Article(id=1322943186552889705, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942592224211277, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200677, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1599148800000, receivedDateStr=2020-09-04, revisedDate=1602691200000, revisedDateStr=2020-10-15, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343834769, onlineDateStr=2026-10-30, pubDate=1621440000000, pubDateStr=2021-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343834769, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343834769, creator=13701087609, updateTime=1793343834769, updator=13701087609, issue=Issue{id=1322942592224211277, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='5', pageStart='807', pageEnd='1032', issueExtLink='null', onlineDate='null', pubDate='1621440000000', pubDateStr='2021-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343693071, creator='13701087609', updateTime=1793345545174, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950360561754466, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942592224211277, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950360565948771, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942592224211277, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=901, endPage=909, ext={EN=ArticleExt(id=1322943186750021994, articleId=1322943186552889705, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Composition and Nano-structure of C-(A)-S-H Gels in Cement Pastes after Sulphate Attack, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

The nano-structural change of hydrated calcium silicate gels (C-(A)-S-H) in Portland cement (PC) and high-sulphate resistance cement (HSR) mortars under wetting-drying cycling conditions in 5% (mass fraction) MgSO₄ solution was investigated by Fourier-transform infrared spectroscopy (FTIR), thermogravimetry-tifferential scanning calorimetry (TG-DSC), ²⁹Si magic-angle spinning nuclear magnetic resonance (MAS-NMR), and transmission electron microscopy-energy dispersive X-ray spectroscopy (TEM-EDX). The results show that Al-tetrahedra in C-(A)-S-H phase is plausibly the weakness during sulphate attack, the Q¹ (dimer or end-member in the chain) in the main aluminosilicate tetrahedral chain can be easily attacked by MgSO₄ to form M/C-(A)-S-H, and sulphate ions are easily absorbed on the surface of C-(A)-S-H through -Si-O-M²⁺-1/2SO₄^2-. The chemical compositions of C-(A)-S-H in all the samples before and after sulphate attack were simulated by the tobermorite/jennite (T/J) model. The difference between the nano-structural and the average compositional formulas of C-(A)-S-H gels in two cements after sulphate attack was derived from the (T/J) model. It is necessary for the improvement of the resistance of motors against MgSO₄ attack to restrict the expansive corrosion products (i.e., gypsum and AFt) and Al-tetrahedra in the aluminosilicate chain of C-(A)-S-H phase.

, authors=Xiaohong ZHU^{1, 2}, Qing LI^{1, 3}, Ping CHEN¹, Xiaojuan KANG⁴, Kai YANG³, Changhui YANG³, authorsList=Xiaohong ZHU, Qing LI, Ping CHEN, Xiaojuan KANG, Kai YANG, Changhui YANG, authorCompany=null, correspAuthors=Qing LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943186976514411, articleId=1322943186552889705, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=硫酸盐侵蚀条件下C-(A)-S-H组成-结构演化的量化分析, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

采用Fourier变换红外光谱、综合热分析、²⁹Si魔角自旋核磁共振及透射电镜-能谱等方法，研究了5%MgSO₄（质量分数）溶液干湿循环作用下硅酸盐水泥及高抗硫酸盐水泥砂浆中水化硅酸钙凝胶（C-（A）-S-H）结构变化。结果表明：硫酸盐易侵蚀C-（A）-S-H凝胶中[AlO₄]桥氧四面体，[SiO₄]长链中Q¹（二聚体或硅链尾端）也易受MgSO₄侵蚀形成M/C-（A）-S-H凝胶；硫酸根与阳离子桥接，形成-Si-O-M²⁺-1/2SO₄^2-结构吸附于C-（A）-S-H凝胶表层。采用托贝莫来石/羟基硅钙石混合模型（T/J model）推演了硅酸盐水泥和高抗硫酸盐水泥中C-（A）-S-H凝胶在MgSO₄溶液中干湿循环后的结构差异，给出了侵蚀后C-（A）-S-H组成化学式。提升抗MgSO₄侵蚀能力在于控制膨胀产物（石膏及AFt）及C-（A）-S-H凝胶中[AlO₄]桥氧四面体含量。

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