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Article(id=1322636333940588907, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636274364698818, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200300, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1587916800000, receivedDateStr=2020-04-27, revisedDate=1590508800000, revisedDateStr=2020-05-27, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270675406, onlineDateStr=2026-10-29, pubDate=1605801600000, pubDateStr=2020-11-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270675406, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270675406, creator=13701087609, updateTime=1793270675406, updator=13701087609, issue=Issue{id=1322636274364698818, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='11', pageStart='1689', pageEnd='1864', issueExtLink='null', onlineDate='null', pubDate='1605801600000', pubDateStr='2020-11-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270661202, creator='13701087609', updateTime=1793277186220, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663642319930111, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636274364698818, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663642319930112, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636274364698818, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1824, endPage=1833, ext={EN=ArticleExt(id=1322636334154498412, articleId=1322636333940588907, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Composition Optimization and Strength Decline Mechanism of Oil Well Cement Slurry at 200 ℃, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

The influence of adding crystalline silica and silica fume on the mineral composition and physical-mechanical properties of the set-cement was investigated. The results show that optimizing the particle size distribution of cement dry blend can improve the 7-d compressive strength. Increasing the total silica addition can enhance the 30-d compressive strength. At 30-d curing, two optimized systems have an average compressive strength of greater than 40 MPa and a water permeability of lower than 2×10-6 μm2. The physical, mechanical, mineral and microstructual property evolution of the two systems within 30 d were analyzed. It is indicated that there are little changes in the mineral compositions and their crystallinity during 7-30 d. However, apparent microstructure coarsening occurs, leading to the decline in compressive strength and modulus of elasticity as well as the almost linear increase in water permeability of the set cement as a function of time.

, authors=Ning LI1, Xueyu PANG2, 3, Zhengqing AI1, Jiankun QIN3, Zhongfei LIU1, Honglu WANG3, Yindong WANG1, authorsList=Ning LI, Xueyu PANG, Zhengqing AI, Jiankun QIN, Zhongfei LIU, Honglu WANG, Yindong WANG, authorCompany=null, correspAuthors=Xueyu PANG, authorNote=

LI Ning (1970-), male, Senior Engineer. E-mail:

, correspAuthorsNote=
PANG Xueyu (1982-), male, Ph.D., Professor. E-mail:
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通过研究200 ℃超高温环境下2种不同目数硅砂以及微硅等外掺料加量和配比对水泥石矿物成分及物理力学性能的影响，发现优化颗粒级配可以显著提高水泥石7 d抗压强度，同时提高SiO2总加量可以明显改善30 d长期强度。经过优化后的2套配方30 d抗压强度达到40 MPa以上，水测渗透率低于2×10-6 μm2。通过分析该两套配方物理力学性能在30 d内物理力学性能及微观结构成分随养护时间的演化规律，发现水泥石矿物成分及矿物结晶状态在7 d至30 d基本没有变化，但微观结构有粗化现象，从而导致其抗压强度、弹性模量等力学性能随时间降低，水测渗透率随时间近乎线性增长。

, authors=李宁1, 庞学玉2, 3, 艾正青1, 秦建鲲3, 刘忠飞1, 王洪路3, 王银东1, authorsList=李宁, 庞学玉, 艾正青, 秦建鲲, 刘忠飞, 王洪路, 王银东, authorCompany=null, correspAuthors=庞学玉, authorNote=

李宁（1970—），男，高级工程师。

, correspAuthorsNote=
庞学玉（1982—），男，博士，教授。
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LI Ning (1970-), male, Senior Engineer. E-mail:

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李宁（1970—），男，高级工程师。

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200 ℃加砂硅酸盐水泥配方优化设计及强度衰退机理
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李宁 1 , 庞学玉 2, 3 , 艾正青 1 , 秦建鲲 3 , 刘忠飞 1 , 王洪路 3 , 王银东 1
硅酸盐学报 | 研究论文 2020,48(11): 1824-1833
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硅酸盐学报 |研究论文 2020 , 48 (11) : 1824 -1833
200 ℃加砂硅酸盐水泥配方优化设计及强度衰退机理
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李宁1 , 庞学玉2, 3 , 艾正青1, 秦建鲲3, 刘忠飞1, 王洪路3, 王银东1
作者信息
  • 1．中石油塔里木油田分公司油气工程研究院，新疆 库尔勒 841000
  • 2．非常规油气开发教育部重点实验室，中国石油大学（华东），山东 青岛 266580
  • 3．中国石油大学（华东）石油工程学院，山东 青岛 266580
通讯作者:
庞学玉（1982—），男，博士，教授。
作者简介:

李宁（1970—），男，高级工程师。

Composition Optimization and Strength Decline Mechanism of Oil Well Cement Slurry at 200 ℃
Ning LI1 , Xueyu PANG2, 3 , Zhengqing AI1, Jiankun QIN3, Zhongfei LIU1, Honglu WANG3, Yindong WANG1
Affiliations
  • 1.Oil and Gas Engineering Research Institute, Petro China Tarim Oilfield Company, Korla 841000, Xinjiang, China
  • 2.Key Laboratory of Unconventional Oil & Gas Development, China University of Petroleum (East China), Ministry of Education, Qingdao 266580, Shandong, China
  • 3.School of Petroleum Engineering, China University of Petroleum (East China), Qingdao 266580, Shandong, China
    • Corresponding Author:
    PANG Xueyu (1982-), male, Ph.D., Professor. E-mail:

    LI Ning (1970-), male, Senior Engineer. E-mail:

出版时间: 2020-11-20 doi: 10.14062/j.issn.0454-5648.20200300
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摘要
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通过研究200 ℃超高温环境下2种不同目数硅砂以及微硅等外掺料加量和配比对水泥石矿物成分及物理力学性能的影响，发现优化颗粒级配可以显著提高水泥石7 d抗压强度，同时提高SiO2总加量可以明显改善30 d长期强度。经过优化后的2套配方30 d抗压强度达到40 MPa以上，水测渗透率低于2×10-6 μm2。通过分析该两套配方物理力学性能在30 d内物理力学性能及微观结构成分随养护时间的演化规律，发现水泥石矿物成分及矿物结晶状态在7 d至30 d基本没有变化，但微观结构有粗化现象，从而导致其抗压强度、弹性模量等力学性能随时间降低，水测渗透率随时间近乎线性增长。

高温  /  高压  /  强度衰退  /  水测渗透率  /  气测渗透率  /  弹性模量  /  Poisson比  /  物相分析

The influence of adding crystalline silica and silica fume on the mineral composition and physical-mechanical properties of the set-cement was investigated. The results show that optimizing the particle size distribution of cement dry blend can improve the 7-d compressive strength. Increasing the total silica addition can enhance the 30-d compressive strength. At 30-d curing, two optimized systems have an average compressive strength of greater than 40 MPa and a water permeability of lower than 2×10-6 μm2. The physical, mechanical, mineral and microstructual property evolution of the two systems within 30 d were analyzed. It is indicated that there are little changes in the mineral compositions and their crystallinity during 7-30 d. However, apparent microstructure coarsening occurs, leading to the decline in compressive strength and modulus of elasticity as well as the almost linear increase in water permeability of the set cement as a function of time.

high temperature  /  high pressure  /  strength retrogression  /  water permeability  /  gas permeability  /  modulus of elasticity  /  Poisson's ratio  /  phase analysis
李宁, 庞学玉, 艾正青, 秦建鲲, 刘忠飞, 王洪路, 王银东. 200 ℃加砂硅酸盐水泥配方优化设计及强度衰退机理. 硅酸盐学报, 2020 , 48 (11) : 1824 -1833 . DOI: 10.14062/j.issn.0454-5648.20200300
Ning LI, Xueyu PANG, Zhengqing AI, Jiankun QIN, Zhongfei LIU, Honglu WANG, Yindong WANG. Composition Optimization and Strength Decline Mechanism of Oil Well Cement Slurry at 200 ℃[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (11) : 1824 -1833 . DOI: 10.14062/j.issn.0454-5648.20200300
基金
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  • 国家自然科学基金项目“油井水泥水化动力学实验研究及数值模拟”(51974352)
  • 中石油重大专项2018E-1808“超深进钻井提速提质关键技术研究与应用”
  • 中石油塔里木油田“200 ℃超高温水泥石长期强度稳定研究与应用”
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2020年第48卷第11期
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文章信息
doi: 10.14062/j.issn.0454-5648.20200300
  • 接收时间：2020-04-27
  • 首发时间：2026-10-29
  • 出版时间：2020-11-20
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  • 收稿日期：2020-04-27
  • 修回日期：2020-05-27
基金
国家自然科学基金项目“油井水泥水化动力学实验研究及数值模拟”(51974352)
中石油重大专项2018E-1808“超深进钻井提速提质关键技术研究与应用”
中石油塔里木油田“200 ℃超高温水泥石长期强度稳定研究与应用”
作者信息
    1．中石油塔里木油田分公司油气工程研究院，新疆 库尔勒 841000
    2．非常规油气开发教育部重点实验室，中国石油大学（华东），山东 青岛 266580
    3．中国石油大学（华东）石油工程学院，山东 青岛 266580

通讯作者:

庞学玉（1982—），男，博士，教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200300
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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