Article(id=1322636211773092119, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322636193100050547, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190744, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1573401600000, receivedDateStr=2019-11-11, revisedDate=1575820800000, revisedDateStr=2019-12-09, acceptedDate=null, acceptedDateStr=null, onlineDate=1793270646279, onlineDateStr=2026-10-29, pubDate=1600531200000, pubDateStr=2020-09-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793270646279, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793270646279, creator=13701087609, updateTime=1793270646279, updator=13701087609, issue=Issue{id=1322636193100050547, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='9', pageStart='1353', pageEnd='1510', issueExtLink='null', onlineDate='null', pubDate='1594569600000', pubDateStr='2020-07-13', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793270641826, creator='13701087609', updateTime=1793270641826, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext=null, issueFiles=null, downloadFileDto=null}, startPage=1430, endPage=1436, ext={EN=ArticleExt(id=1322636212469346584, articleId=1322636211773092119, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Interfacial Microstructure and Mechanical Property of ZrO2 Joints Brazed with Ni-Ti Filler Metal, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

ZrO2 ceramics were brazed with Ni-Ti filler metal. The microstructure of the joint and the effect of holding time on the interfacial microstructure and mechanical property were investigated. The results show that TiO+Ni2Ti4O layer is formed at the interface of ceramic and filler metal at 1 350 ℃ for 10 min. TiO distributes as a discontinuous layer next to the ceramic, while Ni2Ti4O is a continuous layer. The center of brazing seam consists of NiTi and Ni3Ti. TiO decreases and finally disappears, the thickness of Ni2Ti4O layer increases with the increase of holding time. Some cracks appear in Ni2Ti4O layer when the holding time is 40 min. The shear strength of the joints firstly increases and then decreases with increasing holding time. The shear strength of the joint reaches the maximum value of 88.7 MPa when the holding time is 30 min.

, authors=Qi ZHANG1, 2, Juan WANG2, 3, 4, Kaihong ZHENG2, 3, 4, Hongwang YANG1, authorsList=Qi ZHANG, Juan WANG, Kaihong ZHENG, Hongwang YANG, authorCompany=null, correspAuthors=Juan WANG, authorNote=

ZHANG Qi (1994-), male, Doctorial candidate. E-mail:

, correspAuthorsNote=
WANG Juan (1981-), female, Ph.D., Professor. E-mail:
, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322636212955885849, articleId=1322636211773092119, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=Ni-Ti钎料钎焊ZrO2陶瓷的界面组织及接头的力学性能, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用Ni-Ti钎料实现ZrO2陶瓷自身的钎焊连接,研究接头组织结构以及钎焊保温时间对界面组织和力学性能的影响。结果表明:在1350 ℃保温10 min的钎焊条件下,陶瓷与钎料界面处生成TiO+Ni2Ti4O反应层,TiO紧靠陶瓷呈非连续层状分布,Ni2Ti4O呈连续层状分布,焊缝中心区域由NiTi和Ni3Ti构成。随着保温时间的延长,反应层中TiO逐渐减少直至消失,Ni2Ti4O层的厚度逐渐增大;当保温时间为40 min时,Ni2Ti4O层中出现明显的裂纹。接头剪切强度随着保温时间的延长呈先增大后减小的趋势,当保温时间为30 min时,接头剪切强度达到最大值88.7 MPa。

, authors=张琦1, 2, 王娟2, 3, 4, 郑开宏2, 3, 4, 杨红旺1, authorsList=张琦, 王娟, 郑开宏, 杨红旺, authorCompany=null, correspAuthors=王娟, authorNote=

张琦(1994—),男,博士研究生。

, correspAuthorsNote=
王娟(1981—),女,博士,教授。
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Ni-Ti钎料钎焊ZrO2陶瓷的界面组织及接头的力学性能
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张琦 1, 2 , 王娟 2, 3, 4 , 郑开宏 2, 3, 4 , 杨红旺 1
硅酸盐学报 | 2020,48(9): 1430-1436
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硅酸盐学报 | 2020 , 48 (9) : 1430 -1436
Ni-Ti钎料钎焊ZrO2陶瓷的界面组织及接头的力学性能
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张琦(1994—),男,博士研究生。

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张琦1, 2 , 王娟2, 3, 4 , 郑开宏2, 3, 4, 杨红旺1
作者信息
  • 1.沈阳工业大学材料科学与工程学院,沈阳 110870
  • 2.广东省科学院广东省材料与加工研究所,广州 510650
  • 3.广东省金属强韧化技术与应用重点实验室,广州 510650
  • 4.广州市先进金属结构材料重点实验室,广州 510650
通讯作者:
王娟(1981—),女,博士,教授。
作者简介:

张琦(1994—),男,博士研究生。

Interfacial Microstructure and Mechanical Property of ZrO2 Joints Brazed with Ni-Ti Filler Metal
Qi ZHANG1, 2 , Juan WANG2, 3, 4 , Kaihong ZHENG2, 3, 4, Hongwang YANG1
Affiliations
  • 1.School of Materials Science and Engineering, Shenyang University of Technology, Shenyang 110870, China
  • 2.Guangdong Institute of Materials and Processing, Guangdong Academy of Science, Guangzhou 510650, China
  • 3.Guangdong Key Laboratory for Technology and Application of Metal Toughening, Guangzhou 510650, China
  • 4.Guangzhou Key Laboratory of Advanced Structural Metal Materials, Guangzhou 510650, China
  • Corresponding Author:
    WANG Juan (1981-), female, Ph.D., Professor. E-mail:

    ZHANG Qi (1994-), male, Doctorial candidate. E-mail:

出版时间: 2020-09-20 doi: 10.14062/j.issn.0454-5648.20190744
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采用Ni-Ti钎料实现ZrO2陶瓷自身的钎焊连接,研究接头组织结构以及钎焊保温时间对界面组织和力学性能的影响。结果表明:在1350 ℃保温10 min的钎焊条件下,陶瓷与钎料界面处生成TiO+Ni2Ti4O反应层,TiO紧靠陶瓷呈非连续层状分布,Ni2Ti4O呈连续层状分布,焊缝中心区域由NiTi和Ni3Ti构成。随着保温时间的延长,反应层中TiO逐渐减少直至消失,Ni2Ti4O层的厚度逐渐增大;当保温时间为40 min时,Ni2Ti4O层中出现明显的裂纹。接头剪切强度随着保温时间的延长呈先增大后减小的趋势,当保温时间为30 min时,接头剪切强度达到最大值88.7 MPa。

镍钛钎料  /  氧化锆陶瓷  /  钎焊  /  界面组织  /  剪切强度

ZrO2 ceramics were brazed with Ni-Ti filler metal. The microstructure of the joint and the effect of holding time on the interfacial microstructure and mechanical property were investigated. The results show that TiO+Ni2Ti4O layer is formed at the interface of ceramic and filler metal at 1 350 ℃ for 10 min. TiO distributes as a discontinuous layer next to the ceramic, while Ni2Ti4O is a continuous layer. The center of brazing seam consists of NiTi and Ni3Ti. TiO decreases and finally disappears, the thickness of Ni2Ti4O layer increases with the increase of holding time. Some cracks appear in Ni2Ti4O layer when the holding time is 40 min. The shear strength of the joints firstly increases and then decreases with increasing holding time. The shear strength of the joint reaches the maximum value of 88.7 MPa when the holding time is 30 min.

nickel-titanium filler metal  /  zirconia ceramics  /  brazing  /  interfacial microstructure  /  shear strength
张琦, 王娟, 郑开宏, 杨红旺. Ni-Ti钎料钎焊ZrO2陶瓷的界面组织及接头的力学性能. 硅酸盐学报, 2020 , 48 (9) : 1430 -1436 . DOI: 10.14062/j.issn.0454-5648.20190744
Qi ZHANG, Juan WANG, Kaihong ZHENG, Hongwang YANG. Interfacial Microstructure and Mechanical Property of ZrO2 Joints Brazed with Ni-Ti Filler Metal[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (9) : 1430 -1436 . DOI: 10.14062/j.issn.0454-5648.20190744
  • 广东省科学院建设国内一流研究机构行动专项(2019GDASYL-0501014)
  • 广州市科技计划项目(201906040007)
  • 广东省重点研发项目(2019B010942001)
  • 广东特支计划项目(2017TQ04C645)
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2020年第48卷第9期
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doi: 10.14062/j.issn.0454-5648.20190744
  • 接收时间:2019-11-11
  • 首发时间:2026-10-29
  • 出版时间:2020-09-20
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  • 收稿日期:2019-11-11
  • 修回日期:2019-12-09
基金
广东省科学院建设国内一流研究机构行动专项(2019GDASYL-0501014)
广州市科技计划项目(201906040007)
广东省重点研发项目(2019B010942001)
广东特支计划项目(2017TQ04C645)
作者信息
    1.沈阳工业大学材料科学与工程学院,沈阳 110870
    2.广东省科学院广东省材料与加工研究所,广州 510650
    3.广东省金属强韧化技术与应用重点实验室,广州 510650
    4.广州市先进金属结构材料重点实验室,广州 510650

通讯作者:

王娟(1981—),女,博士,教授。
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2种不同金属材料的力学参数
科
Family
属数
Number of
genus
种数
Number of
species
占总种数比例
Percentage of
total species (%)
属
Genus
种数
Number of
species
占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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