Article(id=1322612227920740896, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190273, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1556035200000, receivedDateStr=2019-04-24, revisedDate=1556985600000, revisedDateStr=2019-05-05, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264928082, onlineDateStr=2026-10-29, pubDate=1584633600000, pubDateStr=2020-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264928082, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264928082, creator=13701087609, updateTime=1793264928082, updator=13701087609, issue=Issue{id=1322612191723897081, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='3', pageStart='325', pageEnd='462', issueExtLink='null', onlineDate='null', pubDate='1584633600000', pubDateStr='2020-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264919452, creator='13701087609', updateTime=1793277037156, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663017125368549, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663017125368550, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=455, endPage=462, ext={EN=ArticleExt(id=1322612228122067489, articleId=1322612227920740896, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=ZIF-67 and Its Mother Liquor Derived Co₃O₄ as Catalyst Precursors for Hydrolysis of Ammonia Borane to Generate Hydrogen, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

ZIF-67 as one kind of zeolitic imidazolate frameworks was synthesized by a conventional precipitation method, and the mother liquor was concentrated and crystallized to recover cobalt-based compounds. For AB hydrolysis, two kinds of Co₃O₄ catalyst precursors (i.e., Co₃O₄-S and Co₃O₄-L) were prepared from the ZIF-67 and recovered compounds via calcination treatment, respectively. The morphology and phase composition of the samples were characterized by field-emission scanning electron microscopy and X-ray diffraction, respectively. Effects of AB and catalyst concentration and reaction temperature on the hydrogen generation rates and kinetics were investigated. The results show that Co₃O₄-S has a porous and polyhedral structure, and Co₃O₄-L is composed of nanoparticles. In addition, increasing AB and catalyst concentration can enhance the hydrogen generation rates. The maximum hydrogen production rates do not decline in the presence of Co₃O₄-S, but decrease to 78% of the initial level in the presence of Co₃O₄-L after recycling for four times.

, authors=Lei WEI, Hongyan LIU, Dongsheng WANG, Qian WANG, Liwen MA, authorsList=Lei WEI, Hongyan LIU, Dongsheng WANG, Qian WANG, Liwen MA, authorCompany=null, correspAuthors=null, authorNote=, correspAuthorsNote=null, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322612228352754210, articleId=1322612227920740896, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=ZIF-67及其母液衍生Co₃O₄催化氨硼烷水解制氢, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

采用常规液相沉淀反应合成了沸石咪唑酯金属有机骨架化合物ZIF-67，并对母液进行浓缩结晶以回收钴基化合物。通过高温焙烧的方式将ZIF-67及其母液转化为2种Co₃O₄（记作Co₃O₄-S和Co₃O₄-L）作为氨硼烷水解的催化剂前驱体。考察了反应液中氨硼烷浓度、催化剂浓度和反应温度对体系产氢速率的影响，并进行动力学分析。结果表明：Co₃O₄-S为多孔多面体结构而Co₃O₄-L为纳米颗粒；增加反应液中氨硼烷浓度和催化剂浓度有助于提升体系的产氢速率；经4次循环使用后，Co₃O₄-S催化产氢速率无衰减，Co₃O₄-L催化产氢速率为初始值的78%。

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WEI Lei (1986-), male, Ph.D., Associate Professor.. E-mail: weilei@lfnu.edu.cn

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WEI Lei (1986-), male, Ph.D., Associate Professor.. E-mail: weilei@lfnu.edu.cn

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魏磊（1986—），男，博士，副教授。

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魏磊（1986—），男，博士，副教授。

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