Article(id=1322636217993249340, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636193100050547, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20200181, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1584374400000, receivedDateStr=2020-03-17, revisedDate=1586275200000, revisedDateStr=2020-04-08, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270647762, onlineDateStr=2026-10-29, pubDate=1600531200000, pubDateStr=2020-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270647762, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270647762, creator=13701087609, updateTime=1793270647762, updator=13701087609, issue=Issue{id=1322636193100050547, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='9', pageStart='1353', pageEnd='1510', issueExtLink='null', onlineDate='null', pubDate='1594569600000', pubDateStr='2020-07-13', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270641826, creator='13701087609', updateTime=1793270641826, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=1405, endPage=1413, ext={EN=ArticleExt(id=1322636218177798717, articleId=1322636217993249340, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Dielectric Properties and Impedance of BaTiO₃@Ag Core-shell Composite Ceramic, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Silver (Ag) was coated on the surface of nano-sized BaTiO₃ powder by a chemical coating method, and BaTiO₃@Ag composite ceramic was prepared by a solid-state method. The effect of Ag content on the composition, fracture surface microstructure, dielectric properties, and impedance spectroscopy of ceramics were investigated. The results indicate that BaTiO₃@Ag composite ceramic is a core-shell structure, and the main phase is a pure perovskite phase. BaTiO₃@Ag composite ceramic contains fine and homogeneous grains. The dielectric constant and loss decrease with increasing of Ag content and the δ_min is 0.004 87. The curie peaks widen, and the diffusion factor γ increases from 1.08 to 1.42. The thermal stability is improved due to the Ag introduction. The temperature stability coefficient decreases from 0.194 0 to 0.004 8. In addition, the dielectric relaxation of BaTiO₃@Ag composite ceramic occurs at 200 ℃. The conductance activation energy and relaxation activation energy determined by impedance spectroscopy show that the relaxation phenomena occurs due to the short jump of the defective dipoles, which are formed by the conducting electrons generated from the double ionization of the oxygen vacancy and the surrounding ions.

, authors=Cuiying MA, Huiling DU, Jia LIU, Xian DU, Ke YU, Xueyan XI, Hongpei RAN, authorsList=Cuiying MA, Huiling DU, Jia LIU, Xian DU, Ke YU, Xueyan XI, Hongpei RAN, authorCompany=null, correspAuthors=Huiling DU, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322636218408485438, articleId=1322636217993249340, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=核-壳结构BaTiO₃@Ag复合陶瓷的介电性能及阻抗谱, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用化学沉淀法还原制备了不同Ag含量[0%、1%、3%、5%（质量分数）]包覆的BaTiO₃纳米颗粒，通过烧结制备出BaTiO₃@Ag复合陶瓷。研究了复合陶瓷的相组成、微观形貌、介电性能以及阻抗谱。结果表明：Ag包覆后BaTiO₃颗粒呈“核-壳”结构，主相为单一钙钛矿相，烧结陶瓷晶粒细化均匀。随着Ag包覆量的增加，BaTiO₃@Ag复合陶瓷的峰值介电常数和损耗均降低，损耗最小为0.00487。Curie峰弥散展宽，弥散因子γ从1.08提高到1.42。温度稳定性提高，介电常数温度稳定性系数TCP由0.194降低到0.0048。另外，BaTiO₃@Ag复合陶瓷在200 ℃左右出现热激活介电弛豫现象，阻抗谱计算拟合所得电导激活能和弛豫激活能表明，此类弛豫现象由氧空位的双电离产生的导电电子与周围离子形成的缺陷偶极子短程跳跃所引起。

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MA Cuiying (1984-), female, Doctoral candidate. E-mail: mcy@xust.edu.cn

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马翠英（1984—），女，博士研究生。

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马翠英（1984—），女，博士研究生。

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