Article(id=1322942885892600590, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210164, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1615219200000, receivedDateStr=2021-03-09, revisedDate=1617033600000, revisedDateStr=2021-03-30, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343763087, onlineDateStr=2026-10-30, pubDate=1634659200000, pubDateStr=2021-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343763087, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343763087, creator=13701087609, updateTime=1793343763087, updator=13701087609, issue=Issue{id=1322942849381183980, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='10', pageStart='2045', pageEnd='2312', issueExtLink='null', onlineDate='null', pubDate='1634659200000', pubDateStr='2021-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343754382, creator='13701087609', updateTime=1793345931656, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951981580562527, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951981584756832, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2070, endPage=2077, ext={EN=ArticleExt(id=1322942886278476559, articleId=1322942885892600590, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=In Situ Growth of CuO Quantum Dots on Cu-Reconstructed Palygorskite for Wide-Spectrum Photocatalytic Nitrogen Fixation, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Octahedral cations of acid-treated palygorskite clay (Pal) were partially replaced by Cu²⁺ via hydrothermal method to achieve lattice reconstruction (Cu-Pal). CuO quantum dots (CuO QDs) were grown in situ on the surface of Cu-Pal by adjust the pH and thermal treatment in case of excess Cu²⁺, which led to the formation of CuO QDs/Cu-Pal nanocomposite toward photocatalytic nitrogen fixation. The influence of Cu²⁺ content on the microstructure, optical property and band gap structure of Pal were studied. Results showed that the Cu substitution narrowed the band gap of Pal which extended the light response range from ultraviolet light to visible light. When the Cu²⁺ content exceeded 5% (in mass fraction), CuO QDs on the Cu-Pal surface effectively promoted the absorption of NIR light due to its rather low band gap (1.2 eV). 20% Cu-Pal formed the best-matched Type-I heterostructure and demonstrated the highest photocatalytic nitrogen fixation performance due to the enhanced charge separation.

, authors=Song YANG¹, Xini CHU¹, Wenjun LI¹, Chengli HE¹, Xuhua YE¹, Fengqin WU¹, Xiazhang LI^{1, 2}, authorsList=Song YANG, Xini CHU, Wenjun LI, Chengli HE, Xuhua YE, Fengqin WU, Xiazhang LI, authorCompany=null, correspAuthors=Fengqin WU, Xiazhang LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322942886467220240, articleId=1322942885892600590, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Cu重建凹凸棒石原位固载CuO量子点及其宽光谱固氮特性, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

通过水热法用Cu²⁺置换酸活化凹凸棒石黏土（Pal）八面体阳离子实现晶格重建（Cu-Pal），过量的Cu²⁺经过溶液pH值调变和煅烧后，在Cu-Pal表面原位生长出氧化铜量子点（CuO QDs），从而制备出CuO QDs/Cu-Pal纳米复合材料，并将其应用于光催化固氮，考察了Cu²⁺用量对凹凸棒石微观形貌、光学性质和能带结构的影响。结果表明：Cu-Pal具有更窄的带隙，将光响应范围从紫外光拓展到可见光。当Cu²⁺含量超过5%（质量分数）时，Cu-Pal表面的CuO QDs由于窄带隙（1.2 eV）增强了近红外光的吸收。20%含量下Cu-Pal纳米复合材料形成最匹配的Type-I异质结构，有效促进了光生载流子的分离，显著提高了光催化固氮性能。

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YANG Song (1984-), male, PhD candidate. E-mail: 214175924@qq.com

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YANG Song (1984-), male, PhD candidate. E-mail: 214175924@qq.com

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杨松（1984—），男，博士研究生。

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杨松（1984—），男，博士研究生。

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