Article(id=1322622798737035924, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322622757339250965, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190668, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1570636800000, receivedDateStr=2019-10-10, revisedDate=1575907200000, revisedDateStr=2019-12-10, acceptedDate=null, acceptedDateStr=null, onlineDate=1793267448362, onlineDateStr=2026-10-29, pubDate=1595174400000, pubDateStr=2020-07-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793267448362, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793267448362, creator=13701087609, updateTime=1793267448362, updator=13701087609, issue=Issue{id=1322622757339250965, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='7', pageStart='939', pageEnd='1144', issueExtLink='null', onlineDate='null', pubDate='1595174400000', pubDateStr='2020-07-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793267438492, creator='13701087609', updateTime=1793277091258, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663244053992200, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322622757339250965, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663244053992201, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322622757339250965, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=1114, endPage=1121, ext={EN=ArticleExt(id=1322622798934168213, articleId=1322622798737035924, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Crystallization Kinetics of R₂O-CaO-Al₂O₃-SiO₂-F Glass-Ceramics, columnId=1263922769897599102, journalTitle=Journal of the Chinese Ceramic Society, columnName=Research Articles, runingTitle=null, highlight=null, articleAbstract=

R₂O-CaO-SiO₂-Al₂O₃-F (RCSAF) glass-ceramics were prepared via melting method. The nucleation and crystal growth kinetics of RCSAF glass-ceramics were analyzed by thermogravimetric analysis and X-ray diffraction. The nucleation and crystal growth kinetics of the glass-ceramics were obtained by Gaussian fitting. The temperature-time-transition (T-T-T) curve of R₂O-CaO-SiO₂-Al₂O₃-F glass-ceramics under non-isothermal heating conditions was obtained, and the Gaussian fitting of glass-ceramics and crystal growth kinetics were obtained. The crystallization kinetic parameters including the crystallization apparent activation energy (E_a) and the crystallization index (n) were also measured with Ozawa and JMA methods (i.e. E_a=357.74 kJ/mol, n=3.13). Effects of time, temperature and precipitated crystal phase on the crystallization rate curve of R₂O-CaO-SiO₂-Al₂O₃-F glass-ceramics were established. The CaF₂ crystal particles precipitated from glass-ceramics were uniformly distributed in canasite and α-canasite. The crystal precipitation process of RCSAF glass-ceramics was further verified by typical crystal structure presented in scanning electron microscopic images.

, authors=Qingchao ZHAO¹, Hang YANG¹, Jianwei CAO², Weiguang LI¹, Shifu SHEN¹, Haiying LIU¹, authorsList=Qingchao ZHAO, Hang YANG, Jianwei CAO, Weiguang LI, Shifu SHEN, Haiying LIU, authorCompany=null, correspAuthors=Hang YANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322622799152272022, articleId=1322622798737035924, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=R₂O-CaO-SiO₂-Al₂O₃-F系微晶玻璃析晶动力学, columnId=1263922770220560512, journalTitle=硅酸盐学报, columnName=研究论文, runingTitle=null, highlight=null, articleAbstract=

以熔融法制备的R₂O-CaO-SiO₂-Al₂O₃-F（RCSAF）系微晶玻璃为研究对象，利用热重分析、X射线衍射等手段分析微晶玻璃的形核和晶体生长动力学。借助Gaussian拟合，获得了微晶玻璃的形核和晶体生长动力学函数。并绘制了非等温加热条件下R₂O-CaO-SiO₂-Al₂O₃-F系微晶玻璃的温度-时间-转变（T-T-T）曲线，获得了微晶玻璃形核和晶体生长动力学Gaussian拟合函数关系模型。通过无模式函数模型计算得知微晶玻璃的析晶活化能E_a=357.74 kJ/mol，析晶指数n=3.13，微晶玻璃以整体析晶的方式析出晶体。确立了时间、温度和析出晶相对R₂O-CaO-SiO₂-Al₂O₃-F系微晶玻璃析晶率曲线的影响规律。微晶玻璃析出的CaF₂晶体颗粒均匀弥散的分布于硅碱钙石和α-硅碱钙石中，扫描电子显微镜照片呈现的典型晶体结构进一步验证了RCSAF系微晶玻璃的晶体析出过程。

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