Article(id=1322943213866201321, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210532, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1625068800000, receivedDateStr=2021-07-01, revisedDate=1626019200000, revisedDateStr=2021-07-12, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343841281, onlineDateStr=2026-10-30, pubDate=1639929600000, pubDateStr=2021-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343841281, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343841281, creator=13701087609, updateTime=1793343841281, updator=13701087609, issue=Issue{id=1322943149844345666, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='12', pageStart='2549', pageEnd='2816', issueExtLink='null', onlineDate='null', pubDate='1639929600000', pubDateStr='2021-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343826018, creator='13701087609', updateTime=1793345974749, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322952162350859029, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322952162350859030, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322943149844345666, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2581, endPage=2588, ext={EN=ArticleExt(id=1322943214180774122, articleId=1322943213866201321, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Performance of Porous Mullite Lightweight Materials by Microemulsion Template Method, columnId=1322943189916725340, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Topic on Engineering Ceramic Material, runingTitle=null, highlight=null, articleAbstract=

Porous mullite lightweight materials were prepared by a microemulsion template method and subsequent sintering with fly ash and calcined bauxite as raw materials, Isobam 104 as a dispersant, carboxymethyl cellulose as a suspending agent, polyoxyethylene sorbitan monooleate (Tween 80) as a surfactant, isooctane as an oil phase, ethylene glycol glycidyl ether as a binder and tetraethylenepentamine as a curing agent. The influences of fly ash content and Tween 80 content on the phase composition, linear shrinkage, bulk density, porosity, microstructure and mechanical properties of porous mullite lightweight materials were investigated. The results show that the linear shrinkage rate, bulk density and mechanical strength of porous materials prepared with 55% fly ash decrease, but the porosity increases as the volume ratio of Tween 80 to water increases from 2∶100 to 5∶∶100. When the volume ratio of Tween 80 to water is 5∶100, the compressive strength and flexural strength of porous mullite lightweight materials with a porosity of 65.5%, a spherical pore diameter of 162 μm, and a linear shrinkage rate of only 14.5% can reach 42.5 MPa and 26.0 MPa, respectively.

, authors=Jiaqiang YIN1, 2, Chenghao SONG2, Peng JI2, Yunlong WANG2, Yi Zhang2, Xiang DING1, Songlin RAN1, Xiangong DENG1, 2, Haijun ZHANG3, authorsList=Jiaqiang YIN, Chenghao SONG, Peng JI, Yunlong WANG, Yi Zhang, Xiang DING, Songlin RAN, Xiangong DENG, Haijun ZHANG, authorCompany=null, correspAuthors=Xiangong DENG, authorNote=

YIN Jiaqiang (1994-), male, Master candidate. E-mail:

, correspAuthorsNote=
DENG Xiangong (1980-), male, Ph.D., lecturer. E-mail:
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以粉煤灰和煅烧铝矾土为原料、Isobam 104为分散剂、羧甲基纤维素钠(CMC)为悬浮剂、聚氧乙烯山梨醇酐单油酸酯(Tween 80)为表面活性剂、异辛烷为油相、乙二醇缩水甘油醚为黏结剂、四乙烯五胺为固化剂,采用微乳液模板法结合反应烧结制备了多孔莫来石轻质材料。研究了粉煤灰的用量和Tween 80的用量等对多孔莫来石轻质材料物相组成、线收缩率、体积密度、气孔率、显微结构和常温力学性能等的影响。结果表明:粉煤灰的用量为55%(质量分数)时,随着表面活性剂Tween 80与水体积比从2∶100增至5∶100时,所制备试样的线收缩率、体积密度和机械强度逐渐减小,而气孔率逐渐增大。当Tween 80与水体积比为5∶100时,所制备气孔率为65.5%(体积分数)、球形孔径约为162 μm的多孔莫来石轻质材料的抗压强度和抗折强度分别达42.5 MPa和26.0 MPa,其线收缩率仅为14.5%。

, authors=殷加强1, 2, 宋承豪2, 季鹏2, 王云龙2, 张毅2, 丁祥1, 冉松林1, 邓先功1, 2, 张海军3, authorsList=殷加强, 宋承豪, 季鹏, 王云龙, 张毅, 丁祥, 冉松林, 邓先功, 张海军, authorCompany=null, correspAuthors=邓先功, authorNote=

殷加强(1994—),男,硕士研究生。

, correspAuthorsNote=
邓先功(1980—),男,博士,讲师。
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微乳液模板法制备多孔莫来石轻质材料及其性能
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殷加强 1, 2 , 宋承豪 2 , 季鹏 2 , 王云龙 2 , 张毅 2 , 丁祥 1 , 冉松林 1 , 邓先功 1, 2 , 张海军 3
硅酸盐学报 | 工程陶瓷材料专题 2021,49(12): 2581-2588
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硅酸盐学报 |工程陶瓷材料专题 2021 , 49 (12) : 2581 -2588
微乳液模板法制备多孔莫来石轻质材料及其性能
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殷加强1, 2 , 宋承豪2, 季鹏2, 王云龙2, 张毅2, 丁祥1, 冉松林1, 邓先功1, 2 , 张海军3
作者信息
  • 1.冶金工程与资源综合利用安徽省重点实验室(安徽工业大学),安徽 马鞍山 243032
  • 2.安徽工业大学材料科学与工程学院先进金属材料绿色制备与表面技术教育部重点实验室,安徽 马鞍山 243002
  • 3.武汉科技大学省部共建耐火材料与冶金国家重点实验室,武汉 430081
通讯作者:
邓先功(1980—),男,博士,讲师。
作者简介:

殷加强(1994—),男,硕士研究生。

Preparation and Performance of Porous Mullite Lightweight Materials by Microemulsion Template Method
Jiaqiang YIN1, 2 , Chenghao SONG2, Peng JI2, Yunlong WANG2, Yi Zhang2, Xiang DING1, Songlin RAN1, Xiangong DENG1, 2 , Haijun ZHANG3
Affiliations
  • 1.Anhui Province Key Laboratory of Metallurgical Engineering & Resources Recycling (Anhui University of Technology), Ma'anshan 243032, Anhui, China
  • 2.School of Materials Science and Engineering, Key Laboratory of Green Fabrication and Surface Technology of Advanced Metal Materials, Ministry of Education, Anhui University of Technology, Ma'anshan 243002, China
  • 3.The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China
  • Corresponding Author:
    DENG Xiangong (1980-), male, Ph.D., lecturer. E-mail:

    YIN Jiaqiang (1994-), male, Master candidate. E-mail:

出版时间: 2021-12-20 doi: 10.14062/j.issn.0454-5648.20210532
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以粉煤灰和煅烧铝矾土为原料、Isobam 104为分散剂、羧甲基纤维素钠(CMC)为悬浮剂、聚氧乙烯山梨醇酐单油酸酯(Tween 80)为表面活性剂、异辛烷为油相、乙二醇缩水甘油醚为黏结剂、四乙烯五胺为固化剂,采用微乳液模板法结合反应烧结制备了多孔莫来石轻质材料。研究了粉煤灰的用量和Tween 80的用量等对多孔莫来石轻质材料物相组成、线收缩率、体积密度、气孔率、显微结构和常温力学性能等的影响。结果表明:粉煤灰的用量为55%(质量分数)时,随着表面活性剂Tween 80与水体积比从2∶100增至5∶100时,所制备试样的线收缩率、体积密度和机械强度逐渐减小,而气孔率逐渐增大。当Tween 80与水体积比为5∶100时,所制备气孔率为65.5%(体积分数)、球形孔径约为162 μm的多孔莫来石轻质材料的抗压强度和抗折强度分别达42.5 MPa和26.0 MPa,其线收缩率仅为14.5%。

多孔莫来石轻质材料  /  微乳液模板法  /  粉煤灰  /  反应烧结

Porous mullite lightweight materials were prepared by a microemulsion template method and subsequent sintering with fly ash and calcined bauxite as raw materials, Isobam 104 as a dispersant, carboxymethyl cellulose as a suspending agent, polyoxyethylene sorbitan monooleate (Tween 80) as a surfactant, isooctane as an oil phase, ethylene glycol glycidyl ether as a binder and tetraethylenepentamine as a curing agent. The influences of fly ash content and Tween 80 content on the phase composition, linear shrinkage, bulk density, porosity, microstructure and mechanical properties of porous mullite lightweight materials were investigated. The results show that the linear shrinkage rate, bulk density and mechanical strength of porous materials prepared with 55% fly ash decrease, but the porosity increases as the volume ratio of Tween 80 to water increases from 2∶100 to 5∶∶100. When the volume ratio of Tween 80 to water is 5∶100, the compressive strength and flexural strength of porous mullite lightweight materials with a porosity of 65.5%, a spherical pore diameter of 162 μm, and a linear shrinkage rate of only 14.5% can reach 42.5 MPa and 26.0 MPa, respectively.

porous mullite lightweight materials  /  microemulsion template method  /  fly ash  /  reaction sintering
殷加强, 宋承豪, 季鹏, 王云龙, 张毅, 丁祥, 冉松林, 邓先功, 张海军. 微乳液模板法制备多孔莫来石轻质材料及其性能. 硅酸盐学报, 2021 , 49 (12) : 2581 -2588 . DOI: 10.14062/j.issn.0454-5648.20210532
Jiaqiang YIN, Chenghao SONG, Peng JI, Yunlong WANG, Yi Zhang, Xiang DING, Songlin RAN, Xiangong DENG, Haijun ZHANG. Preparation and Performance of Porous Mullite Lightweight Materials by Microemulsion Template Method[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (12) : 2581 -2588 . DOI: 10.14062/j.issn.0454-5648.20210532
  • 安徽省自然科学基金(1908085ME117)
  • 国家自然科学基金(U1860102)
  • 安徽省高校协同创新项目(GXXT-2019-015)
  • 冶金工程与资源综合利用安徽省重点实验室开放基金(SKF20-02)
  • 安徽省大学生创新创业训练计划(S202110360191)
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2021年第49卷第12期
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doi: 10.14062/j.issn.0454-5648.20210532
  • 接收时间:2021-07-01
  • 首发时间:2026-10-30
  • 出版时间:2021-12-20
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出版历史
  • 收稿日期:2021-07-01
  • 修回日期:2021-07-12
基金
安徽省自然科学基金(1908085ME117)
国家自然科学基金(U1860102)
安徽省高校协同创新项目(GXXT-2019-015)
冶金工程与资源综合利用安徽省重点实验室开放基金(SKF20-02)
安徽省大学生创新创业训练计划(S202110360191)
作者信息
    1.冶金工程与资源综合利用安徽省重点实验室(安徽工业大学),安徽 马鞍山 243032
    2.安徽工业大学材料科学与工程学院先进金属材料绿色制备与表面技术教育部重点实验室,安徽 马鞍山 243002
    3.武汉科技大学省部共建耐火材料与冶金国家重点实验室,武汉 430081

通讯作者:

邓先功(1980—),男,博士,讲师。
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Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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