Article(id=1322636225933071160, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636193100050547, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190733, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1573142400000, receivedDateStr=2019-11-08, revisedDate=1577203200000, revisedDateStr=2019-12-25, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270649655, onlineDateStr=2026-10-29, pubDate=1600531200000, pubDateStr=2020-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270649655, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270649655, creator=13701087609, updateTime=1793270649655, updator=13701087609, issue=Issue{id=1322636193100050547, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='9', pageStart='1353', pageEnd='1510', issueExtLink='null', onlineDate='null', pubDate='1594569600000', pubDateStr='2020-07-13', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270641826, creator='13701087609', updateTime=1793270641826, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=1505, endPage=1510, ext={EN=ArticleExt(id=1322636226109231929, articleId=1322636225933071160, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Evaluation of Creep Results of Silica Brick by Creep Test Method, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Industrial silica bricks were obtained in tunnel kiln by sintering at 1450 ℃ with crystalline silica as a raw material, and lime milk and iron scale as binders. The creep in compression tests was carried out on 7 fired bricks with different residual quartz contents according to the standard GB/T 5073—2005. The results show that the test can be divided into three stages from room temperature to the end of creep according to the change of deformation rate. The distinct expansion stage occurs from room temperature to 900 ℃, and the expansion is positively correlated to the residual quartz content. The distinct shrinkage stage appears from 900 to 1 450 ℃, and the shrinkage is negatively correlated to the residual quartz content. The creep tends to be steady at 1 450 ℃, and the samples with a low residual quartz content show a better stability. The creep curve of silica brick obtained based on GB/T 5073 is not consistent with the expansion or contraction during the whole heating process. At the creep temperature (i.e., ≤1 470 ℃), cristobalite will translate to tridymite, and the samples with a low residual quartz content tend to be negative (i.e., shrinkage), while those with a high residual quartz content are positive (i.e., expansion). The residual quartz content has an influence on the creep process. It could be questionable to evaluate creep high-temperature performance of silica brick just according to GB/T 5073—2005 creep test method.

, authors=Xiuhua ZHANG1, Yong LI1, Zhihong Tian2, Qingyao ZHENG1, Dongming XING1, Xian HE1, Jun BO3, authorsList=Xiuhua ZHANG, Yong LI, Zhihong Tian, Qingyao ZHENG, Dongming XING, Xian HE, Jun BO, authorCompany=null, correspAuthors=Yong LI, authorNote=

ZHANG Xiuhua (1978-), famale, Ph.D.. E-mail:

, correspAuthorsNote=
LI Yong (1964-), male, Ph.D., Professor. E-mail:
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以结晶硅石为原料、石灰乳及铁鳞为结合剂,成型后经隧道窑1450 ℃烧成制得硅砖。取残余石英含量(按YB/T 172测量)不同的烧后砖7块,按照GB/T 5073—2005进行压蠕变实验。结果表明:样品的蠕变特性按形变率变化可分为3个阶段:分别为室温至900 ℃左右的明显膨胀,膨胀量与残余石英量呈正相关;900 ℃至1450 ℃的明显收缩,收缩量与残石英量呈负相关;1450 ℃恒温期间趋于稳态蠕变状态,残余石英量低的样品蠕变曲线变化较平缓。按照GB/T 5073得到的蠕变曲线与硅砖在整个加热升温过程的膨胀或收缩不一致,因蠕变温度≤1470 ℃,方石英最终将向鳞石英转变,低残余石英量的样品可能为负值(收缩),高残余石英量的样品通常为正值(膨胀)。残余石英量对蠕变结果影响大,只是按GB/T 5073—2005压蠕变实验方法评述硅砖蠕变性能对准确评价硅砖的高温性能易产生歧义。

, authors=张秀华1, 李勇1, 田志宏2, 郑清瑶1, 邢东明1, 和弦1, 薄钧3, authorsList=张秀华, 李勇, 田志宏, 郑清瑶, 邢东明, 和弦, 薄钧, authorCompany=null, correspAuthors=李勇, authorNote=

张秀华(1978—),女,博士研究生。

, correspAuthorsNote=
李勇(1964—),男,博士,教授。
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ZHANG Xiuhua (1978-), famale, Ph.D.. E-mail:

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压蠕变实验方法对硅砖蠕变结果的适应性探究
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张秀华 1 , 李勇 1 , 田志宏 2 , 郑清瑶 1 , 邢东明 1 , 和弦 1 , 薄钧 3
硅酸盐学报 | 2020,48(9): 1505-1510
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硅酸盐学报 | 2020 , 48 (9) : 1505 -1510
压蠕变实验方法对硅砖蠕变结果的适应性探究
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张秀华(1978—),女,博士研究生。

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postcode=null, companyName=null, departmentName=null, remark=3.中钢耐火材料有限公司,河南 洛阳 471039)])])]
张秀华1 , 李勇1 , 田志宏2, 郑清瑶1, 邢东明1, 和弦1, 薄钧3
作者信息
  • 1.北京科技大学材料科学与工程学院,北京 100083
  • 2.中冶建筑研究总院有限公司,北京 100088
  • 3.中钢耐火材料有限公司,河南 洛阳 471039
通讯作者:
李勇(1964—),男,博士,教授。
作者简介:

张秀华(1978—),女,博士研究生。

Evaluation of Creep Results of Silica Brick by Creep Test Method
Xiuhua ZHANG1 , Yong LI1 , Zhihong Tian2, Qingyao ZHENG1, Dongming XING1, Xian HE1, Jun BO3
Affiliations
  • 1.School of Material Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China
  • 2.China Metallurgical Research Institute Co., Ltd. Beijing 100088, China
  • 3.Sinosteel refractory Co., LTD, Luoyang, 471039, Henan, China
  • Corresponding Author:
    LI Yong (1964-), male, Ph.D., Professor. E-mail:

    ZHANG Xiuhua (1978-), famale, Ph.D.. E-mail:

出版时间: 2020-09-20 doi: 10.14062/j.issn.0454-5648.20190733
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以结晶硅石为原料、石灰乳及铁鳞为结合剂,成型后经隧道窑1450 ℃烧成制得硅砖。取残余石英含量(按YB/T 172测量)不同的烧后砖7块,按照GB/T 5073—2005进行压蠕变实验。结果表明:样品的蠕变特性按形变率变化可分为3个阶段:分别为室温至900 ℃左右的明显膨胀,膨胀量与残余石英量呈正相关;900 ℃至1450 ℃的明显收缩,收缩量与残石英量呈负相关;1450 ℃恒温期间趋于稳态蠕变状态,残余石英量低的样品蠕变曲线变化较平缓。按照GB/T 5073得到的蠕变曲线与硅砖在整个加热升温过程的膨胀或收缩不一致,因蠕变温度≤1470 ℃,方石英最终将向鳞石英转变,低残余石英量的样品可能为负值(收缩),高残余石英量的样品通常为正值(膨胀)。残余石英量对蠕变结果影响大,只是按GB/T 5073—2005压蠕变实验方法评述硅砖蠕变性能对准确评价硅砖的高温性能易产生歧义。

硅砖  /  高温蠕变  /  残余石英  /  鳞石英  /  方石英

Industrial silica bricks were obtained in tunnel kiln by sintering at 1450 ℃ with crystalline silica as a raw material, and lime milk and iron scale as binders. The creep in compression tests was carried out on 7 fired bricks with different residual quartz contents according to the standard GB/T 5073—2005. The results show that the test can be divided into three stages from room temperature to the end of creep according to the change of deformation rate. The distinct expansion stage occurs from room temperature to 900 ℃, and the expansion is positively correlated to the residual quartz content. The distinct shrinkage stage appears from 900 to 1 450 ℃, and the shrinkage is negatively correlated to the residual quartz content. The creep tends to be steady at 1 450 ℃, and the samples with a low residual quartz content show a better stability. The creep curve of silica brick obtained based on GB/T 5073 is not consistent with the expansion or contraction during the whole heating process. At the creep temperature (i.e., ≤1 470 ℃), cristobalite will translate to tridymite, and the samples with a low residual quartz content tend to be negative (i.e., shrinkage), while those with a high residual quartz content are positive (i.e., expansion). The residual quartz content has an influence on the creep process. It could be questionable to evaluate creep high-temperature performance of silica brick just according to GB/T 5073—2005 creep test method.

silica bricks  /  creep  /  residual quartz  /  tridymite  /  cristobalite
张秀华, 李勇, 田志宏, 郑清瑶, 邢东明, 和弦, 薄钧. 压蠕变实验方法对硅砖蠕变结果的适应性探究. 硅酸盐学报, 2020 , 48 (9) : 1505 -1510 . DOI: 10.14062/j.issn.0454-5648.20190733
Xiuhua ZHANG, Yong LI, Zhihong Tian, Qingyao ZHENG, Dongming XING, Xian HE, Jun BO. Evaluation of Creep Results of Silica Brick by Creep Test Method[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (9) : 1505 -1510 . DOI: 10.14062/j.issn.0454-5648.20190733
  • 国家自然科学基金(51872023)
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2020年第48卷第9期
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doi: 10.14062/j.issn.0454-5648.20190733
  • 接收时间:2019-11-08
  • 首发时间:2026-10-29
  • 出版时间:2020-09-20
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  • 收稿日期:2019-11-08
  • 修回日期:2019-12-25
基金
国家自然科学基金(51872023)
作者信息
    1.北京科技大学材料科学与工程学院,北京 100083
    2.中冶建筑研究总院有限公司,北京 100088
    3.中钢耐火材料有限公司,河南 洛阳 471039

通讯作者:

李勇(1964—),男,博士,教授。
参考文献
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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