Article(id=1322942551241667574, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200588, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1596729600000, receivedDateStr=2020-08-07, revisedDate=1599580800000, revisedDateStr=2020-09-09, acceptedDate=null, acceptedDateStr=null, onlineDate=1793343683299, onlineDateStr=2026-10-30, pubDate=1618848000000, pubDateStr=2021-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793343683299, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793343683299, creator=13701087609, updateTime=1793343683299, updator=13701087609, issue=Issue{id=1322942545734546372, tenantId=1146029695717560320, journalId=1263187385517883426, year='2021', volume='49', issue='4', pageStart='605', pageEnd='806', issueExtLink='null', onlineDate='null', pubDate='1618848000000', pubDateStr='2021-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793343681986, creator='13701087609', updateTime=1793345524324, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322950273110508350, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322950273110508351, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322942545734546372, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=743, endPage=748, ext={EN=ArticleExt(id=1322942551426216951, articleId=1322942551241667574, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Study on Growth and Properties of Large-sized NaCl Crystal, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

After the optimization of temperature field and the process parameters, the NaCl single crystal with the size ofФ130 mm×100 mm was grown by the resistance heating Czochralski (Cz) method and the bottom of the crucible compensation technology. XRD analysis shows that the NaCl crystal is a cubic system with a lattice constant of a=0.564 02 nm. The transmittance test of the crystal suggests that the transmittance of a sample with a thickness of 4 mm is greater than 91.5%. The vickers hardness of the crystal is 21.52 kg/mm2, and the hardness coefficient is 1.672, which proves that NaCl crystal is a soft material. The optical uniformity of the crystal decreases with the dislocation density increase. The thermoluminescence luminescence (TL) curve shows that the thermoluminescence peaks of the crystal are located at 74.35 and 221.14℃, respectively, and the luminous intensity of the latter is more than 5 times that of the former. The results show that NaCl crystal is a high-quality material, which can be used in dosimetry and infrared fields.

, authors=Yongtao LI1, Fanping MENG2, Shuo XU1, Huisheng LIU1, Xuejian ZHANG1, Jinghe LIU3, Chun LI3, Fanming ZENG3, authorsList=Yongtao LI, Fanping MENG, Shuo XU, Huisheng LIU, Xuejian ZHANG, Jinghe LIU, Chun LI, Fanming ZENG, authorCompany=null, correspAuthors=Xuejian ZHANG, Fanming ZENG, authorNote=

LI Yongtao (1989-), male, Master candidate. E-mail:

, correspAuthorsNote=
ZHANG Xuejian (1975-), male, Ph.D., Professor. E-mail:
ZENG Fanming (1976-), male, Ph.D., Professor.
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322942551715623928, articleId=1322942551241667574, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=大截面NaCl晶体的生长和性能, columnId=0, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用电阻加热Czochralski法和坩埚底部补偿技术,在优化温场和工艺参数后,生长出了Ф130 mm×100 mm的NaCl单晶。XRD分析表明,NaCl晶体为立方晶系,晶格常数为a=0.56402 nm。晶体的透光性能测试表明:厚度4 mm的样品的透过率大于91.5%;晶体的Virckers硬度为21.52 kg/mm2,硬度系数为1.672,证明NaCl晶体是一种软质材料;晶体的光学均匀性随着位错密度的增加而降低;热释光发光(TL)曲线表明,NaCl晶体的发光峰位于74.35℃和221.14℃,后者的发光强度是前者的5倍以上,表明NaCl晶体是一种可用于剂量测定和红外领域的优质材料。

, authors=李永涛1, 孟凡萍2, 徐硕1, 刘卉昇1, 张学建1, 刘景和3, 李春3, 曾繁明3, authorsList=李永涛, 孟凡萍, 徐硕, 刘卉昇, 张学建, 刘景和, 李春, 曾繁明, authorCompany=null, correspAuthors=张学建, 曾繁明, authorNote=

李永涛(1989—),男,博士。

, correspAuthorsNote=
张学建(1975—),男,教授。
曾繁明(1976—)男,教授。
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大截面NaCl晶体的生长和性能
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李永涛 1 , 孟凡萍 2 , 徐硕 1 , 刘卉昇 1 , 张学建 1 , 刘景和 3 , 李春 3 , 曾繁明 3
硅酸盐学报 | 2021,49(4): 743-748
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硅酸盐学报 | 2021 , 49 (4) : 743 -748
大截面NaCl晶体的生长和性能
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李永涛(1989—),男,博士。

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李永涛(1989—),男,博士。

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李永涛1 , 孟凡萍2, 徐硕1, 刘卉昇1, 张学建1 , 刘景和3, 李春3, 曾繁明3
作者信息
  • 1.吉林建筑大学,长春 130012
  • 2.中国兵器工业标准化研究所,北京 100089
  • 3.长春理工大学,长春 130022
通讯作者:
张学建(1975—),男,教授。
曾繁明(1976—)男,教授。
作者简介:

李永涛(1989—),男,博士。

Study on Growth and Properties of Large-sized NaCl Crystal
Yongtao LI1 , Fanping MENG2, Shuo XU1, Huisheng LIU1, Xuejian ZHANG1 , Jinghe LIU3, Chun LI3, Fanming ZENG3
Affiliations
  • 1.Jilin JianZhu Univesity, Changchun 130012, China
  • 2.China Ordnance Industry Standardization Institute, Beijing 100089, China
  • 3.Changchun University of Science and Technology, Changchun 130022, China
  • Corresponding Author:
    ZHANG Xuejian (1975-), male, Ph.D., Professor. E-mail:
    ZENG Fanming (1976-), male, Ph.D., Professor.

    LI Yongtao (1989-), male, Master candidate. E-mail:

出版时间: 2021-04-20 doi: 10.14062/j.issn.0454-5648.20200588
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采用电阻加热Czochralski法和坩埚底部补偿技术,在优化温场和工艺参数后,生长出了Ф130 mm×100 mm的NaCl单晶。XRD分析表明,NaCl晶体为立方晶系,晶格常数为a=0.56402 nm。晶体的透光性能测试表明:厚度4 mm的样品的透过率大于91.5%;晶体的Virckers硬度为21.52 kg/mm2,硬度系数为1.672,证明NaCl晶体是一种软质材料;晶体的光学均匀性随着位错密度的增加而降低;热释光发光(TL)曲线表明,NaCl晶体的发光峰位于74.35℃和221.14℃,后者的发光强度是前者的5倍以上,表明NaCl晶体是一种可用于剂量测定和红外领域的优质材料。

氯化钠  /  硬度  /  透过率  /  热释光  /  光学均匀性

After the optimization of temperature field and the process parameters, the NaCl single crystal with the size ofФ130 mm×100 mm was grown by the resistance heating Czochralski (Cz) method and the bottom of the crucible compensation technology. XRD analysis shows that the NaCl crystal is a cubic system with a lattice constant of a=0.564 02 nm. The transmittance test of the crystal suggests that the transmittance of a sample with a thickness of 4 mm is greater than 91.5%. The vickers hardness of the crystal is 21.52 kg/mm2, and the hardness coefficient is 1.672, which proves that NaCl crystal is a soft material. The optical uniformity of the crystal decreases with the dislocation density increase. The thermoluminescence luminescence (TL) curve shows that the thermoluminescence peaks of the crystal are located at 74.35 and 221.14℃, respectively, and the luminous intensity of the latter is more than 5 times that of the former. The results show that NaCl crystal is a high-quality material, which can be used in dosimetry and infrared fields.

sodium chloride  /  hardness  /  transmittance  /  thermoluminescence  /  optical uniformit
李永涛, 孟凡萍, 徐硕, 刘卉昇, 张学建, 刘景和, 李春, 曾繁明. 大截面NaCl晶体的生长和性能. 硅酸盐学报, 2021 , 49 (4) : 743 -748 . DOI: 10.14062/j.issn.0454-5648.20200588
Yongtao LI, Fanping MENG, Shuo XU, Huisheng LIU, Xuejian ZHANG, Jinghe LIU, Chun LI, Fanming ZENG. Study on Growth and Properties of Large-sized NaCl Crystal[J]. Journal of the Chinese Ceramic Society, 2021 , 49 (4) : 743 -748 . DOI: 10.14062/j.issn.0454-5648.20200588
  • 吉林省大学生创新创业训练计划(202010191150)
  • 吉林省科技厅国际合作项目(20200801038GH; 20200403158SF)
  • 吉林省教育厅科研项目(JJKH20200271KJ; JJKH20200272KJ)
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2021年第49卷第4期
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doi: 10.14062/j.issn.0454-5648.20200588
  • 接收时间:2020-08-07
  • 首发时间:2026-10-30
  • 出版时间:2021-04-20
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出版历史
  • 收稿日期:2020-08-07
  • 修回日期:2020-09-09
基金
吉林省大学生创新创业训练计划(202010191150)
吉林省科技厅国际合作项目(20200801038GH; 20200403158SF)
吉林省教育厅科研项目(JJKH20200271KJ; JJKH20200272KJ)
作者信息
    1.吉林建筑大学,长春 130012
    2.中国兵器工业标准化研究所,北京 100089
    3.长春理工大学,长春 130022

通讯作者:

张学建(1975—),男,教授。
曾繁明(1976—)男,教授。
参考文献
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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