Article(id=1322636268475888317, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190704, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1572192000000, receivedDateStr=2019-10-28, revisedDate=1575129600000, revisedDateStr=2019-12-01, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270659797, onlineDateStr=2026-10-29, pubDate=1603123200000, pubDateStr=2020-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270659797, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270659797, creator=13701087609, updateTime=1793270659797, updator=13701087609, issue=Issue{id=1322636234858550134, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='10', pageStart='1505', pageEnd='1688', issueExtLink='null', onlineDate='null', pubDate='1603123200000', pubDateStr='2020-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270651783, creator='13701087609', updateTime=1793277146795, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663476976267430, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663476976267431, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1604, endPage=1612, ext={EN=ArticleExt(id=1322636270040363710, articleId=1322636268475888317, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Effect of P₂O₅ on Properties and Structure of Phase-Separated Opaque Glaze in (K,Na)₂O-CaO-Al₂O₃-B₂O₃-SiO₂ System, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

P₂O₅ was added into (K,Na)₂O-CaO-Al₂O₃-B₂O₃-SiO₂ phase-separated opaque glaze. Effect of P₂O₅ on the glaze properties and structure was investigated by thermal expansion instrument, colorimeter, Vickers hardness tester, scanning electron microscopy, transmission electron microscopy and Fourier transform infrared spectroscopy, respectively. The results show that the glaze whiteness and the Vickers hardness improve as P₂O₅ content increases. The whiteness of the glaze increases from 46.58% to 71.79% and the Vickers hardness increases from 737.94 HV to 1153.03 HV. [PO₄] obtains the bridge oxygen of [BO₄] from the matrix glass phase, promoting the phase separation of the glaze melt by changing [BO₄] to [BO₃] when the mole fraction of P₂O₅ is below 0.58%. Also, P₂O₅ mostly appears in the boron-rich phase separation droplets. The interface between the droplets phase and the matrix phase provides conditions for hexagonal prism shape of Ca₃(PO₄)₂ crystal separated from the glaze, the refractive index difference between heterogeneous particles and matrix phase increases, and Ca₃(PO₄)₂ crystal size is in the visible wavelength range when the mole fraction of P₂O₅ is 1.15%-1.72%, which enhances the Mie scattering and improves the glaze whiteness. In addition, the Vickers hardness of the glaze improves because the density of the glass structure increases with increasing [PO₄] content.

, authors=Ruiqiang YANG, Yongqing WANG, Jian'er ZHOU, Qibing CHANG, Weixia DONG, Qifu BAO, Kun LIU, Peng TONG, authorsList=Ruiqiang YANG, Yongqing WANG, Jian'er ZHOU, Qibing CHANG, Weixia DONG, Qifu BAO, Kun LIU, Peng TONG, authorCompany=null, correspAuthors=Yongqing WANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322636270279439039, articleId=1322636268475888317, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=P₂O₅对（K，Na）₂O-CaO-Al₂O₃-B₂O₃-SiO₂系分相乳浊釉性能及结构的影响, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

在（K，Na）₂O-CaO-Al₂O₃-B₂O₃-SiO₂分相乳浊釉中引入P₂O₅，用热膨胀仪、色度仪、维氏硬度计、扫描电子显微镜、透射电子显微镜、红外光谱等测试方法探究其对釉面性能及釉玻璃结构的影响。结果表明：釉面白度和维氏硬度随P₂O₅引入量的增加而显著提高，白度由46.58%提高至71.79%，维氏硬度由737.94 HV提高至1153.03 HV；在P₂O₅组分引入量较低时（0.58%，摩尔分数，下同），[PO₄]易夺取基质玻璃相中[BO₄]的桥氧促使[BO₄]向[BO₃]转变，促进釉熔体分相，此时P₂O₅多存在于富硼分相液滴中。当P₂O₅组分引入量较高时（1.15%~1.72%），液滴相与基质相之间的界面为釉中晶体成核提供条件，釉中析出六棱柱形Ca₃（PO₄）₂晶体，异相粒子与基质相之间的折射率差值提高，且Ca₃（PO₄）₂晶体尺寸在可见光波长范围内，Mie散射作用加强，釉面白度提升；同时，釉玻璃结构的致密度随[PO₄]含量的增加而提升，促使釉面维氏硬度提高。

, authors=杨瑞强, 汪永清, 周健儿, 常启兵, 董伟霞, 包启富, 刘昆, 童彭, authorsList=杨瑞强, 汪永清, 周健儿, 常启兵, 董伟霞, 包启富, 刘昆, 童彭, authorCompany=null, correspAuthors=汪永清, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=xTomaS/01JerrpiAgweBxA==, magXml=NfGQFhvvBjCSrXEdguMDbw==, pdfUrl=null, pdf=HpEymomqv3EX0W0Ys7OLZw==, pdfFileSize=1832736, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=9nFMWMyy/A/aL62G64xyyA==, mapNumber=null, fund=null)}, authors=[Author(id=1322934401516052531, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322636268475888317, orderNo=0, firstName=null, middleName=null, lastName=null, nameCn=null, orcid=null, stid=null, country=null, authorPic=null, dead=0, email=yrq1117@126.com, emailSecond=null, emailThird=null, correspondingAuthor=0, authorType=1, ext={EN=AuthorExt(id=1322934401591550005, tenantId=1146029695717560320, journalId=1263187385517883426, articleId=1322636268475888317, authorId=1322934401516052531, language=EN, stringName=Ruiqiang YANG, firstName=Ruiqiang, middleName=null, lastName=YANG, prefix=null, suffix=null, authorComment=null, nameInitials=null, affiliation=null, department=null, xref=null, address=School of Materials Science and Engineering, Jingdezhen Ceramic Institute, Jingdezhen 333001, Jiangxi, China, bio={"content":"

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YANG Ruiqiang (1991-), male, Doctoral candidate. E-mail: yrq1117@126.com

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杨瑞强（1991—），男，博士研究生。

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杨瑞强（1991—），男，博士研究生。

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