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Article(id=1322636298217705859, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636274364698818, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200072, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1581609600000, receivedDateStr=2020-02-14, revisedDate=1585843200000, revisedDateStr=2020-04-03, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270666889, onlineDateStr=2026-10-29, pubDate=1605801600000, pubDateStr=2020-11-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270666889, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270666889, creator=13701087609, updateTime=1793270666889, updator=13701087609, issue=Issue{id=1322636274364698818, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='11', pageStart='1689', pageEnd='1864', issueExtLink='null', onlineDate='null', pubDate='1605801600000', pubDateStr='2020-11-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270661202, creator='13701087609', updateTime=1793277186220, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663642319930111, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636274364698818, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663642319930112, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636274364698818, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1834, endPage=1841, ext={EN=ArticleExt(id=1322636298876211588, articleId=1322636298217705859, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Anti-Clay Property and Action Principle of Polycarboxylate Superplasticizer Improved by Cationic Polymer, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

A series of cationic sacrificial agents (CSA) were synthesized via free radical copolymerization of unsaturated quaternary ammonium salt monomer and unsaturated nonionic (anion) monomer. The effect of sacrificial agent on the dispersion of polycarboxylate superplasticizer in cement mixed with montmorillonite (MMT) was evaluated via the fluidity of cement paste. Also, the effects of monomer polymerization ratio, quaternary ammonium salt monomer type and nonionic (anionic) monomer type on the action effect of the sacrificial agent were investigated by organic carbon analysis, thermogravimetry, X-ray diffraction, and scanning electron microscopy. Trimethyl allyl ammonium bromide-acrylamide (ATMA-AM 2∶1) was determined as an optimum structure, and its action mechanism was also analyzed. The fluidity of PCE in cement paste mixed with MMT increases from 156 mm to 225 mm at 1.0% of ATMA-AM (2∶1). The adsorption capacity of PCE on MMT and the holes on the surface of MMT all reduce, thus effectively preventing the polyether side chain of PCE molecule from entering the interlayer of MMT and enhancing MMT effect on the dispersion property of PCE.

, authors=Nanxiao GAO1, 2, Jian CHEN1, 2, 3, Shuang ZHAO1, 2, Min QIAO1, 2, 3, Guangcheng SHAN1, 2, authorsList=Nanxiao GAO, Jian CHEN, Shuang ZHAO, Min QIAO, Guangcheng SHAN, authorCompany=null, correspAuthors=Min QIAO, authorNote=

GAO Nanxiao (1984-), female, Master, Senior Engineer. E-mail:

, correspAuthorsNote=
QIAO Min (1984-), male, Ph.D., Senior Engineer. E-mail:
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以不饱和季铵盐单体与不饱和非（阴）离子单体进行水溶液自由基共聚，合成了系列阳离子聚合物型牺牲剂（CSA）。采用水泥净浆流动度来评价牺牲剂对加蒙脱土水泥中聚羧酸减水剂（PCE）分散性能的影响。结合有机碳吸附、热重分析、X射线衍射等测试手段，不仅考察了聚合单体比例、季铵盐单体种类、非（阴）离子单体种类对牺牲剂作用效果的影响，确定了三甲基烯丙基溴化铵-丙烯酰胺（ATMA-AM 2∶1）为最佳结构，同时也探明了其作用原理。加入ATMA-AM（2∶1）后，有效阻止了PCE分子聚醚侧链进入到蒙脱土层间，显著降低了PCE分子在蒙脱土上的吸附量，增加了其在水泥颗粒上的有效吸附，掺蒙脱土水泥中PCE的流动度由156 mm提升至225 mm，显著改善了蒙脱土对PCE分散性能带来的负面影响。

, authors=高南箫1, 2, 陈健1, 2, 3, 赵爽1, 2, 乔敏1, 2, 3, 单广程1, 2, authorsList=高南箫, 陈健, 赵爽, 乔敏, 单广程, authorCompany=null, correspAuthors=乔敏, authorNote=

高南箫（1984—），女，硕士，高级工程师。

, correspAuthorsNote=
乔敏（1984—），男，博士，高级工程师。
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高南箫（1984—），女，硕士，高级工程师。

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阳离子聚合物改善聚羧酸减水剂抗泥性能及作用原理
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高南箫 1, 2 , 陈健 1, 2, 3 , 赵爽 1, 2 , 乔敏 1, 2, 3 , 单广程 1, 2
硅酸盐学报 | 研究论文 2020,48(11): 1834-1841
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硅酸盐学报 |研究论文 2020 , 48 (11) : 1834 -1841
阳离子聚合物改善聚羧酸减水剂抗泥性能及作用原理
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高南箫1, 2 , 陈健1, 2, 3, 赵爽1, 2, 乔敏1, 2, 3 , 单广程1, 2
作者信息
  • 1．高性能土木工程材料国家重点实验室，南京 210003
  • 2．江苏苏博特新材料股份有限公司，南京 210003
  • 3．博特新材料泰州有限公司，江苏 泰州 225474
通讯作者:
乔敏（1984—），男，博士，高级工程师。
作者简介:

高南箫（1984—），女，硕士，高级工程师。

Anti-Clay Property and Action Principle of Polycarboxylate Superplasticizer Improved by Cationic Polymer
Nanxiao GAO1, 2 , Jian CHEN1, 2, 3, Shuang ZHAO1, 2, Min QIAO1, 2, 3 , Guangcheng SHAN1, 2
Affiliations
  • 1.State Key Laboratory of High Performance Civil Engineering Materials, Nanjing 211103, China
  • 2.Jiangsu Sobute New Materials Co. Ltd., Nanjing 211103, China
  • 3.Bote New Materials Taizhou Co., Ltd., Taizhou 225474, Jiangsu, China
    • Corresponding Author:
    QIAO Min (1984-), male, Ph.D., Senior Engineer. E-mail:

    GAO Nanxiao (1984-), female, Master, Senior Engineer. E-mail:

出版时间: 2020-11-20 doi: 10.14062/j.issn.0454-5648.20200072
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以不饱和季铵盐单体与不饱和非（阴）离子单体进行水溶液自由基共聚，合成了系列阳离子聚合物型牺牲剂（CSA）。采用水泥净浆流动度来评价牺牲剂对加蒙脱土水泥中聚羧酸减水剂（PCE）分散性能的影响。结合有机碳吸附、热重分析、X射线衍射等测试手段，不仅考察了聚合单体比例、季铵盐单体种类、非（阴）离子单体种类对牺牲剂作用效果的影响，确定了三甲基烯丙基溴化铵-丙烯酰胺（ATMA-AM 2∶1）为最佳结构，同时也探明了其作用原理。加入ATMA-AM（2∶1）后，有效阻止了PCE分子聚醚侧链进入到蒙脱土层间，显著降低了PCE分子在蒙脱土上的吸附量，增加了其在水泥颗粒上的有效吸附，掺蒙脱土水泥中PCE的流动度由156 mm提升至225 mm，显著改善了蒙脱土对PCE分散性能带来的负面影响。

阳离子聚合物  /  牺牲剂  /  聚羧酸减水剂  /  蒙脱土  /  吸附  /  插层

A series of cationic sacrificial agents (CSA) were synthesized via free radical copolymerization of unsaturated quaternary ammonium salt monomer and unsaturated nonionic (anion) monomer. The effect of sacrificial agent on the dispersion of polycarboxylate superplasticizer in cement mixed with montmorillonite (MMT) was evaluated via the fluidity of cement paste. Also, the effects of monomer polymerization ratio, quaternary ammonium salt monomer type and nonionic (anionic) monomer type on the action effect of the sacrificial agent were investigated by organic carbon analysis, thermogravimetry, X-ray diffraction, and scanning electron microscopy. Trimethyl allyl ammonium bromide-acrylamide (ATMA-AM 2∶1) was determined as an optimum structure, and its action mechanism was also analyzed. The fluidity of PCE in cement paste mixed with MMT increases from 156 mm to 225 mm at 1.0% of ATMA-AM (2∶1). The adsorption capacity of PCE on MMT and the holes on the surface of MMT all reduce, thus effectively preventing the polyether side chain of PCE molecule from entering the interlayer of MMT and enhancing MMT effect on the dispersion property of PCE.

cationic polymer  /  sacrificial agent  /  polycarboxylate superplasticizer  /  montmorillonite  /  adsorption  /  intercalation
高南箫, 陈健, 赵爽, 乔敏, 单广程. 阳离子聚合物改善聚羧酸减水剂抗泥性能及作用原理. 硅酸盐学报, 2020 , 48 (11) : 1834 -1841 . DOI: 10.14062/j.issn.0454-5648.20200072
Nanxiao GAO, Jian CHEN, Shuang ZHAO, Min QIAO, Guangcheng SHAN. Anti-Clay Property and Action Principle of Polycarboxylate Superplasticizer Improved by Cationic Polymer[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (11) : 1834 -1841 . DOI: 10.14062/j.issn.0454-5648.20200072
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  • 国家重点研发计划(2017YFB0310100)
  • 国家自然科学基金杰出青年基金(51825203)
  • 江苏省第十五批六大人才高峰项目(JZ-058)
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2020年第48卷第11期
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doi: 10.14062/j.issn.0454-5648.20200072
  • 接收时间：2020-02-14
  • 首发时间：2026-10-29
  • 出版时间：2020-11-20
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  • 收稿日期：2020-02-14
  • 修回日期：2020-04-03
基金
国家重点研发计划(2017YFB0310100)
国家自然科学基金杰出青年基金(51825203)
江苏省第十五批六大人才高峰项目(JZ-058)
作者信息
    1．高性能土木工程材料国家重点实验室，南京 210003
    2．江苏苏博特新材料股份有限公司，南京 210003
    3．博特新材料泰州有限公司，江苏 泰州 225474

通讯作者:

乔敏（1984—），男，博士，高级工程师。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20200072
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
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