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Article(id=1322942610834338369, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942592224211277, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200174, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1603814400000, receivedDateStr=2020-10-28, revisedDate=1608912000000, revisedDateStr=2020-12-26, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343697507, onlineDateStr=2026-10-30, pubDate=1621440000000, pubDateStr=2021-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343697507, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343697507, creator=13701087609, updateTime=1793343697507, updator=13701087609, issue=Issue{id=1322942592224211277, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='5', pageStart='807', pageEnd='1032', issueExtLink='null', onlineDate='null', pubDate='1621440000000', pubDateStr='2021-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343693071, creator='13701087609', updateTime=1793345545174, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950360561754466, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942592224211277, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950360565948771, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942592224211277, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1017, endPage=1024, ext={EN=ArticleExt(id=1322942611094385218, articleId=1322942610834338369, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Desulfurization Performance of One-dimensional ZnO Based Composite Desulfurizer, columnId=1319726165087077079, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Article, runingTitle=null, highlight=null, articleAbstract=

An one-dimensional (NixZn1-x)O composite desulfurizer for gasoline was prepared by an one-step composite method. The samples were characterized by X-ray diffraction, H2-temperature programmed reduction measurement, scanning electron microscopy and BET specific surface area analysis. The results show that nickel is doped into the lattice of ZnO by the one-step compounding method, which increases the force between active component nickel and ZnO and improves the active component of nickel thermodynamic stability and chemical stability, thus effectively avoiding the loss in the process of reaction and accumulation by heating during regeneration. Also, at a certain amount of nickel, (NixZn1-x)O composite desulfurizer can maintain an one-dimensional nano-morphology that favors the reduction of active component nickel in the desulfurizer for the desulfurization. At a nickel amount of 8%, (NixZn1-x)O composite desulfurizer has better desulfurization and regeneration performances, and the desulfurization rate becomes 99.0%. The service life of desulfurizer can still maintain to be 90 h after regeneration for seven times.

, authors=Shuanglin LI1, Yujia WANG1, Lei KANG1, Haiyan WANG1, Bing HAN2, authorsList=Shuanglin LI, Yujia WANG, Lei KANG, Haiyan WANG, Bing HAN, authorCompany=null, correspAuthors=Haiyan WANG, authorNote=

LI Shuanglin (1993-), male, Master candidate. E-mail:

, correspAuthorsNote=
WANG Haiyan (1962-), male, Ph.D., Professor. E-mail:
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采用一步复合法制备了一维复合型镍锌汽油脱硫剂，通过X射线衍射仪、扫描电子显微镜和BET比表面积法等对样品进行了表征。结果表明：采用一步复合法可将镍掺入ZnO的晶格中，增加了活性组分镍与ZnO之间的作用力，提高了活性组分镍的热力学稳定性和化学稳定性，进而有效避免了其在反应过程中的流失和再生过程中因受热而发生的聚集。同时通过控制镍量，可以使复合型镍锌脱硫剂保持有利于脱硫的一维纳米形貌，使得脱硫剂中活性组分镍更易于被还原。当镍含量为8%时，复合型镍锌脱硫剂具有较好的脱硫性能和再生性能，脱硫率高达99.0%，脱硫剂经过7次再生后，寿命仍可保持在90 h。

, authors=李双林1, 王钰佳1, 康蕾1, 王海彦1, 韩冰2, authorsList=李双林, 王钰佳, 康蕾, 王海彦, 韩冰, authorCompany=null, correspAuthors=王海彦, authorNote=

李双林（1993—），男，硕士研究生。

, correspAuthorsNote=
王海彦（1962—），男，博士，教授。
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LI Shuanglin (1993-), male, Master candidate. E-mail:

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LI Shuanglin (1993-), male, Master candidate. E-mail:

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李双林（1993—），男，硕士研究生。

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李双林（1993—），男，硕士研究生。

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一维氧化锌基复合脱硫剂的制备及其脱硫性能
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李双林 1 , 王钰佳 1 , 康蕾 1 , 王海彦 1 , 韩冰 2
硅酸盐学报 | 研究论文 2021,49(5): 1017-1024
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硅酸盐学报 |研究论文 2021 , 49 (5) : 1017 -1024
一维氧化锌基复合脱硫剂的制备及其脱硫性能
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李双林1 , 王钰佳1, 康蕾1, 王海彦1 , 韩冰2
作者信息
  • 1．辽宁石油化工大学石油化工学院，辽宁 抚顺 113001
  • 2．中钢集团鞍山热能研究院有限公司，辽宁 鞍山 114044
通讯作者:
王海彦（1962—），男，博士，教授。
作者简介:

李双林（1993—），男，硕士研究生。

Preparation and Desulfurization Performance of One-dimensional ZnO Based Composite Desulfurizer
Shuanglin LI1 , Yujia WANG1, Lei KANG1, Haiyan WANG1 , Bing HAN2
Affiliations
  • 1.School of Petro Chemical Engineering, Liaoning Shihua University, Fushun 113001, Liaoning, China
  • 2.Sinosteel Anshan Research Institute of Thermo-energy Co. LTD, Anshan 114044, Liaoning, China
    • Corresponding Author:
    WANG Haiyan (1962-), male, Ph.D., Professor. E-mail:

    LI Shuanglin (1993-), male, Master candidate. E-mail:

出版时间: 2021-05-20 doi: 10.14062/j.issn.0454-5648.20200174
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采用一步复合法制备了一维复合型镍锌汽油脱硫剂，通过X射线衍射仪、扫描电子显微镜和BET比表面积法等对样品进行了表征。结果表明：采用一步复合法可将镍掺入ZnO的晶格中，增加了活性组分镍与ZnO之间的作用力，提高了活性组分镍的热力学稳定性和化学稳定性，进而有效避免了其在反应过程中的流失和再生过程中因受热而发生的聚集。同时通过控制镍量，可以使复合型镍锌脱硫剂保持有利于脱硫的一维纳米形貌，使得脱硫剂中活性组分镍更易于被还原。当镍含量为8%时，复合型镍锌脱硫剂具有较好的脱硫性能和再生性能，脱硫率高达99.0%，脱硫剂经过7次再生后，寿命仍可保持在90 h。

脱硫剂  /  复合材料  /  氧化锌  /  脱硫性能  /  吸附剂

An one-dimensional (NixZn1-x)O composite desulfurizer for gasoline was prepared by an one-step composite method. The samples were characterized by X-ray diffraction, H2-temperature programmed reduction measurement, scanning electron microscopy and BET specific surface area analysis. The results show that nickel is doped into the lattice of ZnO by the one-step compounding method, which increases the force between active component nickel and ZnO and improves the active component of nickel thermodynamic stability and chemical stability, thus effectively avoiding the loss in the process of reaction and accumulation by heating during regeneration. Also, at a certain amount of nickel, (NixZn1-x)O composite desulfurizer can maintain an one-dimensional nano-morphology that favors the reduction of active component nickel in the desulfurizer for the desulfurization. At a nickel amount of 8%, (NixZn1-x)O composite desulfurizer has better desulfurization and regeneration performances, and the desulfurization rate becomes 99.0%. The service life of desulfurizer can still maintain to be 90 h after regeneration for seven times.

desulfurizer  /  composite  /  zinc oxide  /  desulfurization performance  /  absorber
李双林, 王钰佳, 康蕾, 王海彦, 韩冰. 一维氧化锌基复合脱硫剂的制备及其脱硫性能. 硅酸盐学报, 2021 , 49 (5) : 1017 -1024 . DOI: 10.14062/j.issn.0454-5648.20200174
Shuanglin LI, Yujia WANG, Lei KANG, Haiyan WANG, Bing HAN. Preparation and Desulfurization Performance of One-dimensional ZnO Based Composite Desulfurizer[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (5) : 1017 -1024 . DOI: 10.14062/j.issn.0454-5648.20200174
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  • 辽宁省教育厅青年基金项目(L2017LQN008)
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2021年第49卷第5期
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doi: 10.14062/j.issn.0454-5648.20200174
  • 接收时间：2020-10-28
  • 首发时间：2026-10-30
  • 出版时间：2021-05-20
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  • 收稿日期：2020-10-28
  • 修回日期：2020-12-26
基金
辽宁省教育厅青年基金项目(L2017LQN008)
作者信息
    1．辽宁石油化工大学石油化工学院，辽宁 抚顺 113001
    2．中钢集团鞍山热能研究院有限公司，辽宁 鞍山 114044

通讯作者:

王海彦（1962—），男，博士，教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200174
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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