
  • 慕静怡(1998—),女,硕士研究生,研究方向:食品营养与安全。

通讯作者:

* 张珍珍(ZHANG Zhenzhen),E-mail:
董文江(DONG Wenjiang),E-mail:
Effects of Different Wall Materials on the Microstructure and Thermal Stability of Green Coffee Oil Microcapsules
Jingyi MU1, 2, Faguang HU3, Zhenzhen ZHANG1, * , Wenjiang DONG2, 4, * , Ya'nan LI3, Xiaofei BI3, Rongsuo HU2, 4, Xiao'ai CHEN2, 4
Affiliations
  • 1.College of Food Science and Pharmacy, Xinjiang Agricultural University, Urumqi, Xinjiang 830053, China
  • 2.Spice and Beverage Research Institute, Chinese Academy of Tropical Agricultural Sciences, Wanning, Hainan 571533, China
  • 3.Institute of Tropical and Subtropical Economic Crops, Yunnan Academy of Agricultural Sciences, Baoshan, Yunnan 678000, China
  • 4.Key Laboratory of Processing Suitability and Quality Control of the Special Tropical Crops of Hainan Province, Wanning, Hainan 571533, China
出版时间: 2023-03-25 doi: 10.3969/j.issn.1000-2561.2023.03.022
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分别以阿拉伯胶(gum arabic, GA)与大豆分离蛋白(soybean protein isolate, SPI)、乳清分离蛋白(whey protein isolate, WPI)和酪蛋白酸钠(sodium caseinate, SC)作为壁材,通过复合凝聚法制备3种绿咖啡油(green coffee oil, GCO)微胶囊。结合不同表征技术手段,对壁材的浊度、红外光谱特征、表观形貌以及荧光共定位进行分析;比较3种绿咖啡油微胶囊的包封效率、形貌、粒径、结构表征及热稳定性。结果表明,阿拉伯胶与不同蛋白之间通过静电相互作用形成复聚物,可作为包埋绿咖啡油的新型壁材;红外光谱分析表明,3种壁材均能较好地包埋绿咖啡油,包埋率从大到小依次为SPIGA-GCO(69.26%)>SCGA-GCO(58.69%)>WPIGA-GCO(52.57%);绿咖啡油微胶囊的微观结构表面平坦,无明显裂纹,其中SPIGA-GCO中油滴分布较为均匀;差示扫描热量法分析表明,微胶囊热变性温度较高(103.93~108.33 ℃),具有良好的热稳定性。研究结果表明,SPIGA-GCO微胶囊性能明显优于其他2种壁材制备的微胶囊产品。本研究为开发稳定有效的绿咖啡油微胶囊产品提供技术支撑,也为绿咖啡油的高值化利用提供理论依据。

绿咖啡油  /  微胶囊  /  复合凝聚法  /  结构表征  /  热稳定性

In this paper, three types of green coffee oil microcapsules were prepared by complex coacervation using the combination of gum arabic (GA) with soybean isolate protein (SPI), whey isolate protein (WPI) and sodium caseinate (SC) as wall materials, respectively. The turbidity, infrared spectral characteristics, apparent morphology and fluorescence co-localization of the wall materials were analyzed by combining different characterization techniques; the encapsulation efficiency, morphology, particle size, structural characterization and thermal stability of the three green coffee oil microcapsules were compared. Gum arabic and different proteins formed complexes through electrostatic interactions, which can be used as a new wall material for encapsulating green coffee oil. Infrared spectral analysis showed that the three wall materials could encapsulate green coffee oil better. The encapsulation rate in a descending order was SPIGA-GCO (69.26%), SCGA-GCO (58.69%), WPIGA-GCO (52.57%). The microstructure of green coffee oil microcapsules had a flat surface without obvious cracks, among which the oil droplets were more uniformly distributed in SPIGA-GCO. DSC analysis showed that the thermal denaturation temperature of microcapsules was higher (103.93-108.33 ℃), with good thermal stability. The results showed that the performance of SPIGA-GCO microcapsules was significantly better than the microcapsule products prepared from the other two wall materials. This study would provide technical support for the development of stable and effective green coffee oil microencapsulated products, and also provide a theoretical basis for the high value utilization of green coffee oil.

green coffee oil  /  microcapsules  /  complex coacervation  /  structural characterization  /  thermal stability
慕静怡, 胡发广, 张珍珍, 董文江, 李亚男, 毕晓菲, 胡荣锁, 陈小爱. 不同壁材对绿咖啡油微胶囊微观结构及其热稳定性的影响. 热带作物学报, 2023 , 44 (3) : 647 -660 . DOI: 10.3969/j.issn.1000-2561.2023.03.022
Jingyi MU, Faguang HU, Zhenzhen ZHANG, Wenjiang DONG, Ya'nan LI, Xiaofei BI, Rongsuo HU, Xiao'ai CHEN. Effects of Different Wall Materials on the Microstructure and Thermal Stability of Green Coffee Oil Microcapsules[J]. Chinese Journal of Tropical Crops, 2023 , 44 (3) : 647 -660 . DOI: 10.3969/j.issn.1000-2561.2023.03.022
  • 海南省重点研发计划项目(ZDYF2021XDNY147)
  • 云南省重大科技专项计划项目(202202AE090002)
  • 中央级公益性科研院所基本业务费专项(1630142022010)
2023年第44卷第3期
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doi: 10.3969/j.issn.1000-2561.2023.03.022
  • 接收时间:2022-07-05
  • 首发时间:2026-03-05
  • 出版时间:2023-03-25
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出版历史
  • 收稿日期:2022-07-05
  • 修回日期:2022-08-31
基金
海南省重点研发计划项目(ZDYF2021XDNY147)
云南省重大科技专项计划项目(202202AE090002)
中央级公益性科研院所基本业务费专项(1630142022010)
作者信息
    1.新疆农业大学食品科学与药学学院,新疆乌鲁木齐 830053
    2.中国热带农业科学院香料饮料研究所,海南万宁 571533
    3.云南省农业科学院热带亚热带经济作物研究所,云南保山 678000
    4.海南省特色热带作物适宜性加工与品质控制重点实验室,海南万宁 571533

通讯作者:

* 张珍珍(ZHANG Zhenzhen),E-mail:
董文江(DONG Wenjiang),E-mail:
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2种不同金属材料的力学参数

Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)

Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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