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Article(id=1322943452001993350, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200732, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1601049600000, receivedDateStr=2020-09-26, revisedDate=1605715200000, revisedDateStr=2020-11-19, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343898057, onlineDateStr=2026-10-30, pubDate=1618848000000, pubDateStr=2021-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343898057, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343898057, creator=13701087609, updateTime=1793343898057, updator=13701087609, issue=Issue{id=1322942545734546372, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='4', pageStart='605', pageEnd='806', issueExtLink='null', onlineDate='null', pubDate='1618848000000', pubDateStr='2021-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343681986, creator='13701087609', updateTime=1793345524324, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950273110508350, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950273110508351, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=633, endPage=638, ext={EN=ArticleExt(id=1322943454455661191, articleId=1322943452001993350, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Regulatory Effect of Oxygen Vacancy on Microstructure of La0.9Sr0.1TiO3+δ Layer Perovskite Ceramics, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The microstructure of layer perovskite La0.9Sr0.1TiO3+δ was investigated by high-resolution transmission electron microscopy and high angle annular dark field image analysis. The mechanism of oxygen vacancy on the lattice structure was revealed. Based on the results by X-ray diffraction, the oxygen-difficient environment effect on the lattice structure leads to the change of axial length and volume contraction in the material. The partial atomic plane rearrangement and dislocation caused by oxygen vacancy and continuous lattice distortion are identified based on high-resolution microscopic and Z-contrast atomic images, respectively. The effective regulation of oxygen vacancy defect shows a great significance on changing the microstructure of materials and further preparation of high-performance perovskite materials.

, authors=Yang ZHAO1, Jinpeng ZHU1, 2, Hailong WANG2, Gang SHAO2, Kaijun YANG2, Zhuang MA3, Lihong GAO3, Yongchun SHU1, Jilin HE1, 2, authorsList=Yang ZHAO, Jinpeng ZHU, Hailong WANG, Gang SHAO, Kaijun YANG, Zhuang MA, Lihong GAO, Yongchun SHU, Jilin HE, authorCompany=null, correspAuthors=Jinpeng ZHU, authorNote=

ZHAO Yang (1996-), male, Master candidate. E-mail:

, correspAuthorsNote=
ZHU Jinpeng (1989-), male, Ph.D., Associate Professor. E-mail:
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943457844658824, articleId=1322943452001993350, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=氧空位对La0.9Sr0.1TiO3+δ层状钙钛矿陶瓷微观结构的调控作用, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用高分辨透射电子显微镜（HR-TEM）与球差校正电镜高角环形暗场（HAADF）像研究了层状钙钛矿La0.9Sr0.1TiO3+δ（LST）的显微结构，揭示了该材料体系中存在的氧空位缺陷对晶格结构的作用机制。结果表明：材料晶格结构受缺氧环境的影响会引起LST晶胞a，b轴长度的缩短与c轴的相对伸长，在整体上表现为晶胞的体积收缩。基于高分辨显微像与Z衬度原子像的分析，能够识别由氧空位引发的部分原子面重排以及由连续晶格畸变所导致的位错现象。氧空位缺陷的有效调控将对优化材料微观结构，进一步制备高反射率钙钛矿材料具有重要意义。

, authors=赵阳1, 朱锦鹏1, 2, 王海龙2, 邵刚2, 杨凯军2, 马壮3, 高丽红3, 舒永春1, 何季麟1, 2, authorsList=赵阳, 朱锦鹏, 王海龙, 邵刚, 杨凯军, 马壮, 高丽红, 舒永春, 何季麟, authorCompany=null, correspAuthors=朱锦鹏, authorNote=

赵阳（1996—），男，硕士研究生。

, correspAuthorsNote=
朱锦鹏（1989—），男，博士，副教授。
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ZHAO Yang (1996-), male, Master candidate. E-mail:

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ZHAO Yang (1996-), male, Master candidate. E-mail:

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赵阳（1996—），男，硕士研究生。

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赵阳（1996—），男，硕士研究生。

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氧空位对La0.9Sr0.1TiO3+δ层状钙钛矿陶瓷微观结构的调控作用
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赵阳 1 , 朱锦鹏 1, 2 , 王海龙 2 , 邵刚 2 , 杨凯军 2 , 马壮 3 , 高丽红 3 , 舒永春 1 , 何季麟 1, 2
硅酸盐学报 | 2021,49(4): 633-638
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硅酸盐学报 | 2021 , 49 (4) : 633 -638
氧空位对La0.9Sr0.1TiO3+δ层状钙钛矿陶瓷微观结构的调控作用
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赵阳1 , 朱锦鹏1, 2 , 王海龙2, 邵刚2, 杨凯军2, 马壮3, 高丽红3, 舒永春1, 何季麟1, 2
作者信息
  • 1．郑州大学，河南省资源与材料工业技术研究院，郑州 450001
  • 2．郑州大学材料科学与工程学院，郑州 450001
  • 3．北京理工大学材料科学与工程学院，冲击环境材料技术重点实验室，北京 100081
通讯作者:
朱锦鹏（1989—），男，博士，副教授。
作者简介:

赵阳（1996—），男，硕士研究生。

Regulatory Effect of Oxygen Vacancy on Microstructure of La0.9Sr0.1TiO3+δ Layer Perovskite Ceramics
Yang ZHAO1 , Jinpeng ZHU1, 2 , Hailong WANG2, Gang SHAO2, Kaijun YANG2, Zhuang MA3, Lihong GAO3, Yongchun SHU1, Jilin HE1, 2
Affiliations
  • 1.Henan Province Industrial Technology Research Institute of Resources and Materials, Zhengzhou University, Zhengzhou 450001, China
  • 2.School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, Henan, China
  • 3.National Key Laboratory of Science and Technology on Materials under Shock and Impact, School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China
    • Corresponding Author:
    ZHU Jinpeng (1989-), male, Ph.D., Associate Professor. E-mail:

    ZHAO Yang (1996-), male, Master candidate. E-mail:

出版时间: 2021-04-20 doi: 10.14062/j.issn.0454-5648.20200732
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采用高分辨透射电子显微镜（HR-TEM）与球差校正电镜高角环形暗场（HAADF）像研究了层状钙钛矿La0.9Sr0.1TiO3+δ（LST）的显微结构，揭示了该材料体系中存在的氧空位缺陷对晶格结构的作用机制。结果表明：材料晶格结构受缺氧环境的影响会引起LST晶胞a，b轴长度的缩短与c轴的相对伸长，在整体上表现为晶胞的体积收缩。基于高分辨显微像与Z衬度原子像的分析，能够识别由氧空位引发的部分原子面重排以及由连续晶格畸变所导致的位错现象。氧空位缺陷的有效调控将对优化材料微观结构，进一步制备高反射率钙钛矿材料具有重要意义。

层状钙钛矿  /  氧空位  /  显微结构  /  高角环形暗场像

The microstructure of layer perovskite La0.9Sr0.1TiO3+δ was investigated by high-resolution transmission electron microscopy and high angle annular dark field image analysis. The mechanism of oxygen vacancy on the lattice structure was revealed. Based on the results by X-ray diffraction, the oxygen-difficient environment effect on the lattice structure leads to the change of axial length and volume contraction in the material. The partial atomic plane rearrangement and dislocation caused by oxygen vacancy and continuous lattice distortion are identified based on high-resolution microscopic and Z-contrast atomic images, respectively. The effective regulation of oxygen vacancy defect shows a great significance on changing the microstructure of materials and further preparation of high-performance perovskite materials.

layer perovskite  /  oxygen vacancy  /  microstructure  /  high angle annular dark field
赵阳, 朱锦鹏, 王海龙, 邵刚, 杨凯军, 马壮, 高丽红, 舒永春, 何季麟. 氧空位对La0.9Sr0.1TiO3+δ层状钙钛矿陶瓷微观结构的调控作用. 硅酸盐学报, 2021 , 49 (4) : 633 -638 . DOI: 10.14062/j.issn.0454-5648.20200732
Yang ZHAO, Jinpeng ZHU, Hailong WANG, Gang SHAO, Kaijun YANG, Zhuang MA, Lihong GAO, Yongchun SHU, Jilin HE. Regulatory Effect of Oxygen Vacancy on Microstructure of La0.9Sr0.1TiO3+δ Layer Perovskite Ceramics[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (4) : 633 -638 . DOI: 10.14062/j.issn.0454-5648.20200732
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  • 国家自然科学基金青年项目(52002355)
  • 装备预研重点实验室基金项目(6142902200202)
  • 中国博士后面上基金(2019M652569)
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2021年第49卷第4期
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doi: 10.14062/j.issn.0454-5648.20200732
  • 接收时间：2020-09-26
  • 首发时间：2026-10-30
  • 出版时间：2021-04-20
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  • 收稿日期：2020-09-26
  • 修回日期：2020-11-19
基金
国家自然科学基金青年项目(52002355)
装备预研重点实验室基金项目(6142902200202)
中国博士后面上基金(2019M652569)
作者信息
    1．郑州大学，河南省资源与材料工业技术研究院，郑州 450001
    2．郑州大学材料科学与工程学院，郑州 450001
    3．北京理工大学材料科学与工程学院，冲击环境材料技术重点实验室，北京 100081

通讯作者:

朱锦鹏（1989—），男，博士，副教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200732
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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