Article(id=1322636245818266577, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200071, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1581609600000, receivedDateStr=2020-02-14, revisedDate=1585324800000, revisedDateStr=2020-03-28, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270654395, onlineDateStr=2026-10-29, pubDate=1603123200000, pubDateStr=2020-10-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270654395, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270654395, creator=13701087609, updateTime=1793270654395, updator=13701087609, issue=Issue{id=1322636234858550134, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='10', pageStart='1505', pageEnd='1688', issueExtLink='null', onlineDate='null', pubDate='1603123200000', pubDateStr='2020-10-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270651783, creator='13701087609', updateTime=1793277146795, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663476976267430, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663476976267431, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636234858550134, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1589, endPage=1596, ext={EN=ArticleExt(id=1322636247416296402, articleId=1322636245818266577, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation of Crystalline Silicon by Magnesiothermic Reduction Combined Acid Etching Routes from Silica Fume, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Silica fume (SF, containing SiO₂>85%, in mass fraction) collected from emitting soot of silicon-metallurgical workshop was used as a raw material for preparation of pure crystalline silicon. Silicon was prepared via refining pretreatment of pristine SF and ball-milling mixing to make magnesium and SF powder reactant, subsequent magnesiothermic reduction reaction (MRR) process and final purification by two-step acid-etching treatment of HCl-HF acids. The experimental results show that a core-shell structure Mg@SiO₂, i.e., Mg particles coated uniformly by a dense layer of submicron-sized primary particles of silica fume in a desired stoichiometric ratio of reactants Mg:SiO₂ of 0.85∶1.00, is formed via micron-scale diffusion reaction after mixing for 12 h at a rotational speed of 150 r/min. A high-performance route of MRR was proposed based on the wrapping-micron-reactor model. The extent of MRR is as high as 96% and Si species of HCl-etched sample are more than 90% (in mass fraction), and the final prepared product of crystalline silicon achieves a purity of 99.88% (in mass fraction) after HF+CH₃COOH acid-etching.

, authors=Yongcheng HUANG¹, Zhining CHEN¹, Lin ZHANG¹, Xiao REN¹, Yuzhong GUO¹, Ruian HUANG², Bin LI³, authorsList=Yongcheng HUANG, Zhining CHEN, Lin ZHANG, Xiao REN, Yuzhong GUO, Ruian HUANG, Bin LI, authorCompany=null, correspAuthors=Yuzhong GUO, Ruian HUANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322636247600845779, articleId=1322636245818266577, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=采用镁热还原-复合酸浸法从微硅粉制备晶体硅, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用硅冶金工业烟尘副产物微硅粉[含SiO₂>85%（质量分数）]为原料，经预处理提纯、镁粉-微硅粉球磨混料、镁热还原处理后，再以HCl-HF两步酸浸除杂工艺来制备晶体硅。结果表明：经150 r/min球磨混合12 h后，镁球表面均匀包覆了一层致密的SiO₂初级粒子层，形成了氧化硅和镁反应物料的近乎理想配比（Mg/SiO₂质量比为0.85∶1.00），和仅需微米尺度扩散的Mg@SiO₂核壳结构；提出了基于包裹-微反应器模型的高效镁热还原路线。球磨包裹物料Mg@SiO₂经镁热还原、HCl浸蚀后，产物还原程度高达96%，Si相组成大于90%（质量分数）；再经HF+CH₃COOH酸浸纯化，可制得纯度达99.88%（质量分数）的晶体硅。

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HUANG Yongcheng (1994-), male, Master candidate. E-mail: 982634899@qq.com

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HUANG Yongcheng (1994-), male, Master candidate. E-mail: 982634899@qq.com

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黄永成（1994—），男，硕士研究生。

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黄永成（1994—），男，硕士研究生。

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