Article(id=1322943986758976182, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942627649303277, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200601, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1597507200000, receivedDateStr=2020-08-16, revisedDate=1600272000000, revisedDateStr=2020-09-17, acceptedDate=null, acceptedDateStr=null, onlineDate=1793344025554, onlineDateStr=2026-10-30, pubDate=1624118400000, pubDateStr=2021-06-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793344025554, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793344025554, creator=13701087609, updateTime=1793344025554, updator=13701087609, issue=Issue{id=1322942627649303277, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='6', pageStart='1033', pageEnd='1246', issueExtLink='null', onlineDate='null', pubDate='1624118400000', pubDateStr='2021-06-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343701517, creator='13701087609', updateTime=1793345989266, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322952223231181603, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942627649303277, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322952223231181604, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942627649303277, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1048, endPage=1055, ext={EN=ArticleExt(id=1322943987975324344, articleId=1322943986758976182, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Synthesis and Electrochemical Properties of Spinel Li
1.02Ni
0.05Mn
1.93O
4 Cathode Materials, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=
Li1.02Ni0.05Mn1.93O4(LNMO) cathode materials were synthesized via liquid flameless combustion at 500℃ for 1 h and subsequent calcination at 700℃ for 3, 6, 9 h and 12 h. The effect of calcination time on the structure, morphology, electrochemical and kinetic properties of the LNMO samples was investigated. The results show that all the samples synthesized have a spinel structure of LiMn2O4, and the particle size and crystallinity increase with the increase of calcination time. The LNMO-6 sample has a superior electrochemical performance (i.e., the first discharge specific capacity of 118.7 mA·h/g and the capacity retention rate of 87.0% after 200 cycles at 1 C). At high rates of 5 C and 10 C, the LNMO-6 sample still maintains capacity retention rates of 76.3% and 75.5% after 1 000 cycles. Based on the results by cyclic voltammetry and electrochemical impedance spectroscopy, the LNMO-6 sample has the maximum diffusion coefficient (i.e., 3.74×10-15 cm2/s) and the minimal apparent activation energy (i.e., 22.72 kJ/mol).
, authors=Qimei LIANG
1, 2, 3, Qing LIU
1, 2, 3, Junming GUO
1, 2, 3, Wei BAI
1, 2, 3, Mingwu XIANG
1, 2, 3, Xiaofang LIU
1, 2, 3, Hongli BAI
1, 2, 3, authorsList=Qimei LIANG, Qing LIU, Junming GUO, Wei BAI, Mingwu XIANG, Xiaofang LIU, Hongli BAI, authorCompany=null, correspAuthors=Junming GUO, authorNote=
, correspAuthorsNote=
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943990051504826, articleId=1322943986758976182, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=尖晶石型Li
1.02Ni
0.05Mn
1.93O
4正极材料的合成及电化学性能, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=
采用无焰燃烧法在500℃燃烧反应3 h并在700℃二次焙烧3、6、9 h和12 h合成了尖晶石型Li1.02Ni0.05Mn1.93O4（LNMO）正极材料，研究了焙烧时间对LNMO正极材料结构、形貌、电化学性能以及动力学性能的影响。制备的所有样品均具有LiMn2O4的尖晶石型结构，并且随着焙烧时间的延长，样品的颗粒尺寸逐渐增大，结晶性逐渐增强。焙烧时间为6 h样品（LNMO-6）展现出较为优异的电化学性能，在1 C，该样品的首次放电比容量为118.7 mA·h/g，经200次充放电循环后其容量保持率为87.0%，甚至在5 C和10 C高倍率下循环1 000次后仍具有76.3%和75.5%容量保持率。循环伏安和电化学阻抗测试结果表明：样品LNMO-6具有最大的Li+扩散系数（3.74×10-15 cm2/s）以及最低的表观活化能（22.72 kJ/mol）。
, authors=梁其梅
1, 2, 3, 刘清
1, 2, 3, 郭俊明
1, 2, 3, 白玮
1, 2, 3, 向明武
1, 2, 3, 刘晓芳
1, 2, 3, 白红丽
1, 2, 3, authorsList=梁其梅, 刘清, 郭俊明, 白玮, 向明武, 刘晓芳, 白红丽, authorCompany=null, correspAuthors=郭俊明, authorNote=
, correspAuthorsNote=
郭俊明（1962—），男，硕士，教授。
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1, 2, 3, address=
1.School of Chemistry and Environment, Kunming 650500, China
2.Yunnan Minzu University; National and Local Joint Engineering Research Center for Green Preparation Technology of Biobased Materials, Kunming 650500, China
3.Yunnan Provincial Higher Educational Key Laboratory of Green-chemical Materials, Kunming 650500, China, bio={"content":"
LIANG Qimei (1996-), female, Master candidate. E-mail: 3286049631@qq.com
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LIANG Qimei (1996-), female, Master candidate. E-mail: 3286049631@qq.com
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1, 2, 3, address=
1．云南民族大学化学与环境学院，昆明 650500
2．生物基材料绿色制备技术国家地方联合工程研究中心，昆明 650500
3．云南省高校绿色化学材料重点实验室，昆明 650500, bio={"content":"
梁其梅（1996—），女，硕士研究生。
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梁其梅（1996—），女，硕士研究生。
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1.School of Chemistry and Environment, Kunming 650500, China
2.Yunnan Minzu University; National and Local Joint Engineering Research Center for Green Preparation Technology of Biobased Materials, Kunming 650500, China
3.Yunnan Provincial Higher Educational Key Laboratory of Green-chemical Materials, Kunming 650500, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1322943995936113367, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322943986758976182, authorId=1322943995202110161, language=CN, stringName=刘清, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
1, 2, 3, address=
1．云南民族大学化学与环境学院，昆明 650500
2．生物基材料绿色制备技术国家地方联合工程研究中心，昆明 650500
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1, 2, 3, address=
1.School of Chemistry and Environment, Kunming 650500, China
2.Yunnan Minzu University; National and Local Joint Engineering Research Center for Green Preparation Technology of Biobased Materials, Kunming 650500, China
3.Yunnan Provincial Higher Educational Key Laboratory of Green-chemical Materials, Kunming 650500, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1322943996800139999, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322943986758976182, authorId=1322943996355543769, language=CN, stringName=郭俊明, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
1, 2, 3, address=
1．云南民族大学化学与环境学院，昆明 650500
2．生物基材料绿色制备技术国家地方联合工程研究中心，昆明 650500
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1, 2, 3, address=
1.School of Chemistry and Environment, Kunming 650500, China
2.Yunnan Minzu University; National and Local Joint Engineering Research Center for Green Preparation Technology of Biobased Materials, Kunming 650500, China
3.Yunnan Provincial Higher Educational Key Laboratory of Green-chemical Materials, Kunming 650500, China, bio=null, bioImg=null, bioContent=null, aboutCorrespAuthor=null), CN=AuthorExt(id=1322943998930846440, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322943986758976182, authorId=1322943996930163426, language=CN, stringName=白玮, firstName=null, middleName=null, lastName=null, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=
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