Article(id=1322609027192836228, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, articleNumber=null, orderNo=null, doi=10.14062/j.issn.0454-5648.20190432, pmid=null, cstr=null, oa=null, hot=null, price=null, onlineType=0, articleFormat=0, articleType=null, articleTypeStr=null, receivedDate=1555516800000, receivedDateStr=2019-04-18, revisedDate=1569513600000, revisedDateStr=2019-09-27, acceptedDate=null, acceptedDateStr=null, onlineDate=1793264164970, onlineDateStr=2026-10-29, pubDate=1582128000000, pubDateStr=2020-02-20, doiRegisterDate=null, doiRegisterDateStr=null, onlineIssueDate=1793264164970, onlineIssueDateStr=2026-10-29, onlineJustAcceptDate=null, onlineJustAcceptDateStr=null, onlineFirstDate=null, onlineFirstDateStr=null, sourceXml=null, magXml=null, createTime=1793264164970, creator=13701087609, updateTime=1793264164970, updator=13701087609, issue=Issue{id=1322608967147172356, tenantId=1146029695717560320, journalId=1263187385517883426, year='2020', volume='48', issue='2', pageStart='147', pageEnd='324', issueExtLink='null', onlineDate='null', pubDate='1582128000000', pubDateStr='2020-02-20', beforeIssueId=null, nextIssueId=null, price=null, status=1, issueComplete=1, articleOrder=1, issueType=-1, specialIssue=null, createTime=1793264150653, creator='13701087609', updateTime=1793276939599, updator='13701087609', preIssue=null, nextIssue=null, articleTotal=null, ext={EN=IssueExt(id=1322662607933255748, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=EN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=), CN=IssueExt(id=1322662607933255749, tenantId=1146029695717560320, journalId=1263187385517883426, issueId=1322608967147172356, language=CN, specialIssueTitle=, coverIllustrator=null, specialIssueEditor=, specialIssueAbout=)}, issueFiles=null, downloadFileDto=null}, startPage=246, endPage=252, ext={EN=ArticleExt(id=1322609027343831173, articleId=1322609027192836228, tenantId=1146029695717560320, journalId=1263187385517883426, language=EN, title=Influence of Hydrolysis Rate of Carboxylates on Dispersion Performance of Slow-release PolycarboxylateSuperplasticizer, columnId=null, journalTitle=Journal of the Chinese Ceramic Society, columnName=null, runingTitle=null, highlight=null, articleAbstract=

To study the influence of unsaturated carboxylate on the dispersing and flow releasing ability of slow-release polycarboxylate superplasticizer(PCE), the hydrolysis behaviors of carboxylates in sodium hydroxide solution at pH value of 12.0 was investigated, and the constants of hydrolysis rate were derived via a linear fitting. Mini slump was used to examine the variation of flow of cement pastes containing the synthesized slow releasing PCE over time, and the results were compared and analyzed to coordinate the relationship of hydrolysis behaviors of carboxylates and slow-release effectiveness of PCE. The results indicate that PCE with the substitution of acrylic acid with 33.3% methyl acrylate and 25.0% dimethyl itaconite showed significant slow-release effect, the initial fluidity of cement paste was 149 mm and 104 mm afterwards increased to 223 mm and 212 mm after 2 h respectively. PCE with carboxylate monomer of faster hydrolysis rate exhibited quicker flow releasing property, and PCE with carboxylate monomer containing more ester grouped manifested stronger flow releasing ability, but need longer time. The flow releasing property of PCE not only depended on the hydrolysis rate and ester group amount of monomer, but also related to its reactivity of monomer to match the copolymerization system.

, authors=Huiqun LI¹, Yan YAO^{1, 2}, Ziming WANG^{1, 3}, Suping CUI^{1, 3}, authorsList=Huiqun LI, Yan YAO, Ziming WANG, Suping CUI, authorCompany=null, correspAuthors=Ziming WANG, authorNote=, correspAuthorsNote=, copyrightStatement=null, copyrightOwner=null, extLink=null, articleAbsUrl=null, sourceXml=null, magXml=null, pdfUrl=null, pdf=null, pdfFileSize=null, pdfExtLink=null, richHtmlUrl=null, mobilePdfUrl=null, reviewReport=null, pdfFirstPage=null, abstractGraph=null, abstractGraphContent=null, abstractVideo=null, citation=null, cebUrl=null, magXmlContent=null, mapNumber=null, fund=null), CN=ArticleExt(id=1322609027570323590, articleId=1322609027192836228, tenantId=1146029695717560320, journalId=1263187385517883426, language=CN, title=羧酸酯水解速率对缓释型聚羧酸超塑化剂分散性能的影响, columnId=null, journalTitle=硅酸盐学报, columnName=, runingTitle=null, highlight=null, articleAbstract=

为研究羧酸酯单体对缓释型聚羧酸超塑化剂（PCE）缓释及其分散性能的影响，首先系统测定了不同结构的羧酸酯单体在pH=12.0的氢氧化钠溶液中水解率随反应时间的变化趋势，通过线性拟合得到羧酸酯的水解反应速率常数。以不同结构的不饱和羧酸酯作为功能单体制备缓释型聚羧酸超塑化剂，测定掺加缓释型聚羧酸超塑化剂水泥净浆流动度随时间的变化趋势。分析了羧酸酯的水解速率对超塑化剂的分散及缓释效果的影响。结果表明：丙烯酸甲酯和亚甲基丁二酸二甲酯各代替33.3%和25.0%的丙烯酸使PCE分散性能增强明显，水泥净浆流动度在2 h内分别从149 mm和104 mm增加到223 mm和212 mm；羧酸酯水解速率越快，所制备的PCE的缓释速率越快，达到最高分散性能所需的时间越短；所制备的PCE所含酯基越多，得到的PCE缓释能力越强，分散性能随时间增加越明显。聚羧酸超塑化剂的缓释效果不仅与所含羧酸酯的水解反应速率和可释放的羧基数量有关，还取决于其羧酸酯单体聚合活性与聚合反应体系的匹配程度。

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