Article(id=1322943118437393176, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200620, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1597593600000, receivedDateStr=2020-08-17, revisedDate=1600099200000, revisedDateStr=2020-09-15, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343818530, onlineDateStr=2026-10-30, pubDate=1618848000000, pubDateStr=2021-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343818530, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343818530, creator=13701087609, updateTime=1793343818530, updator=13701087609, issue=Issue{id=1322942545734546372, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='4', pageStart='605', pageEnd='806', issueExtLink='null', onlineDate='null', pubDate='1618848000000', pubDateStr='2021-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343681986, creator='13701087609', updateTime=1793345524324, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950273110508350, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950273110508351, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=702, endPage=707, ext={EN=ArticleExt(id=1322943118827463449, articleId=1322943118437393176, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Characterization of Tetragonal Zirconia by Step Pressure Assisted Flash Sintering, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The secondary pressure assisted flash sintering process of tetragonal zirconia ceramics was developed. The process optimized the process and eliminated the deterioration of microstructure caused by high power flash sintering at critical flash temperature. The results show that: the multi-step pressure assisted flash sintering process retains the advantages of low-temperature and instantaneous sintering, avoids the complex green pressing process and the high cost of precious metal electrode. Yttrium stabilized zirconia can be densified by multiple flash sintering. The sintering temperature is lower than 1 050℃ and the sintering time is less than 200 s. The density of tetragonal zirconia ceramic material prepared by this process is more than 90%.

, authors=Shuai LUO, Chengwei YU, Yanghui LU, Lijun WEI, authorsList=Shuai LUO, Chengwei YU, Yanghui LU, Lijun WEI, authorCompany=null, correspAuthors=Yanghui LU, authorNote=

LUO Shuai (1987-), male, Ph.D. E-mail:

, correspAuthorsNote=
LU Yanghui (1981-), male, Master. E-mail:
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开发了一种四方相氧化锆陶瓷材料的二次分步加压辅助闪烧烧结工艺,该工艺对加压辅助闪烧工艺进行了优化,消除了临界闪烧温度下高功率闪烧导致的微观组织结构劣化现象。结果表明:多次分步加压辅助闪烧工艺保留了闪烧方法低温、瞬时烧结的优点,规避了复杂生坯压制工序和贵金属电极高昂成本,钇稳氧化锆可通过多次闪烧获得致密化,该工艺烧结温度低于1050℃,烧结时间小于200 s,制备的四方氧化锆陶瓷材料的密度达到90%以上。

, authors=罗帅, 于成伟, 鲁仰辉, 魏立军, authorsList=罗帅, 于成伟, 鲁仰辉, 魏立军, authorCompany=null, correspAuthors=鲁仰辉, authorNote=

罗帅(1987—),男,博士,高级工程师。

, correspAuthorsNote=
鲁仰辉(1981—),男,硕士,高级工程师。
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四方相氧化锆分步加压辅助闪烧烧结制备及性能
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罗帅 , 于成伟 , 鲁仰辉 , 魏立军
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四方相氧化锆分步加压辅助闪烧烧结制备及性能
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罗帅 , 于成伟, 鲁仰辉 , 魏立军
作者信息
  • 国家电投集团科学技术研究院有限公司,北京 102209
通讯作者:
鲁仰辉(1981—),男,硕士,高级工程师。
作者简介:

罗帅(1987—),男,博士,高级工程师。

Preparation and Characterization of Tetragonal Zirconia by Step Pressure Assisted Flash Sintering
Shuai LUO , Chengwei YU, Yanghui LU , Lijun WEI
Affiliations
  • State Power Investment Corporation Research Institute, Co. Ltd, Beijing 102209, China
  • Corresponding Author:
    LU Yanghui (1981-), male, Master. E-mail:

    LUO Shuai (1987-), male, Ph.D. E-mail:

出版时间: 2021-04-20 doi: 10.14062/j.issn.0454-5648.20200620
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开发了一种四方相氧化锆陶瓷材料的二次分步加压辅助闪烧烧结工艺,该工艺对加压辅助闪烧工艺进行了优化,消除了临界闪烧温度下高功率闪烧导致的微观组织结构劣化现象。结果表明:多次分步加压辅助闪烧工艺保留了闪烧方法低温、瞬时烧结的优点,规避了复杂生坯压制工序和贵金属电极高昂成本,钇稳氧化锆可通过多次闪烧获得致密化,该工艺烧结温度低于1050℃,烧结时间小于200 s,制备的四方氧化锆陶瓷材料的密度达到90%以上。

氧化锆  /  闪烧烧结  /  低温快速烧结  /  四方相  /  多次分步闪烧

The secondary pressure assisted flash sintering process of tetragonal zirconia ceramics was developed. The process optimized the process and eliminated the deterioration of microstructure caused by high power flash sintering at critical flash temperature. The results show that: the multi-step pressure assisted flash sintering process retains the advantages of low-temperature and instantaneous sintering, avoids the complex green pressing process and the high cost of precious metal electrode. Yttrium stabilized zirconia can be densified by multiple flash sintering. The sintering temperature is lower than 1 050℃ and the sintering time is less than 200 s. The density of tetragonal zirconia ceramic material prepared by this process is more than 90%.

zirconia  /  flash sintering  /  low temperature rapid sintering  /  tetragonal  /  pressure assisted stepped flash sintering
罗帅, 于成伟, 鲁仰辉, 魏立军. 四方相氧化锆分步加压辅助闪烧烧结制备及性能. 硅酸盐学报, 2021 , 49 (4) : 702 -707 . DOI: 10.14062/j.issn.0454-5648.20200620
Shuai LUO, Chengwei YU, Yanghui LU, Lijun WEI. Preparation and Characterization of Tetragonal Zirconia by Step Pressure Assisted Flash Sintering[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (4) : 702 -707 . DOI: 10.14062/j.issn.0454-5648.20200620
  • 国家核电技术有限公司科研项目-大晶粒二氧化铀燃料材料试制(2015SN010-003)
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doi: 10.14062/j.issn.0454-5648.20200620
  • 接收时间:2020-08-17
  • 首发时间:2026-10-30
  • 出版时间:2021-04-20
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  • 收稿日期:2020-08-17
  • 修回日期:2020-09-15
基金
国家核电技术有限公司科研项目-大晶粒二氧化铀燃料材料试制(2015SN010-003)
作者信息
    国家电投集团科学技术研究院有限公司,北京 102209

通讯作者:

鲁仰辉(1981—),男,硕士,高级工程师。
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属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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