Article(id=1322622806290977484, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322622757339250965, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.2020.07.20190684, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1571068800000, receivedDateStr=2019-10-15, revisedDate=1575820800000, revisedDateStr=2019-12-09, acceptedDate=null, acceptedDateStr=null, onlineDate=1793267450163, onlineDateStr=2026-10-29, pubDate=1595174400000, pubDateStr=2020-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793267450163, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793267450163, creator=13701087609, updateTime=1793267450163, updator=13701087609, issue=Issue{id=1322622757339250965, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='7', pageStart='939', pageEnd='1144', issueExtLink='null', onlineDate='null', pubDate='1595174400000', pubDateStr='2020-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793267438492, creator='13701087609', updateTime=1793277091258, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663244053992200, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322622757339250965, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663244053992201, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322622757339250965, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1134, endPage=1144, ext={EN=ArticleExt(id=1322622808119694030, articleId=1322622806290977484, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Controllable Preparation and Decorative Effect of Iron-based Crystalline Glazes, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

Based on the study of ancient black glazed porcelains, high-fired glazes of SiO₂-Al₂O_3-K₂O-MgO-CaO-Fe₂O₃ system were designed and prepared. Different glaze decoration effects were achieved by changing the firing schedules to modify the crystallization behavior and microstructure of the glazes. The influence of thermal history on the crystal attribute and morphology, glaze appearance and coloring mechanism was investigated by using optical microscopy, field emission scanning electron microscopy, electron backscattered diffraction, X-ray diffraction and Raman spectroscopy, respectively. ε-Fe₂O₃ crystalline layer was prepared in a slight oxidation atmosphere at about 1 000-1 050 ℃. The results show that α-Fe₂O₃ crystals precipitated on the glaze surface have a good orientation and a variety of morphologies, which are related to the crystallization position and the direction of the crystallization plane. α-Fe₂O₃ crystals on the glaze surface show a silvery metallic luster, which belongs to a physical structural color.

, authors=Mei LI^{1, 2, 3}, Weidong LI^{1, 3}, Xiaoke LU^{1, 3}, Changsong XU^{1, 3}, authorsList=Mei LI, Weidong LI, Xiaoke LU, Changsong XU, authorCompany=null, correspAuthors=Weidong LI, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322622808358769359, articleId=1322622806290977484, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=铁系结晶釉的可控制备与装饰效果, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

以古代黑釉瓷研究为基础，设计并制备SiO₂-Al₂O₃-K₂O-MgO-CaO-Fe₂O₃多元系统高温釉。通过改变烧成制度调控釉的析晶行为和显微结构，得到了外观各异的釉面装饰效果。利用光学显微镜、场发射扫描电子显微镜、电子背散射衍射仪、X射线衍射仪和Raman光谱仪，分析了热历史对析晶种类及其形貌的影响规律，研究了釉面外观的影响因素及呈色机理，并在1 000~1 050 ℃弱氧化的气氛下成功制备了ε-Fe₂O₃析晶层。结果表明：釉表面析出的α-Fe₂O₃晶体具有较好的取向排列及多种显微形貌，与器物的析晶位置和析晶面的方向有关。表面析晶的α-Fe₂O₃呈银色金属光泽，属于物理结构色。

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LI Mei(1995-), female, Master candidate. E-mail: limei@student.sic.ac.cn

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LI Mei(1995-), female, Master candidate. E-mail: limei@student.sic.ac.cn

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李玫（1995—），女，硕士研究生。

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