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journalId=1319355259157577875, language=EN, title=Preparation of FOX-7 Nanosheets via PVP Induced Crystallization, columnId=null, journalTitle=Chinese Journal of Explosives & Propellants, columnName=null, runingTitle=null, highlight=null, articleAbstract=null, authors=null, authorsList=null, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1320429105993069068, articleId=1320429080395231746, tenantId=1146029695717560320, journalId=1319355259157577875, language=CN, title=PVP诱导结晶制备FOX-7纳米片, columnId=null, journalTitle=火炸药学报, columnName=null, runingTitle=null, highlight=null, articleAbstract=为了获得片层结构的1,1-二氨基-2,2-二硝基乙烯(FOX-7),以聚乙烯吡咯烷酮(PVP)为结晶诱导剂,通过溶剂-非溶剂法制备了FOX-7纳米片; 采用SEM、XRD、DSC对所制备样品的形貌、结构与热性能进行了表征,并对其机械感度进行了测试分析。结果表明,在不同含量的PVP的诱导下,FOX-7分子结晶向层状堆积方向生长,重结晶成不同横向尺寸和厚度的片状晶体; 当PVP的质量分数为1.5%时,所制备的FOX-7片状晶体的横向尺寸最大; 当PVP的质量分数为3%时,所制备的FOX-7片状晶体的厚度在200～300nm之间。PVP对FOX-7的吸附作用及两者之间氢键的形成对FOX-7纳米片的形成具有重要影响; 所制备的 FOX-7纳米片的表观分解放热焓随PVP含量的增加而逐渐提高,同时其热分解温度范围相比原料变窄,放热效率提高; 与原料相比,所制备的片层FOX-7的摩擦感度有较大幅度下降, FOX-7片状晶体的滑移降感效果较明显; 当PVP质量分数为1.5%时,所制备的FOX-7片层颗粒较完美,摩擦感度最低,为288N。, authors=null, authorsList=null, authorCompany=null, correspAuthors=null, authorNote=null, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, 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