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Article(id=1322612349152899261, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.2020.05.20190745, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1573401600000, receivedDateStr=2019-11-11, revisedDate=1575388800000, revisedDateStr=2019-12-04, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264956987, onlineDateStr=2026-10-29, pubDate=1589904000000, pubDateStr=2020-05-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264956987, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264956987, creator=13701087609, updateTime=1793264956987, updator=13701087609, issue=Issue{id=1322612265061306700, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='5', pageStart='615', pageEnd='786', issueExtLink='null', onlineDate='null', pubDate='1589904000000', pubDateStr='2020-05-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264936938, creator='13701087609', updateTime=1793276961694, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322662700602208333, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322662700602208334, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612265061306700, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=718, endPage=722, ext={EN=ArticleExt(id=1322612349316477118, articleId=1322612349152899261, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Temperature Dependence of Viscosity and Fragility of Ge10As40Se50 Chalcogenide Glass, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The viscosity of Ge10As40Se50 chalcogenide glass was investigated by fiber elongation and rotation methods. The Vogel-Fulcher-Tammann equation was proposed as an optimal fitting model after comparing to the accuracy of different equations. GexAsySe1-x-y glasses were compared according to the fragility, m, derived from the Angell plot. The network structure of Ge10As40Se50 chalcogenide glass was investigated by X-ray photoelectron spectroscopy (XPS). The results show that the fragility change of GexAsySe1-x-y glasses follows the topological constraint theory in the range of the average coordination numbers (i.e., r=2.0-2.6). The m of GexAsySe1-x-y glasses decreases as r increases. However, the m does not strictly decrease as r increases when r is greater than 2.2. Based on the XPS results, Ge10As40Se50 chalcogenide glass exists Se chain in the network structure, thus affecting the stability and results at a greater m.

, authors=Peng ZHOU1, Hua ZHAO1, Chengkui ZU1, Tengxiao GUO2, Jianjie XU2, Yonghua LIU1, Haizheng TAO3, Kaiwen SHI3, Rui ZHANG1, Wei CHEN1, authorsList=Peng ZHOU, Hua ZHAO, Chengkui ZU, Tengxiao GUO, Jianjie XU, Yonghua LIU, Haizheng TAO, Kaiwen SHI, Rui ZHANG, Wei CHEN, authorCompany=null, correspAuthors=Chengkui ZU, authorNote=

ZHOU Peng (1990-), male, Master candidate. E-mail:

, correspAuthorsNote=
ZU Chengkui (1964-), male, Ph.D., Professor. E-mail:
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采用纤维伸长法、旋转法测试了Ge10As40Se50硫系玻璃的黏度。通过比较不同方程的准确性，确定Vogel-Fulcher-Tammann方程为该玻璃黏度拟合的最优模型，推导出玻璃黏度随温度的变化关系，根据Angell图计算其强弱性指数m，与其他GexAsySe1-x-y玻璃的m进行比较，采用X射线光电子能谱仪对其网络结构进行分析。结果表明：在平均配位数r为2.0~2.6区间内，GexAsySe1-x-y系统玻璃的动力学强弱性整体的变化趋势符合拓扑约束理论，表现为随着r变大，GexAsySe1-x-y系统的m整体上呈现降低的趋势，但是当r大于2.2，m值并不严格随着r的变大而减小，r为2.6的Ge10As40Se50硫系玻璃存在的Se链结构影响了网络结构稳定性，导致其强弱性指数m偏高。

, authors=周鹏1, 赵华1, 祖成奎1, 郭腾霄2, 徐建洁2, 刘永华1, 陶海征3, 石凯文3, 张瑞1, 陈玮1, authorsList=周鹏, 赵华, 祖成奎, 郭腾霄, 徐建洁, 刘永华, 陶海征, 石凯文, 张瑞, 陈玮, authorCompany=null, correspAuthors=祖成奎, authorNote=

周鹏（1990—），男，硕士研究生。

, correspAuthorsNote=
祖成奎（1964—），男，博士，教授。
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ZHOU Peng (1990-), male, Master candidate. E-mail:

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ZHOU Peng (1990-), male, Master candidate. E-mail:

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周鹏（1990—），男，硕士研究生。

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周鹏（1990—），男，硕士研究生。

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Ge10As40Se50硫系玻璃黏温性能及动力学强弱性
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周鹏 1 , 赵华 1 , 祖成奎 1 , 郭腾霄 2 , 徐建洁 2 , 刘永华 1 , 陶海征 3 , 石凯文 3 , 张瑞 1 , 陈玮 1
硅酸盐学报 | 2020,48(5): 718-722
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硅酸盐学报 | 2020 , 48 (5) : 718 -722
Ge10As40Se50硫系玻璃黏温性能及动力学强弱性
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周鹏1 , 赵华1, 祖成奎1 , 郭腾霄2, 徐建洁2, 刘永华1, 陶海征3, 石凯文3, 张瑞1, 陈玮1
作者信息
  • 1．中国建筑材料科学研究总院有限公司玻璃科学研究院，北京 100024
  • 2．国民核生化灾害防护国家重点实验室，北京 102205
  • 3．硅酸盐建筑材料国家重点实验室，武汉理工大学，武汉 430070
通讯作者:
祖成奎（1964—），男，博士，教授。
作者简介:

周鹏（1990—），男，硕士研究生。

Temperature Dependence of Viscosity and Fragility of Ge10As40Se50 Chalcogenide Glass
Peng ZHOU1 , Hua ZHAO1, Chengkui ZU1 , Tengxiao GUO2, Jianjie XU2, Yonghua LIU1, Haizheng TAO3, Kaiwen SHI3, Rui ZHANG1, Wei CHEN1
Affiliations
  • 1.Institute of Glass Science, China Building Material Academy, Beijing 100024, China
  • 2.National Key Laboratory of Nuclear and Biochemical Disaster Prevention, Beijing 102205, China
  • 3.State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan 430070, China
    • Corresponding Author:
    ZU Chengkui (1964-), male, Ph.D., Professor. E-mail:

    ZHOU Peng (1990-), male, Master candidate. E-mail:

出版时间: 2020-05-20 doi: 10.14062/j.issn.0454-5648.2020.05.20190745
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采用纤维伸长法、旋转法测试了Ge10As40Se50硫系玻璃的黏度。通过比较不同方程的准确性，确定Vogel-Fulcher-Tammann方程为该玻璃黏度拟合的最优模型，推导出玻璃黏度随温度的变化关系，根据Angell图计算其强弱性指数m，与其他GexAsySe1-x-y玻璃的m进行比较，采用X射线光电子能谱仪对其网络结构进行分析。结果表明：在平均配位数r为2.0~2.6区间内，GexAsySe1-x-y系统玻璃的动力学强弱性整体的变化趋势符合拓扑约束理论，表现为随着r变大，GexAsySe1-x-y系统的m整体上呈现降低的趋势，但是当r大于2.2，m值并不严格随着r的变大而减小，r为2.6的Ge10As40Se50硫系玻璃存在的Se链结构影响了网络结构稳定性，导致其强弱性指数m偏高。

硫系玻璃  /  黏温特性  /  强弱特性  /  网络结构

The viscosity of Ge10As40Se50 chalcogenide glass was investigated by fiber elongation and rotation methods. The Vogel-Fulcher-Tammann equation was proposed as an optimal fitting model after comparing to the accuracy of different equations. GexAsySe1-x-y glasses were compared according to the fragility, m, derived from the Angell plot. The network structure of Ge10As40Se50 chalcogenide glass was investigated by X-ray photoelectron spectroscopy (XPS). The results show that the fragility change of GexAsySe1-x-y glasses follows the topological constraint theory in the range of the average coordination numbers (i.e., r=2.0-2.6). The m of GexAsySe1-x-y glasses decreases as r increases. However, the m does not strictly decrease as r increases when r is greater than 2.2. Based on the XPS results, Ge10As40Se50 chalcogenide glass exists Se chain in the network structure, thus affecting the stability and results at a greater m.

chalcogenide glass  /  temperature dependence of viscosity  /  fragility  /  network structure
周鹏, 赵华, 祖成奎, 郭腾霄, 徐建洁, 刘永华, 陶海征, 石凯文, 张瑞, 陈玮. Ge10As40Se50硫系玻璃黏温性能及动力学强弱性. 硅酸盐学报, 2020 , 48 (5) : 718 -722 . DOI: 10.14062/j.issn.0454-5648.2020.05.20190745
Peng ZHOU, Hua ZHAO, Chengkui ZU, Tengxiao GUO, Jianjie XU, Yonghua LIU, Haizheng TAO, Kaiwen SHI, Rui ZHANG, Wei CHEN. Temperature Dependence of Viscosity and Fragility of Ge10As40Se50 Chalcogenide Glass[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (5) : 718 -722 . DOI: 10.14062/j.issn.0454-5648.2020.05.20190745
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  • 国家自然基金(60808024)
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2020年第48卷第5期
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doi: 10.14062/j.issn.0454-5648.2020.05.20190745
  • 接收时间：2019-11-11
  • 首发时间：2026-10-29
  • 出版时间：2020-05-20
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  • 收稿日期：2019-11-11
  • 修回日期：2019-12-04
基金
国家自然基金(60808024)
作者信息
    1．中国建筑材料科学研究总院有限公司玻璃科学研究院，北京 100024
    2．国民核生化灾害防护国家重点实验室，北京 102205
    3．硅酸盐建筑材料国家重点实验室，武汉理工大学，武汉 430070

通讯作者:

祖成奎（1964—），男，博士，教授。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.2020.05.20190745
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2种不同金属材料的力学参数
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Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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