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Article(id=1322943133612376072, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942446610559222, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200476, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1593360000000, receivedDateStr=2020-06-29, revisedDate=1596470400000, revisedDateStr=2020-08-04, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343822148, onlineDateStr=2026-10-30, pubDate=1613750400000, pubDateStr=2021-02-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343822148, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343822148, creator=13701087609, updateTime=1793343822148, updator=13701087609, issue=Issue{id=1322942446610559222, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='2', pageStart='211', pageEnd='440', issueExtLink='null', onlineDate='null', pubDate='1613750400000', pubDateStr='2021-02-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343658354, creator='13701087609', updateTime=1793345474672, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950064863314723, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942446610559222, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950064863314724, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942446610559222, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=220, endPage=228, ext={EN=ArticleExt(id=1322943136548388873, articleId=1322943133612376072, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Surface-enhanced Raman Scattering from Electrospun Cellulose Acetate Nanofibers Loaded with Aggregated Ag-nanocubes, columnId=1319987100586459893, journalTitle=Journal of the Chinese Ceramic Society, columnName=Special Issue on Inerim Achievements of Key Program of National Natural Science Foundation of China, runingTitle=null, highlight=null, articleAbstract=

Cellulose acetate (CA) nanofibers were embedded with aggregated silver-nanocubes (AgNCs) by a coaxial electrospinning method. AgNCs were dispersed with CA and acetone-dimethylacetamide (DMAc) as a precursor solution, and AgNCs aggregation was induced with acetone. The nanofibers have a remarkable surface-enhanced Raman scattering (SERS) activity due to the strong plasmon coupling between neighboring AgNCs, which is 4 times of the monomeric-AgNC/CA sample. As a result, 0.1 nmol/L p-aminothiophenol (p-ATP) and 10 nmol/L methyl parathion can be identified, respectively. The nanofibers generate large-area homogeneous SERS signals with a relative signal deviation of less than 12% over 1 mm×1 mm area due to the homogeneous adsorption of target molecules. It is thus indicated that aggregated-AgNCs/CA nanofibers have a promising potential in SERS-based detection of organic pollutants in aqueous solutions.

, authors=Yan KE1, 3, Bin CHEN1, Ningning ZHOU1, Zhulin HUANG1, Guowen MENG1, 2, authorsList=Yan KE, Bin CHEN, Ningning ZHOU, Zhulin HUANG, Guowen MENG, authorCompany=null, correspAuthors=Zhulin HUANG, Guowen MENG, authorNote=

KE Yan (1989-), male, Ph.D.; E-mail:

CHEN Bin (1986-), male, Ph.D., Associate Professor.

, correspAuthorsNote=
MENG Guowen (1960-), male, Ph.D., Professor. E-mail:
HUANG Zhulin (1984-), male, Ph.D., Associate Professor.
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322943138234499082, articleId=1322943133612376072, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=负载银纳米立方体的醋酸纤维素纳米纤维及其SERS活性, columnId=1322942447482974456, journalTitle=硅酸盐学报, columnName=国家自然科学基金重点项目中期成果专题, runingTitle=null, highlight=null, articleAbstract=

报道了一种采用同轴静电纺丝法制备的表面增强Raman散射（SERS）活性衬底，用于微量环境污染物的快速检测。采用醋酸纤维素（CA）/丙酮-二甲基乙酰胺溶液作为前驱液分散银纳米立方体，利用丙酮促进银颗粒适度团聚，采用同轴静电纺丝法制备了大面积银立方体/CA纳米纤维。由于团聚态银纳米立方体之间的等离子体耦合作用，复合薄膜具有优异的SERS活性，是单分散态的银立方体/CA纳米纤维SERS灵敏度的4倍，实现了0.1 nmol/L的对巯基苯胺以及10 nmol/L的甲基对硫磷农药的SERS检测，SERS信号强度偏差小于12%。

, authors=柯岩1, 3, 陈斌1, 周宁宁1, 黄竹林1, 孟国文1, 2, authorsList=柯岩, 陈斌, 周宁宁, 黄竹林, 孟国文, authorCompany=null, correspAuthors=黄竹林, 孟国文, authorNote=

柯岩（1989—），男，博士；

陈斌（1986—），男，博士，副研究员。

, correspAuthorsNote=
孟国文（1960—），男，博士，研究员；
黄竹林（1984—），男，博士，副研究员。
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CHEN Bin (1986-), male, Ph.D., Associate Professor.

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负载银纳米立方体的醋酸纤维素纳米纤维及其SERS活性
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柯岩 1, 3 , 陈斌 1 , 周宁宁 1 , 黄竹林 1 , 孟国文 1, 2
硅酸盐学报 | 国家自然科学基金重点项目中期成果专题 2021,49(2): 220-228
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硅酸盐学报 |国家自然科学基金重点项目中期成果专题 2021 , 49 (2) : 220 -228
负载银纳米立方体的醋酸纤维素纳米纤维及其SERS活性
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柯岩1, 3 , 陈斌1 , 周宁宁1, 黄竹林1 , 孟国文1, 2
作者信息
  • 1．中国科学院合肥物质科学研究院，固体物理研究所，材料物理重点实验室和安徽省纳米材料与技术重点实验室，合肥 230031
  • 2．中国科学技术大学化学与材料科学学院 合肥 230026
  • 3．广东溢达纺织有限公司，广东 佛山 528500
通讯作者:
孟国文（1960—），男，博士，研究员；
黄竹林（1984—），男，博士，副研究员。
作者简介:

柯岩（1989—），男，博士；

陈斌（1986—），男，博士，副研究员。

Surface-enhanced Raman Scattering from Electrospun Cellulose Acetate Nanofibers Loaded with Aggregated Ag-nanocubes
Yan KE1, 3 , Bin CHEN1 , Ningning ZHOU1, Zhulin HUANG1 , Guowen MENG1, 2
Affiliations
  • 1.Key Laboratory of Materials Physics and Anhui Key Laboratory of Nanomaterials and Technology, Institute of Solid State Physics, HFIPS, Chinese Academy of Sciences, Hefei 230031, China
  • 2.School of Chemistry and Materials Science, University of Science and Technology of China, Hefei 230026, China
  • 3.Guangdong Esquel Textiles Company Limited, Foshan 528500, Guangdong, China
    • Corresponding Author:
    MENG Guowen (1960-), male, Ph.D., Professor. E-mail:
    HUANG Zhulin (1984-), male, Ph.D., Associate Professor.

    KE Yan (1989-), male, Ph.D.; E-mail:

    CHEN Bin (1986-), male, Ph.D., Associate Professor.

出版时间: 2021-02-20 doi: 10.14062/j.issn.0454-5648.20200476
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摘要
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报道了一种采用同轴静电纺丝法制备的表面增强Raman散射（SERS）活性衬底，用于微量环境污染物的快速检测。采用醋酸纤维素（CA）/丙酮-二甲基乙酰胺溶液作为前驱液分散银纳米立方体，利用丙酮促进银颗粒适度团聚，采用同轴静电纺丝法制备了大面积银立方体/CA纳米纤维。由于团聚态银纳米立方体之间的等离子体耦合作用，复合薄膜具有优异的SERS活性，是单分散态的银立方体/CA纳米纤维SERS灵敏度的4倍，实现了0.1 nmol/L的对巯基苯胺以及10 nmol/L的甲基对硫磷农药的SERS检测，SERS信号强度偏差小于12%。

表面增强拉曼散射  /  银纳米方块  /  纳米纤维  /  静电纺丝

Cellulose acetate (CA) nanofibers were embedded with aggregated silver-nanocubes (AgNCs) by a coaxial electrospinning method. AgNCs were dispersed with CA and acetone-dimethylacetamide (DMAc) as a precursor solution, and AgNCs aggregation was induced with acetone. The nanofibers have a remarkable surface-enhanced Raman scattering (SERS) activity due to the strong plasmon coupling between neighboring AgNCs, which is 4 times of the monomeric-AgNC/CA sample. As a result, 0.1 nmol/L p-aminothiophenol (p-ATP) and 10 nmol/L methyl parathion can be identified, respectively. The nanofibers generate large-area homogeneous SERS signals with a relative signal deviation of less than 12% over 1 mm×1 mm area due to the homogeneous adsorption of target molecules. It is thus indicated that aggregated-AgNCs/CA nanofibers have a promising potential in SERS-based detection of organic pollutants in aqueous solutions.

surface-enhanced Raman scattering  /  Ag-nanocube  /  nanofiber  /  electrospinning
柯岩, 陈斌, 周宁宁, 黄竹林, 孟国文. 负载银纳米立方体的醋酸纤维素纳米纤维及其SERS活性. 硅酸盐学报, 2021 , 49 (2) : 220 -228 . DOI: 10.14062/j.issn.0454-5648.20200476
Yan KE, Bin CHEN, Ningning ZHOU, Zhulin HUANG, Guowen MENG. Surface-enhanced Raman Scattering from Electrospun Cellulose Acetate Nanofibers Loaded with Aggregated Ag-nanocubes[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (2) : 220 -228 . DOI: 10.14062/j.issn.0454-5648.20200476
基金
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  • 国家自然科学基金(51632009; 91963202; 21673245)
  • 中科院前沿科学重点研究计划(QYZDJ-SSW-SLH046)
  • 中科院青年创新促进会
  • 安徽省自然科学基金(1908085QE173)
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2021年第49卷第2期
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doi: 10.14062/j.issn.0454-5648.20200476
  • 接收时间：2020-06-29
  • 首发时间：2026-10-30
  • 出版时间：2021-02-20
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出版历史
  • 收稿日期：2020-06-29
  • 修回日期：2020-08-04
基金
国家自然科学基金(51632009; 91963202; 21673245)
中科院前沿科学重点研究计划(QYZDJ-SSW-SLH046)
中科院青年创新促进会
安徽省自然科学基金(1908085QE173)
作者信息
    1．中国科学院合肥物质科学研究院，固体物理研究所，材料物理重点实验室和安徽省纳米材料与技术重点实验室，合肥 230031
    2．中国科学技术大学化学与材料科学学院 合肥 230026
    3．广东溢达纺织有限公司，广东 佛山 528500

通讯作者:

孟国文（1960—），男，博士，研究员；
黄竹林（1984—），男，博士，副研究员。
参考文献
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200476
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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