Article(id=1322942874102411944, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200912, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1607616000000, receivedDateStr=2020-12-11, revisedDate=1618588800000, revisedDateStr=2021-04-17, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343760276, onlineDateStr=2026-10-30, pubDate=1634659200000, pubDateStr=2021-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343760276, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343760276, creator=13701087609, updateTime=1793343760276, updator=13701087609, issue=Issue{id=1322942849381183980, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='10', pageStart='2045', pageEnd='2312', issueExtLink='null', onlineDate='null', pubDate='1634659200000', pubDateStr='2021-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343754382, creator='13701087609', updateTime=1793345931656, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951981580562527, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951981584756832, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942849381183980, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2089, endPage=2097, ext={EN=ArticleExt(id=1322942874265989801, articleId=1322942874102411944, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Solid-State Synthesis of Spherical-like Silicalite-1 Zeolite, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Clustered crystals of Silicalite-1 forming spherical-like structures were synthesized by a solvent-free solid-state method using activated carbon as a hard template. The influence of activated carbon dosage on the Silicalite-1 zeolite was explored by X-ray diffraction, specific surface area analysis, scanning electron microscopy, transmission electron microscopy, infrared spectroscopy, and X-ray photoelectric spectroscopy. The results show that the C—O—Si bond is formed between hydroxyl groups on the surface of activated carbon and silicic acid, growing and aggregating along the activated carbon and formed spherical-like Silicalite-1 zeolites after calcination. The spherical-like Silicalite-1 prepared with 10% (in mass fraction) activated carbon has a greater crystallinity with great specific surface area and pore volume as well as uniform particle size.

, authors=Mingquan LI, Jiayuan WANG, Yajie FU, Xu SUN, Ruiqin YANG, Chuang XING, authorsList=Mingquan LI, Jiayuan WANG, Yajie FU, Xu SUN, Ruiqin YANG, Chuang XING, authorCompany=null, correspAuthors=Chuang XING, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322942874471510698, articleId=1322942874102411944, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=固相合成法制备类球形Silicalite-1分子筛, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

以活性炭为硬模板，采用固相合成法制备了具有类球形结构的silicalite-1分子筛。采用X射线衍射仪、BET比表面分析仪、扫描电子显微镜、透射电子显微镜、红外光谱仪、X射线光电子能谱仪等研究了活性炭用量对silicalite-1分子筛的影响。结果表明：利用活性炭表面的羟基，与硅酸形成C—O—Si键，并沿着活性炭表面生长、聚集，焙烧后形成类球形silicalite-1分子筛，其中添加10%（质量分数）活性炭所制备的类球形silicalite-1具有较高的结晶度、比表面积、孔容以及均一的颗粒尺寸。

, authors=李明权, 王佳元, 傅亚杰, 孙旭, 杨瑞芹, 邢闯, authorsList=李明权, 王佳元, 傅亚杰, 孙旭, 杨瑞芹, 邢闯, authorCompany=null, correspAuthors=邢闯, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=673e5bWB1FStRy4meUYJFg==, magXml=WrLPMPpvSnrY11wLMpJ+GQ==, pdfUrl=null, pdf=e3ItveK3FMIbaT4K/yD8FQ==, pdfFileSize=5616349, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=X71Yl274J7vv4gfNY/YgqA==, mapNumber=null, fund=null)}, authors=[Author(id=1322942876350558895, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942874102411944, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=limingquan0420@163.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1322942876426056369, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322942874102411944, authorId=1322942876350558895, language=EN, stringName=Mingquan LI, firstName=Mingquan, middleName=null, lastName=LI, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=School of Biological and Chemical Engineering, Zhejiang University of Science and Technology, Hangzhou 310023, China, bio={"content":"

LI Mingquan (1997-), male, Master candidate. E-mail: limingquan0420@163.com

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LI Mingquan (1997-), male, Master candidate. E-mail: limingquan0420@163.com

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李明权（1997—），男，硕士研究生。

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李明权（1997—），男，硕士研究生。

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