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Article(id=1322612315145483225, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612228126265395, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190488, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1562774400000, receivedDateStr=2019-07-11, revisedDate=1569859200000, revisedDateStr=2019-10-01, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264948878, onlineDateStr=2026-10-29, pubDate=1587312000000, pubDateStr=2020-04-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264948878, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264948878, creator=13701087609, updateTime=1793264948878, updator=13701087609, issue=Issue{id=1322612228126265395, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='4', pageStart='463', pageEnd='614', issueExtLink='null', onlineDate='null', pubDate='1587312000000', pubDateStr='2020-04-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264928132, creator='13701087609', updateTime=1793276729826, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322661728073138752, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612228126265395, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322661728073138753, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612228126265395, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=584, endPage=591, ext={EN=ArticleExt(id=1322612315573302234, articleId=1322612315145483225, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Preparation and Properties of Corrosion Inhibitor-Loaded Hollow Silica Microspheres, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

Polystyrene microspheres were prepared via an emulsion polymerization method and used as hard templates to form hollow mesoporous silica microspheres. The structural properties of silica microspheres were characterized by scanning electron microscopy, transmission electron microscopy, thermogravity analysis, small angle X-ray diffraction, nitrogen adsorption-desorption isotherm analysis. The effects of synthesis parameters (i.e., amounts of ammonia and silane precursor) on the microsphere size, thickness and mesopore size of silica microspheres were investigated, and the optimum reaction conditions were 6.25 mL of ammonia and 10 g of tetraethylorthosilicate. The hollow microspheres as a host are loaded with benzotriazole, and then coated with a two-layer polyelectrolyte shell by a layer-by-layer deposition process. The inhibitor release profile revealed that the polyelectrolyte shell lowered the release rate of benzotriazole-loaded hollow silica microspheres by 5 times.

, authors=Jiawen CAI1, Yue LI2, 3, Chunchun WU2, 3, Xingeng DING1, Hui YANG1, 2, 3, authorsList=Jiawen CAI, Yue LI, Chunchun WU, Xingeng DING, Hui YANG, authorCompany=null, correspAuthors=Yue LI, authorNote=

CAI Jiawen (1995-), male, Master candidate. E-mail:

, correspAuthorsNote=
LI Yue (1988-), male, Ph.D., Assistant Research Fellow. E-mail:
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以乳液聚合法制备的聚苯乙烯微球为模板制备中空介孔二氧化硅微球，经扫描电子显微镜、透射电子显微镜、热重分析、小角度X射线衍射、氮气吸附-脱附等手段对制备得到的中空微球进行性能结构表征。考察了氨水和硅源前驱体用量等制备条件对中空微球的尺寸、介孔孔径、球壳厚度等的影响，6.25 mL氨水和10 g正硅酸乙酯的用量为最佳制备条件。中空SiO2微球作为载体，负载缓蚀剂苯并三氮唑，并对负载缓蚀剂的微球表面进行高分子双电层的修饰，释放曲线实验表明，高分子双电层修饰使微球中缓蚀剂释放速率降低5倍。

, authors=蔡佳文1, 李跃2, 3, 吴春春2, 3, 丁新更1, 杨辉1, 2, 3, authorsList=蔡佳文, 李跃, 吴春春, 丁新更, 杨辉, authorCompany=null, correspAuthors=李跃, authorNote=

蔡佳文（1995—），男，硕士研究生。

, correspAuthorsNote=
李跃（1988—），男，博士，助理研究员。
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CAI Jiawen (1995-), male, Master candidate. E-mail:

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CAI Jiawen (1995-), male, Master candidate. E-mail:

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蔡佳文（1995—），男，硕士研究生。

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蔡佳文（1995—），男，硕士研究生。

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缓蚀剂负载中空SiO2微球的制备及性能
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蔡佳文 1 , 李跃 2, 3 , 吴春春 2, 3 , 丁新更 1 , 杨辉 1, 2, 3
硅酸盐学报 | 2020,48(4): 584-591
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硅酸盐学报 | 2020 , 48 (4) : 584 -591
缓蚀剂负载中空SiO2微球的制备及性能
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2.浙江大学浙江-加州国际纳米技术研究院，杭州 310058
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蔡佳文1 , 李跃2, 3 , 吴春春2, 3, 丁新更1, 杨辉1, 2, 3
作者信息
  • 1.浙江大学材料科学与工程学院，杭州 310058
  • 2.浙江大学浙江-加州国际纳米技术研究院，杭州 310058
  • 3.浙江大学台州研究院，浙江 台州 318000
通讯作者:
李跃（1988—），男，博士，助理研究员。
作者简介:

蔡佳文（1995—），男，硕士研究生。

Preparation and Properties of Corrosion Inhibitor-Loaded Hollow Silica Microspheres
Jiawen CAI1 , Yue LI2, 3 , Chunchun WU2, 3, Xingeng DING1, Hui YANG1, 2, 3
Affiliations
  • 1.School of Materials Science and Engineering, Zhejiang University, Hangzhou 310058, China
  • 2.Zhejiang-California Nano-Systems Institute, Zhejiang University, Hangzhou 310058, China
  • 3.Research Institute of Zhejiang University-Taizhou, Taizhou 318000, Zhejiang, China
    • Corresponding Author:
    LI Yue (1988-), male, Ph.D., Assistant Research Fellow. E-mail:

    CAI Jiawen (1995-), male, Master candidate. E-mail:

出版时间: 2020-04-20 doi: 10.14062/j.issn.0454-5648.20190488
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摘要
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以乳液聚合法制备的聚苯乙烯微球为模板制备中空介孔二氧化硅微球，经扫描电子显微镜、透射电子显微镜、热重分析、小角度X射线衍射、氮气吸附-脱附等手段对制备得到的中空微球进行性能结构表征。考察了氨水和硅源前驱体用量等制备条件对中空微球的尺寸、介孔孔径、球壳厚度等的影响，6.25 mL氨水和10 g正硅酸乙酯的用量为最佳制备条件。中空SiO2微球作为载体，负载缓蚀剂苯并三氮唑，并对负载缓蚀剂的微球表面进行高分子双电层的修饰，释放曲线实验表明，高分子双电层修饰使微球中缓蚀剂释放速率降低5倍。

二氧化硅微球  /  聚苯乙烯微球  /  苯并三氮唑  /  缓释释放

Polystyrene microspheres were prepared via an emulsion polymerization method and used as hard templates to form hollow mesoporous silica microspheres. The structural properties of silica microspheres were characterized by scanning electron microscopy, transmission electron microscopy, thermogravity analysis, small angle X-ray diffraction, nitrogen adsorption-desorption isotherm analysis. The effects of synthesis parameters (i.e., amounts of ammonia and silane precursor) on the microsphere size, thickness and mesopore size of silica microspheres were investigated, and the optimum reaction conditions were 6.25 mL of ammonia and 10 g of tetraethylorthosilicate. The hollow microspheres as a host are loaded with benzotriazole, and then coated with a two-layer polyelectrolyte shell by a layer-by-layer deposition process. The inhibitor release profile revealed that the polyelectrolyte shell lowered the release rate of benzotriazole-loaded hollow silica microspheres by 5 times.

silicon dioxide microspheres  /  polystyrene microspheres  /  benzotriazole  /  sustained release
蔡佳文, 李跃, 吴春春, 丁新更, 杨辉. 缓蚀剂负载中空SiO2微球的制备及性能. 硅酸盐学报, 2020 , 48 (4) : 584 -591 . DOI: 10.14062/j.issn.0454-5648.20190488
Jiawen CAI, Yue LI, Chunchun WU, Xingeng DING, Hui YANG. Preparation and Properties of Corrosion Inhibitor-Loaded Hollow Silica Microspheres[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (4) : 584 -591 . DOI: 10.14062/j.issn.0454-5648.20190488
基金
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  • 浙江省重点研发计划(018C04007)
  • 金属防腐功能涂层材料与应用技术创新团队项目
  • 中央高校基本科研业务费专项资金资助（面向海洋防腐功能材料应用技术研究）
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2020年第48卷第4期
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文章信息
doi: 10.14062/j.issn.0454-5648.20190488
  • 接收时间：2019-07-11
  • 首发时间：2026-10-29
  • 出版时间：2020-04-20
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出版历史
  • 收稿日期：2019-07-11
  • 修回日期：2019-10-01
基金
浙江省重点研发计划(018C04007)
金属防腐功能涂层材料与应用技术创新团队项目
中央高校基本科研业务费专项资金资助（面向海洋防腐功能材料应用技术研究）
作者信息
    1.浙江大学材料科学与工程学院，杭州 310058
    2.浙江大学浙江-加州国际纳米技术研究院，杭州 310058
    3.浙江大学台州研究院，浙江 台州 318000

通讯作者:

李跃（1988—），男，博士，助理研究员。
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https://castjournals.cast.org.cn/joweb/gsyxb/CN/10.14062/j.issn.0454-5648.20190488
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2种不同金属材料的力学参数
科
Family		 属数
Number of
genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
species (%)
鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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