Article(id=1322636252927610890, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200103, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1582560000000, receivedDateStr=2020-02-25, revisedDate=1586361600000, revisedDateStr=2020-04-09, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270656090, onlineDateStr=2026-10-29, pubDate=1603123200000, pubDateStr=2020-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270656090, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270656090, creator=13701087609, updateTime=1793270656090, updator=13701087609, issue=Issue{id=1322636234858550134, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='10', pageStart='1505', pageEnd='1688', issueExtLink='null', onlineDate='null', pubDate='1603123200000', pubDateStr='2020-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270651783, creator='13701087609', updateTime=1793277146795, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663476976267430, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663476976267431, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1574, endPage=1580, ext={EN=ArticleExt(id=1322636253107965963, articleId=1322636252927610890, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of ZnO Photoanode for Dye-Sensitized Solar Cell by Pyrolysis of Metal-Organic Framework-5, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=
Hexagonal ZnO with different average particle sizes and crystallinities were synthesized via pyrolysis of metal-organic framework-5 (MOF-5) at various temperatures. ZnO pastes were prepared, and then ZnO photoanodes were obtained by a doctor blade method, thus assembling into dye-sensitized solar cells (DSSC). The phase composition and morphology of MOF-5, ZnO nanoparticles, and ZnO photoanode were characterized by X-ray diffraction and scanning electronic microscopy, and the effects of ZnO nanoparticle morphology and photoanode thickness on the properties of DSSC were investigated. The average particle size and crystallinity of ZnO nanoparticles increase with increasing the calcination temperature for MOF-5. ZnO nanoparticles with a small particle size have a great specific surface area, and the prepared photoanode has a large amount of dye adsorption, which is conducive to obtaining DSSC with a high photoelectric conversion efficiency. However, the crystallinity is low as ZnO nanoparticles are rather small, thus decreasing the efficiency of DSSC. The optimum efficiency of DSSC is obtained at the average size of ZnO nanoparticles of 65.5 nm. The optimum efficiency of DSSC is 3.86% at the optimal thickness of photoanode of 48 μm.
, authors=Pingchun GUO, Mengmeng SONG, Hua ZHU, Jiake LI, Yanxiang WANG, authorsList=Pingchun GUO, Mengmeng SONG, Hua ZHU, Jiake LI, Yanxiang WANG, authorCompany=null, correspAuthors=null, authorNote=
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在不同温度下热分解金属-有机框架-5（MOF-5），制备不同平均粒径、不同结晶度的六方纤锌结构纳米ZnO，通过刮刀法将制备所得ZnO浆料制备成ZnO光阳极薄膜，并组装成染料敏化太阳能电池（DSSC）。采用X射线衍射仪和扫描电子显微镜对合成的MOF-5、ZnO纳米粒和ZnO光阳极薄膜的物相和形貌进行表征，研究了ZnO纳米粒形貌和光阳极厚度对电池性能的影响。结果表明：MOF-5的煅烧温度越高，获得的ZnO纳米粒粒径越大，结晶度越高。ZnO纳米粒粒径越小，比表面积越大，制备的光阳极膜染料吸附量越大，DSSC的光电转换效率越高。然而，如果ZnO纳米粒粒径过小，结晶度太低，则会降低电池的光电转换效率。当ZnO纳米粒平均粒径为65.5 nm，制备所得的电池效率最高；通过优化光阳极膜厚度，可进一步提高电池效率，当厚度为48 μm时电池效率最高，为3.86%。
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