Article(id=1322942843198779836, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20210032, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1610294400000, receivedDateStr=2021-01-11, revisedDate=1614787200000, revisedDateStr=2021-03-04, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343752907, onlineDateStr=2026-10-30, pubDate=1632067200000, pubDateStr=2021-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343752907, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343752907, creator=13701087609, updateTime=1793343752907, updator=13701087609, issue=Issue{id=1322942780003201932, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='9', pageStart='1785', pageEnd='2044', issueExtLink='null', onlineDate='null', pubDate='1632067200000', pubDateStr='2021-09-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343737841, creator='13701087609', updateTime=1793345873558, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951737916665918, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951737916665919, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942780003201932, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=2009, endPage=2016, ext={EN=ArticleExt(id=1322942844981359037, articleId=1322942843198779836, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Synthesis of ZSM-5 Zeolite with High Si/Al Ratio in Ethanol System, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

ZSM-5 zeolite with a high Si/Al ratio (n(SiO₂)/n(Al₂O₃)>70) was synthesized in ethanol system via seed-assisted crystallization. The crystal form, morphology and pore structure of ZSM-5 zeolite were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results show that ZSM-5 zeolite with high crystallinity and well-dispersion can be directly synthesized in a single ethanol system when Si/Al ratio is lower than 70 and ethanol/Si ratio is 1.5. However, it is difficult to synthesize ZSM-5 zeolite with a high crystallinity in a single ethanol system when Si/Al ratio is greater than 90. Also, the addition of a small amount of seed can increase Si/Al ratio of ZSM-5 zeolite synthesized in ethanol system to 150, and shorten the crystallization induction period and overall crystallization time. The morphology of ZSM-5 zeolite in seed-assisted crystallization is different from that of ZSM-5 zeolite synthesized in seed or ethanol alone, and the grain sizes are more uniform and the dispersion is higher. The optimum ratio of alkali to silicon decreases with the increase of Si/Al ratio, but it is still necessary to provide enough alkali to dissolve silicon source for crystallization.

, authors=Jinquan TAO^{1, 2}, Yan CUI¹, Shuying ZHANG^{1, 2}, Kebin CHI¹, Yasong ZHOU², authorsList=Jinquan TAO, Yan CUI, Shuying ZHANG, Kebin CHI, Yasong ZHOU, authorCompany=null, correspAuthors=Yan CUI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322942845253988798, articleId=1322942843198779836, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=乙醇体系合成高硅铝比ZSM-5分子筛, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

在乙醇体系内合成高硅铝摩尔比[n（SiO₂）/n（Al₂O₃）>70]的ZSM-5分子筛，使用晶种辅助晶化，通过精确调整乙醇用量、晶化时间、碱硅比的条件合成出高硅铝比ZSM-5分子筛，采用X射线衍射谱、扫描电子显微镜等方式对其晶型、形貌、孔道结构进行了表征。结果表明：当硅铝比低于70，醇硅比为1.5时在单一的乙醇体系内可以直接合成出结晶度较高、分散度较好的ZSM-5分子筛，当硅铝比大于90时单一的乙醇体系中难以合成出高结晶度的ZSM-5分子筛。加入微量晶种可明显提高乙醇体系下可合成出ZSM-5分子筛的硅铝比范围至150，并且可以缩短晶化诱导期及总体晶化时间。加入晶种辅助晶化的产品ZSM-5分子筛形貌区别于单独以晶种或乙醇体系合成的ZSM-5分子筛，晶粒尺寸更加均一，且分散性更高。以晶种辅助晶化时最佳碱硅比随着硅铝比的提高有所下降，但仍需提供体系足够的碱性以溶解硅源以发生晶化反应。

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TAO Jinquan (1994-), male, Master. E-mail: 807680745@qq.com

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TAO Jinquan (1994-), male, Master. E-mail: 807680745@qq.com

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陶金泉（1994—），男，硕士研究生。

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陶金泉（1994—），男，硕士研究生。

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