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Article(id=1322944185963250049, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200921, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1608048000000, receivedDateStr=2020-12-16, revisedDate=1614873600000, revisedDateStr=2021-03-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1793344073048, onlineDateStr=2026-10-30, pubDate=1632067200000, pubDateStr=2021-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793344073048, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793344073048, creator=13701087609, updateTime=1793344073048, updator=13701087609, issue=Issue{id=1322942780003201932, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='9', pageStart='1785', pageEnd='2044', issueExtLink='null', onlineDate='null', pubDate='1632067200000', pubDateStr='2021-09-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343737841, creator='13701087609', updateTime=1793345873558, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951737916665918, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951737916665919, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2036, endPage=2044, ext={EN=ArticleExt(id=1322944188077179266, articleId=1322944185963250049, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of Nano-Carbon/MgAl2O4 Spinel Composite Powder on Properties of Low-carbon Al2O3-C Refractories, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

A nano-carbon/MgAl2O4 spinel composite powder was prepared with magnesia citrate and alumina via buried carbon-bed sintering. The nano-carbon/MgAl2O4 spinel composite powder was investigated by X-ray diffraction, field emission scanning electron microscopy and energy dispersive spectroscopy. The effect of composite powder amount on the physical properties, oxidation resistance, slag corrosion resistance and thermal shock resistance for low-carbon Al2O3-C refractories was investigated. The results show that carbon in the nano-carbon/MgAl2O4 spinel composite powder is equally distributed, and attached onto the spinel grain surface or mixed between the grains, leading to the composite powder having the corrosion resistance and thermal shock resistance for the low-carbon Al2O3-C refractories. Compared to the blank sample, the corrosion resistance of the sample with nano-carbon/MgAl2O4 spinel composite powder of 4.5% (in mass fraction) is increased by 71.3%, the thermal shock resistance is improved, and the residual strength retention rate is increased by 43.2%, thus indicating that the nano- carbon/MgAl2O4 spinel composite powder can improve the properties of low-carbon Al2O3-C refractories.

, authors=Guodan LI1, Donghai DING1, Guoqing XIAO1, Lihua LV2, Changkun LEI1, Jianjun CHEN1, authorsList=Guodan LI, Donghai DING, Guoqing XIAO, Lihua LV, Changkun LEI, Jianjun CHEN, authorCompany=null, correspAuthors=Guoqing XIAO, authorNote=

LI Guodan (1995-), female, Master candidate. E-mail:

, correspAuthorsNote=
XIAO Guoqing (1967-), male, Professor. E-mail:
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以柠檬酸镁和氧化铝为原料，采用埋碳烧结法合成纳米碳/镁铝尖晶石复合粉，并代替铝碳耐火材料中的部分石墨，通过X射线衍射仪、场发射扫描电子显微镜以及能谱分析仪表征纳米碳/镁铝尖晶石复合粉，研究了加入不同量的复合粉对铝碳耐火材料物理性能、抗氧化性、抗渣侵蚀性以及抗热震性的影响。结果表明：纳米碳/镁铝尖晶石复合粉中碳分布均匀，分散在尖晶石晶粒表面或者夹杂在晶粒之间，使得复合粉在铝碳耐火材料抗侵蚀性和抗热震性等方面有显著作用。与空白样品相比，加入4.5%（质量分数）纳米碳/镁铝尖晶石复合粉的样品抗渣侵蚀性能提高71.3%；且抗热震性能有所改善，残余强度保持率提高43.2%。表明纳米碳/镁铝尖晶石复合粉能提高低碳铝碳耐火材料的性能。

, authors=李国丹1, 丁冬海1, 肖国庆1, 吕李华2, 雷长坤1, 陈建军1, authorsList=李国丹, 丁冬海, 肖国庆, 吕李华, 雷长坤, 陈建军, authorCompany=null, correspAuthors=肖国庆, authorNote=

李国丹（1995—），女，硕士研究生。

, correspAuthorsNote=
肖国庆（1967—），男，教授。
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LI Guodan (1995-), female, Master candidate. E-mail:

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LI Guodan (1995-), female, Master candidate. E-mail:

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李国丹（1995—），女，硕士研究生。

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李国丹（1995—），女，硕士研究生。

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纳米碳/镁铝尖晶石复合粉对低碳铝碳耐火材料性能的影响
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李国丹 1 , 丁冬海 1 , 肖国庆 1 , 吕李华 2 , 雷长坤 1 , 陈建军 1
硅酸盐学报 | 研究论文 2021,49(9): 2036-2044
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硅酸盐学报 |研究论文 2021 , 49 (9) : 2036 -2044
纳米碳/镁铝尖晶石复合粉对低碳铝碳耐火材料性能的影响
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李国丹1 , 丁冬海1, 肖国庆1 , 吕李华2, 雷长坤1, 陈建军1
作者信息
  • 1．西安建筑科技大学材料科学与工程学院，西安 710055
  • 2．山西工程技术学院，山西 阳泉 045000
通讯作者:
肖国庆（1967—），男，教授。
作者简介:

李国丹（1995—），女，硕士研究生。

Effect of Nano-Carbon/MgAl2O4 Spinel Composite Powder on Properties of Low-carbon Al2O3-C Refractories
Guodan LI1 , Donghai DING1, Guoqing XIAO1 , Lihua LV2, Changkun LEI1, Jianjun CHEN1
Affiliations
  • 1.College of Materials Science and Engineering, Xi'an University of Architecture and Technology, Xi'an 710055, China
  • 2.Shanxi Institute of Technology, Yangquan 045000, Shanxi, China
    • Corresponding Author:
    XIAO Guoqing (1967-), male, Professor. E-mail:

    LI Guodan (1995-), female, Master candidate. E-mail:

出版时间: 2021-09-20 doi: 10.14062/j.issn.0454-5648.20200921
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以柠檬酸镁和氧化铝为原料，采用埋碳烧结法合成纳米碳/镁铝尖晶石复合粉，并代替铝碳耐火材料中的部分石墨，通过X射线衍射仪、场发射扫描电子显微镜以及能谱分析仪表征纳米碳/镁铝尖晶石复合粉，研究了加入不同量的复合粉对铝碳耐火材料物理性能、抗氧化性、抗渣侵蚀性以及抗热震性的影响。结果表明：纳米碳/镁铝尖晶石复合粉中碳分布均匀，分散在尖晶石晶粒表面或者夹杂在晶粒之间，使得复合粉在铝碳耐火材料抗侵蚀性和抗热震性等方面有显著作用。与空白样品相比，加入4.5%（质量分数）纳米碳/镁铝尖晶石复合粉的样品抗渣侵蚀性能提高71.3%；且抗热震性能有所改善，残余强度保持率提高43.2%。表明纳米碳/镁铝尖晶石复合粉能提高低碳铝碳耐火材料的性能。

铝碳耐火材料  /  纳米碳/镁铝尖晶石复合粉  /  抗热震性能

A nano-carbon/MgAl2O4 spinel composite powder was prepared with magnesia citrate and alumina via buried carbon-bed sintering. The nano-carbon/MgAl2O4 spinel composite powder was investigated by X-ray diffraction, field emission scanning electron microscopy and energy dispersive spectroscopy. The effect of composite powder amount on the physical properties, oxidation resistance, slag corrosion resistance and thermal shock resistance for low-carbon Al2O3-C refractories was investigated. The results show that carbon in the nano-carbon/MgAl2O4 spinel composite powder is equally distributed, and attached onto the spinel grain surface or mixed between the grains, leading to the composite powder having the corrosion resistance and thermal shock resistance for the low-carbon Al2O3-C refractories. Compared to the blank sample, the corrosion resistance of the sample with nano-carbon/MgAl2O4 spinel composite powder of 4.5% (in mass fraction) is increased by 71.3%, the thermal shock resistance is improved, and the residual strength retention rate is increased by 43.2%, thus indicating that the nano- carbon/MgAl2O4 spinel composite powder can improve the properties of low-carbon Al2O3-C refractories.

low-carbon aluminum carbon refractories  /  nano carbon/magnesium aluminum spinel composite powder  /  thermal shock resistance
李国丹, 丁冬海, 肖国庆, 吕李华, 雷长坤, 陈建军. 纳米碳/镁铝尖晶石复合粉对低碳铝碳耐火材料性能的影响. 硅酸盐学报, 2021 , 49 (9) : 2036 -2044 . DOI: 10.14062/j.issn.0454-5648.20200921
Guodan LI, Donghai DING, Guoqing XIAO, Lihua LV, Changkun LEI, Jianjun CHEN. Effect of Nano-Carbon/MgAl2O4 Spinel Composite Powder on Properties of Low-carbon Al2O3-C Refractories[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (9) : 2036 -2044 . DOI: 10.14062/j.issn.0454-5648.20200921
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  • 陕西省重点研发项目(2018ZDXM-GY-128)
  • 国家自然科学基金(51572212; 51772236)
  • 陕西省教育厅协同创新项目(Z20200170)
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2021年第49卷第9期
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doi: 10.14062/j.issn.0454-5648.20200921
  • 接收时间：2020-12-16
  • 首发时间：2026-10-30
  • 出版时间：2021-09-20
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  • 收稿日期：2020-12-16
  • 修回日期：2021-03-05
基金
陕西省重点研发项目(2018ZDXM-GY-128)
国家自然科学基金(51572212; 51772236)
陕西省教育厅协同创新项目(Z20200170)
作者信息
    1．西安建筑科技大学材料科学与工程学院，西安 710055
    2．山西工程技术学院，山西 阳泉 045000

通讯作者:

肖国庆（1967—），男，教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200921
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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