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Article(id=1322612211026084239, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190285, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1556380800000, receivedDateStr=2019-04-28, revisedDate=1557244800000, revisedDateStr=2019-05-08, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264924054, onlineDateStr=2026-10-29, pubDate=1584633600000, pubDateStr=2020-03-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264924054, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264924054, creator=13701087609, updateTime=1793264924054, updator=13701087609, issue=Issue{id=1322612191723897081, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='3', pageStart='325', pageEnd='462', issueExtLink='null', onlineDate='null', pubDate='1584633600000', pubDateStr='2020-03-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264919452, creator='13701087609', updateTime=1793277037156, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322663017125368549, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322663017125368550, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322612191723897081, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=391, endPage=398, ext={EN=ArticleExt(id=1322612211328074128, articleId=1322612211026084239, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Hydrothermal Aging of Zirconia Ceramics Consolidated by Oscillatory Pressure Sintering, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

The use of zirconia ceramics in humid environments is limited by the phase transformation from the tetragonal phase to the monoclinic phase. In this study, an oscillatory pressure sintering (OPS) technique was developed for the preparation of zirconia ceramics that were characterized by high density, fine grain size and excellent mechanical properties. The hydrothermal aging behaviors of the oscillatory pressure sintered and hot-pressed zirconia were investigated. The Raman analysis showed strong peaks at 178 and 189 cm-1 in both the oscillatory pressure sintered and the hot-pressed specimens, but the peak intensities of the oscillatory pressure sintered specimen were much weaker than those of the hot-pressed specimen. When the specimens were aged for 18 h, the flexural strength of the oscillatory pressure sintered zirconia reached approximately 1 216 MPa, which is much higher than that of the hot-pressed zirconia. Therefore, the OPS technique is promising for the preparation of zirconia ceramics that are used in the biomedical field.

, authors=Shuang LI1, Zhaolu Meng2, Zhipeng XIE3, Chuncheng WEI1, Peng WANG1, Lijuan ZHOU1, authorsList=Shuang LI, Zhaolu Meng, Zhipeng XIE, Chuncheng WEI, Peng WANG, Lijuan ZHOU, authorCompany=null, correspAuthors=null, authorNote=

LI Shuang (1981-), male, Ph.D., Associated Professor. E-mail:

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采用振荡压力烧结法制备了致密度高、晶粒细化、力学性能优异的氧化锆陶瓷，研究了水热老化时间对两种氧化锆陶瓷（振荡压力烧结OPS，热压烧结HP）的显微结构、相变及力学性能的作用规律及机制。Raman分析表明：随着老化时间的延长，2种材料中单斜相氧化锆的含量缓慢增加，但OPS氧化锆在178、189 cm-1处的峰值强度显著低于HP氧化锆。水热老化导致氧化锆表面微裂纹、颗粒粗化等现象，当老化时间为18 h时OPS氧化锆和HP氧化锆的抗弯强度分别为1 216和878 MPa。纳米压痕测试表明：OPS氧化锆的力学参数显著优于HP氧化锆。因此，OPS烧结技术有望极大拓展氧化锆陶瓷在生物医学领域的应用。

, authors=李双1, 孟兆禄2, 谢志鹏3, 魏春城1, 王鹏1, 周立娟1, authorsList=李双, 孟兆禄, 谢志鹏, 魏春城, 王鹏, 周立娟, authorCompany=null, correspAuthors=null, authorNote=

李双（1 981—），男，博士，副教授。

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LI Shuang (1981-), male, Ph.D., Associated Professor. E-mail:

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LI Shuang (1981-), male, Ph.D., Associated Professor. E-mail:

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李双（1 981—），男，博士，副教授。

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李双（1 981—），男，博士，副教授。

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基于振荡压力烧结的氧化锆陶瓷水热老化行为
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李双 1 , 孟兆禄 2 , 谢志鹏 3 , 魏春城 1 , 王鹏 1 , 周立娟 1
硅酸盐学报 | 2020,48(3): 391-398
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硅酸盐学报 | 2020 , 48 (3) : 391 -398
基于振荡压力烧结的氧化锆陶瓷水热老化行为
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李双1 , 孟兆禄2, 谢志鹏3, 魏春城1, 王鹏1, 周立娟1
作者信息
  • 1.山东理工大学资源与环境工程学院，山东 淄博 255049
  • 2.潍坊市生态环境局临朐分局，山东 潍坊 262600
  • 3.清华大学材料学院，新型陶瓷与精细工艺国家重点实验室，北京 100084
作者简介:

李双（1 981—），男，博士，副教授。

Hydrothermal Aging of Zirconia Ceramics Consolidated by Oscillatory Pressure Sintering
Shuang LI1 , Zhaolu Meng2, Zhipeng XIE3, Chuncheng WEI1, Peng WANG1, Lijuan ZHOU1
Affiliations
  • 1.School of Resources and Environmental Engineering, Shandong University of Technology, Zibo 255049, Shandong, China
  • 2.Ecology and Environment Bureau of Weifang, Weifang 262600, Shandong, China
  • 3.State Key Laboratory of New Ceramics and Fine Processing, School of Materials Science and Engineering, Tsinghua University, Beijing 100084, China

    • LI Shuang (1981-), male, Ph.D., Associated Professor. E-mail:

出版时间: 2020-03-20 doi: 10.14062/j.issn.0454-5648.20190285
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采用振荡压力烧结法制备了致密度高、晶粒细化、力学性能优异的氧化锆陶瓷，研究了水热老化时间对两种氧化锆陶瓷（振荡压力烧结OPS，热压烧结HP）的显微结构、相变及力学性能的作用规律及机制。Raman分析表明：随着老化时间的延长，2种材料中单斜相氧化锆的含量缓慢增加，但OPS氧化锆在178、189 cm-1处的峰值强度显著低于HP氧化锆。水热老化导致氧化锆表面微裂纹、颗粒粗化等现象，当老化时间为18 h时OPS氧化锆和HP氧化锆的抗弯强度分别为1 216和878 MPa。纳米压痕测试表明：OPS氧化锆的力学参数显著优于HP氧化锆。因此，OPS烧结技术有望极大拓展氧化锆陶瓷在生物医学领域的应用。

振荡压力烧结  /  相变  /  抗弯强度  /  晶粒尺寸

The use of zirconia ceramics in humid environments is limited by the phase transformation from the tetragonal phase to the monoclinic phase. In this study, an oscillatory pressure sintering (OPS) technique was developed for the preparation of zirconia ceramics that were characterized by high density, fine grain size and excellent mechanical properties. The hydrothermal aging behaviors of the oscillatory pressure sintered and hot-pressed zirconia were investigated. The Raman analysis showed strong peaks at 178 and 189 cm-1 in both the oscillatory pressure sintered and the hot-pressed specimens, but the peak intensities of the oscillatory pressure sintered specimen were much weaker than those of the hot-pressed specimen. When the specimens were aged for 18 h, the flexural strength of the oscillatory pressure sintered zirconia reached approximately 1 216 MPa, which is much higher than that of the hot-pressed zirconia. Therefore, the OPS technique is promising for the preparation of zirconia ceramics that are used in the biomedical field.

oscillatory pressure sintering  /  phase transformation  /  flexural strength  /  grain size
李双, 孟兆禄, 谢志鹏, 魏春城, 王鹏, 周立娟. 基于振荡压力烧结的氧化锆陶瓷水热老化行为. 硅酸盐学报, 2020 , 48 (3) : 391 -398 . DOI: 10.14062/j.issn.0454-5648.20190285
Shuang LI, Zhaolu Meng, Zhipeng XIE, Chuncheng WEI, Peng WANG, Lijuan ZHOU. Hydrothermal Aging of Zirconia Ceramics Consolidated by Oscillatory Pressure Sintering[J]. Journal of the Chinese Ceramic Society, 2020 , 48 (3) : 391 -398 . DOI: 10.14062/j.issn.0454-5648.20190285
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  • 辽宁科技大学开放课题(USTLGCZX201804)
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doi: 10.14062/j.issn.0454-5648.20190285
  • 接收时间：2019-04-28
  • 首发时间：2026-10-29
  • 出版时间：2020-03-20
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  • 收稿日期：2019-04-28
  • 修回日期：2019-05-08
基金
辽宁科技大学开放课题(USTLGCZX201804)
作者信息
    1.山东理工大学资源与环境工程学院，山东 淄博 255049
    2.潍坊市生态环境局临朐分局，山东 潍坊 262600
    3.清华大学材料学院，新型陶瓷与精细工艺国家重点实验室，北京 100084
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2种不同金属材料的力学参数
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genus		 种数
Number of
species		 占总种数比例
Percentage of
total species (%)		 属
Genus		 种数
Number of
species		 占总种数比例
Percentage of total
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鹅膏菌科Amanitaceae 2 11 5.26 鹅膏菌属 Amanita 10 4.78
小菇科 Mycenaceae 2 12 5.74 丝盖伞属 Inocybe 5 2.39
多孔菌科 Polyporaceae 8 14 6.70 蜡蘑属 Laccaria 5 2.39
红菇科 Russulaceae 3 23 11.00 小皮伞属 Marasmius 6 2.87
小菇属 Mycena 11 5.26
光柄菇属 Pluteus 5 2.39
红菇属 Russula 17 8.13
栓菌属 Trametes 5 2.39
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