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Article(id=1322917115992354994, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322917095268295267, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200340, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1589472000000, receivedDateStr=2020-05-15, revisedDate=1592150400000, revisedDateStr=2020-06-15, acceptedDate=null, acceptedDateStr=null, onlineDate=1793337619063, onlineDateStr=2026-10-30, pubDate=1608393600000, pubDateStr=2020-12-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793337619063, onlineIssueDateStr=2026-10-30, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793337619063, creator=13701087609, updateTime=1793337619063, updator=13701087609, issue=Issue{id=1322917095268295267, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='12', pageStart='1865', pageEnd='2010', issueExtLink='null', onlineDate='null', pubDate='1608393600000', pubDateStr='2020-12-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793337614123, creator='13701087609', updateTime=1793345927101, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322951962475507806, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322917095268295267, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322951962475507807, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322917095268295267, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1966, endPage=1975, ext={EN=ArticleExt(id=1322917118043369651, articleId=1322917115992354994, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Synthesis of NaP Zeolite Doped with Titanium and Its Adsorption Performance, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

A NaP zeolite doped with titanium (Ti-NaP) was prepared by a hydrothermal method and a complexation method using sodium silicate and sodium meta-aluminate from coal fly ash by grading extraction as raw materials based on a scientific concept of "sewage purification by solid waste". The crystal phase, morphology, and existed state of elements in NaP zeolites before and after doping titanium were characterized by X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy and solid magic angle spinning nuclear magnetic resonance of silicon and aluminum. The adsorption performance of Ti-NaP was also evaluated. The experimental results show that when n(Al2O3)∶n(TBOT)=6∶1, the crystallinity of Ti-NaP reaches 98.2%, and the existed state of titanium in NaP zeolite mainly includes the isomorphous substitution with silicon atom in the skeleton and the balance of skeletal negative charge. The specific surface area of Ti-NaP is 123 m2/g, which is approximately 3.6 times greater than that of NaP zeolite un-doped with titanium (27 m2/g). The test results of Zn(II) adsorption show that the removal rate of Zn(II) of Ti-NaP is 97.71%. Moreover, Ti-NaP still remains a good adsorption stability after 5 cycles of adsorption-regeneration.

, authors=Yanan ZHANG1, 2, Hongjing HAN1, 2, Mei ZHANG1, 2, Changxiu ZHAI3, Haiying WANG1, 2, Yanguang CHEN1, 2, Jie SUN1, 2, Xiuqi YANG1, 2, Hao WANG1, 2, authorsList=Yanan ZHANG, Hongjing HAN, Mei ZHANG, Changxiu ZHAI, Haiying WANG, Yanguang CHEN, Jie SUN, Xiuqi YANG, Hao WANG, authorCompany=null, correspAuthors=Yanguang CHEN, authorNote=

ZHANG Yanan (1993-), female, Doctorial candidate. E-mail:

, correspAuthorsNote=
CHEN Yanguang (1977-), male, Ph.D., Professor. E-mail:
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以粉煤灰分级提取的硅酸钠与偏铝酸钠为原料，提出了水热合成与络合法协同制备Ti掺杂NaP分子筛（Ti-NaP）的方法。采用X射线衍射、扫描电子显微镜、X射线光电子能谱和固体硅铝核磁（MAS NMR）对Ti掺杂NaP分子筛前后产物进行了晶相、形貌和元素赋存状态研究，并对Ti-NaP吸附性能进行评价。结果表明，当n（Al2O3）∶n（TBOT）摩尔比为6∶1时，Ti-NaP结晶度可达98.2%，且Ti在NaP分子筛中有两种主要的赋存状态：即与骨架硅原子同晶取代和平衡骨架负电荷。与未掺杂Ti的NaP分子筛相比，Ti-NaP比表面积约增大3.6倍（从27 m2/g增大至123 m2/g）。Zn（II）吸附测试表明，Ti-NaP对Zn（II）吸附去除率可达97.71%，经再生循环使用5次，仍具有良好的吸附稳定性。

, authors=张亚男1, 2, 韩洪晶1, 2, 张梅1, 2, 翟昌休3, 王海英1, 2, 陈彦广1, 2, 孙杰1, 2, 杨秀琪1, 2, 王皓1, 2, authorsList=张亚男, 韩洪晶, 张梅, 翟昌休, 王海英, 陈彦广, 孙杰, 杨秀琪, 王皓, authorCompany=null, correspAuthors=陈彦广, authorNote=

张亚男（1993—），女，博士研究生。

, correspAuthorsNote=
陈彦广（1977—），男，博士，教授。
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ZHANG Yanan (1993-), female, Doctorial candidate. E-mail:

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ZHANG Yanan (1993-), female, Doctorial candidate. E-mail:

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张亚男（1993—），女，博士研究生。

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Ti掺杂NaP分子筛的合成及其吸附性能
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张亚男 1, 2 , 韩洪晶 1, 2 , 张梅 1, 2 , 翟昌休 3 , 王海英 1, 2 , 陈彦广 1, 2 , 孙杰 1, 2 , 杨秀琪 1, 2 , 王皓 1, 2
硅酸盐学报 | 2020,48(12): 1966-1975
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硅酸盐学报 | 2020 , 48 (12) : 1966 -1975
Ti掺杂NaP分子筛的合成及其吸附性能
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张亚男（1993—），女，博士研究生。

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张亚男1, 2 , 韩洪晶1, 2, 张梅1, 2, 翟昌休3, 王海英1, 2, 陈彦广1, 2 , 孙杰1, 2, 杨秀琪1, 2, 王皓1, 2
作者信息
  • 1．东北石油大学化学化工学院，黑龙江 大庆 163318
  • 2．黑龙江省石油与天然气化工重点实验室，黑龙江 大庆 163318
  • 3．中国石油大庆化工研究中心，黑龙江 大庆 163714
通讯作者:
陈彦广（1977—），男，博士，教授。
作者简介:

张亚男（1993—），女，博士研究生。

Synthesis of NaP Zeolite Doped with Titanium and Its Adsorption Performance
Yanan ZHANG1, 2 , Hongjing HAN1, 2, Mei ZHANG1, 2, Changxiu ZHAI3, Haiying WANG1, 2, Yanguang CHEN1, 2 , Jie SUN1, 2, Xiuqi YANG1, 2, Hao WANG1, 2
Affiliations
  • 1.College of Chemistry & Chemical Engineering, Northeast Petroleum University, Daqing 163318, Heilongjiang, China
  • 2.Heilongjiang Provincial Key Laboratory of Oil and Gas Chemical Technology, Daqing 163318, Heilongjiang, China
  • 3.Daqing Petrochemical Research Center, PetroChina, Daqing 163714, Heilongjiang, China
    • Corresponding Author:
    CHEN Yanguang (1977-), male, Ph.D., Professor. E-mail:

    ZHANG Yanan (1993-), female, Doctorial candidate. E-mail:

出版时间: 2020-12-20 doi: 10.14062/j.issn.0454-5648.20200340
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以粉煤灰分级提取的硅酸钠与偏铝酸钠为原料，提出了水热合成与络合法协同制备Ti掺杂NaP分子筛（Ti-NaP）的方法。采用X射线衍射、扫描电子显微镜、X射线光电子能谱和固体硅铝核磁（MAS NMR）对Ti掺杂NaP分子筛前后产物进行了晶相、形貌和元素赋存状态研究，并对Ti-NaP吸附性能进行评价。结果表明，当n（Al2O3）∶n（TBOT）摩尔比为6∶1时，Ti-NaP结晶度可达98.2%，且Ti在NaP分子筛中有两种主要的赋存状态：即与骨架硅原子同晶取代和平衡骨架负电荷。与未掺杂Ti的NaP分子筛相比，Ti-NaP比表面积约增大3.6倍（从27 m2/g增大至123 m2/g）。Zn（II）吸附测试表明，Ti-NaP对Zn（II）吸附去除率可达97.71%，经再生循环使用5次，仍具有良好的吸附稳定性。

粉煤灰  /  NaP分子筛  /  钛掺杂  /  络合  /  吸附性能

A NaP zeolite doped with titanium (Ti-NaP) was prepared by a hydrothermal method and a complexation method using sodium silicate and sodium meta-aluminate from coal fly ash by grading extraction as raw materials based on a scientific concept of "sewage purification by solid waste". The crystal phase, morphology, and existed state of elements in NaP zeolites before and after doping titanium were characterized by X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy and solid magic angle spinning nuclear magnetic resonance of silicon and aluminum. The adsorption performance of Ti-NaP was also evaluated. The experimental results show that when n(Al2O3)∶n(TBOT)=6∶1, the crystallinity of Ti-NaP reaches 98.2%, and the existed state of titanium in NaP zeolite mainly includes the isomorphous substitution with silicon atom in the skeleton and the balance of skeletal negative charge. The specific surface area of Ti-NaP is 123 m2/g, which is approximately 3.6 times greater than that of NaP zeolite un-doped with titanium (27 m2/g). The test results of Zn(II) adsorption show that the removal rate of Zn(II) of Ti-NaP is 97.71%. Moreover, Ti-NaP still remains a good adsorption stability after 5 cycles of adsorption-regeneration.

coal fly ash  /  NaP zeolite  /  titanium-doping  /  complexation  /  adsorption performance
张亚男, 韩洪晶, 张梅, 翟昌休, 王海英, 陈彦广, 孙杰, 杨秀琪, 王皓. Ti掺杂NaP分子筛的合成及其吸附性能. 硅酸盐学报, 2020 , 48 (12) : 1966 -1975 . DOI: 10.14062/j.issn.0454-5648.20200340
Yanan ZHANG, Hongjing HAN, Mei ZHANG, Changxiu ZHAI, Haiying WANG, Yanguang CHEN, Jie SUN, Xiuqi YANG, Hao WANG. Synthesis of NaP Zeolite Doped with Titanium and Its Adsorption Performance[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (12) : 1966 -1975 . DOI: 10.14062/j.issn.0454-5648.20200340
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  • 国家自然科学基金(51674089; 21908021)
  • 黑龙江省杰出青年基金(JC2018002)
  • 东北石油大学研究生创新项目(JYCX_CX03_2018)
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2020年第48卷第12期
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doi: 10.14062/j.issn.0454-5648.20200340
  • 接收时间：2020-05-15
  • 首发时间：2026-10-30
  • 出版时间：2020-12-20
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  • 收稿日期：2020-05-15
  • 修回日期：2020-06-15
基金
国家自然科学基金(51674089; 21908021)
黑龙江省杰出青年基金(JC2018002)
东北石油大学研究生创新项目(JYCX_CX03_2018)
作者信息
    1．东北石油大学化学化工学院，黑龙江 大庆 163318
    2．黑龙江省石油与天然气化工重点实验室，黑龙江 大庆 163318
    3．中国石油大庆化工研究中心，黑龙江 大庆 163714

通讯作者:

陈彦广（1977—），男，博士，教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200340
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
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红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
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